The invention discloses a flaky
copper powder preparation method and flaky
copper powder.The flaky
copper powder preparation method comprises the following steps that under the stirring condition, spherical copper powder, an
antioxidant A and a
grinding aid are dispersed in a
solvent, and a
mixed solution is obtained;
zirconium beads are added into the obtained
mixed solution for ball milling treatment, the
antioxidant B is added again in the ball milling process, and a
solid phase is obtained; the obtained
solid phase is washed and dried, and flaky copper powder is obtained; according to the preparation method, the flaky copper powder is prepared through a physical preparation method, the
antioxidant is added twice before ball milling and during ball milling, the
oxidation resistance of the copper powder can be effectively improved, the spherical copper powder, the antioxidant and the
grinding aid are dissolved in the
solvent to form the
mixed solution, the risk that the spherical copper powder is oxidized due to
exposure in air can be effectively reduced, and the service life of the spherical copper powder is prolonged. And finally, a
solid phase obtained after ball milling is subjected to acid
pickling to be used for removing surface oxides, and the prepared flaky copper powder is high in
oxidation resistance, good in flaky effect, smooth in surface, good in
conductivity, small in resistance and small in environmental
pollution.