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55 results about "Laboratory methods" patented technology

Polymerase Chain Reaction (PCR) PCR is a laboratory method used for making a very large number of copies of short sections of DNA from a very small sample of genetic material. This process is called "amplifying" the DNA and it enables specific genes of interest to be detected or measured.

Microwave homogeneous hydrothermal synthesis method of magnesium-aluminum hydrotalcite

The invention belongs to the field of preparation of inorganic materials, and particularly relates to a microwave homogeneous hydrothermal synthesis method of magnesium-aluminum hydrotalcite. The method comprises the following steps: weighing soluble magnesium nitrate, aluminum nitrate and urea according to a certain ratio, and dissolving in deionized water; subpackaging the solution in a microwave digestion tank, sealing, putting in a microwave digestion instrument, and performing microwave heating at a set temperature for a set time to quickly finish synthesis; and pouring out all solids and liquids in the microwave tank, washing with deionized water and anhydrous ethanol, performing vacuum drying, grinding, and storing. By adopting microwave radiation heating, the method provided by the invention has the characteristics of energy saving and high efficiency, can realize temperature and pressure on-line control, and has the advantages of high reproducibility and operational safety; meanwhile, the method does not need pH regulation, and is simple to operate; and the product is high in particle size uniformity. In general, the microwave homogeneous hydrothermal synthesis method established by the invention has the characteristic of being simple, quick and efficient to operate, and is a laboratory method for quickly synthesizing magnesium-aluminum hydrotalcite of a uniform particle size.
Owner:INTEGRATED TECHNICAL SERVICE CENT OF FUQING ENTRY EXIT INSPECTION & QUARANTINE BUREAU

Quick detection and evaluation method of harmful precipitated phase in two-phase stainless steel

The invention discloses a quick detection and evaluation method of harmful precipitated phase in two-phase stainless steel. The method comprises the following steps: S1, determining harmful phase content in two-phase stainless steel at different sensitization time by using a counting method and a ferrite instrument, and drawing two results as a relation graph; S2, determining the hardness of the two-phase stainless steel with different harmful phase contents, and drawing a relation graph of the harmful phase content and the hardness; S3, respectively performing solution corrosion and electrolytic corrosion on the two-phase stainless steel with different harmful phase contents, and observing the similarity of the metallographic structure of two corrosion methods, thereby acquiring a metallographic atlas; and S4, comparing with a field detection result according to relation graphs and the metallographic atlas, judging whether the harmful phase is existent in the two-phase steel in site,and estimating the volume fraction of the harmful phase. By establishing the correlation between an accurate laboratory method and an operable field method, whether the harmful phase is existent in the two-phase steel base material can be quickly judged in site, the method is simple and practical, and the time and cost for sampling to the laboratory to analyze are saved.
Owner:HEFEI GENERAL MACHINERY RES INST +1

Near-infrared measurement method applicable to real-time on-line measuring-point-free temperature compensation

The invention relates to a near-infrared measurement method applicable to real-time on-line measuring-point-free temperature compensation. The method comprises the following steps: measuring physical property parameter standard data by utilizing a laboratory method; acquiring the near infrared spectrum of a same sample under different temperature levels; performing preprocessing and principal component analysis on the acquired spectral data, and performing non-separated latent variable modeling on the temperature by using partial least squares so as to acquire a physical property parameter measurement value at the present moment; and acquiring a new spectral data set online, constructing an on-line recursive algorithm, updating the physical property parameter measurement value, and finishing near-infrared on-line measurement capable of achieving a measuring-point-free temperature compensation function. According to the method disclosed by the invention, the temperature serving as a non-separated latent factor variable participates in the near-infrared modeling process, and the recursive algorithm is formed based on the to-be-measured property parameters, so that the property parameter measurement under different temperatures can be finished by virtue of adaptation of the model on the temperature, and direct temperature measurement information and correlation calculation are not needed; and therefore, the established model has the high universality. The on-line recursive algorithm is not sensitive on sample temperature change, and the measurement result has a relatively small integrated error.
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