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30results about How to "Meet the preparation requirements" patented technology

Preparation method of high-performance printing ink resin

The invention relates to plastic gravure printing ink resin, in particular to high-performance alcohol-water based printing ink resin and a preparation method thereof. The high-performance alcohol-water based printing ink resin in the invention is polyurethane grafted polyacrylate copolymer obtained by reaction of polyacrylate with a hydroxyl and polyurethane prepolymer with the end group of isocyanate. A polyurethane chain is introduced, thus the resin has good adhesive force to various plastic film substrate (BOPP (biaxially oriented polypropylene), PET (polyethylene terephthalate), PA (polyamide), PVC (polyvinyl chloride), PE (poly ethylene), PC (polycarbonate) and the like), adapts to various laminated adhesives (ester soluble ones and alcohol soluble ones) and has high combined strength. The preparation method of the plastic gravure printing ink resin in the invention is simple, and the prepared printing ink has good printing effect and strong adaptability, thus realizing integrated adaptation to the substrate and laminated adhesive and being capable of using for printing of various plastic substrates; no crosslinking component is required, tolerance to poaching at high temperature of 98 DEG C is achieved, operation is easy, and combined strength is high; and the resin is alcohol soluble, economic and environment-friendly and has a wide application prospect in the plastic gravure printing ink field.
Owner:CHENGDU XINJIN TUOZHAN PRINTING INK

Preparation method of polyacrylate-polyurethane resin binder for single-fluid general plastic gravure alcohol-soluble and water-soluble composite ink

The invention relates to a resin binder for the plastic gravure composite ink, in particular to a preparation method of a resin binder for the single-fluid general plastic gravure alcohol-soluble and water-soluble composite ink. The invention provides a preparation method of a polyacrylate-polyurethane resin binder for the single-fluid general plastic gravure alcohol-soluble and water-soluble composite ink. The method uses (methyl) acrylate, vinyl acetate, polymerizable polyurethane macromonomer and activated functional monomer as raw materials and is prepared by the radical polymerization of solution. As polyurethane branch chains are introduced, the composite ink has good adhesive force to various plastic film substrates such as BOPP, PET, PA, PVC, PE and PC, good printing adaptability and high combined strength, and can adapt to various laminating adhesives such as fat-soluble laminating adhesives and alcohol-soluble laminating adhesives. The preparation method of the resin binder for the ink is easy, the prepared ink has good printing effect and high adaptability and can be used for printing various plastic substrates; crosslinking component is not needed to use, the resin binder has convenient operation and high combined strength; the resin binder is alcohol-soluble, water-soluble, economical and environmentally friendly, and has wide application prospect in the plastic gravure composite ink field.
Owner:CHENGDU XINJIN TUOZHAN PRINTING INK

Agomelatine-containing medicinal composition

The invention provides an agomelatine-containing medicinal composition, which not only solves the problem of the dissolution of agomelatine in different crystal forms, but also meets the requirements of preparations for prescriptions and processes. The composition has the advantages of simple preparation process, convenience for operation, transport and storage, wide application range and suitability for large-scale production.
Owner:万全万特制药江苏有限公司

Cephalosporin ester drug particle in non-gel state after meeting water, and preparation method and application of drug particle

The invention relates to a cephalosporin ester drug particle in a non-gel state after meeting water, and a preparation method and an application of the drug particle, and belongs to the technical field of pharmaceutical preparations. The drug particle comprises the following raw and auxiliary materials: a cephalosporin ester drug with the bulk density of 0.1-0.3g / ml, and the following auxiliary materials accounting for the mass percentage of the cephalosporin ester drug as follows: 2-4.5% of micropowder silica gel, 2-4.5% of anti-gel adjuvant, and 12-16% of disintegrating agent, wherein the anti-gel adjuvant is a glidant and / or a lubricant with the bulk density greater than 0.50g / ml. According to the cephalosporin ester drug particle in the non-gel state after meeting the water, and the preparation method and the application of the drug particle, the problem that the dissolution rate is relatively low due to the fact that gelatinization is severe when the cephalosporin ester drug is dissolved out in the water in the prior art is solved, the dispersity and the hydrophilicity in a dissolution-out process are good, no gelatinization exists, and the dissolution rate is increased greatly.
Owner:SUZHOU CHUNGHWA CHEM & PHARMA IND

Health-care food

The invention relates to the technical field of health-care products, particularly to a health-care food. The health-care food comprises the following components: 15-25% of L-arabinose, 10-15% of polygonum multiflorum, 13-18% of fructus cannabis, 8-12 parts of platycladi seeds, 1-5% of black sesames and 3-8% of walnut kernels. The health-care food provided by the invention has strict formula, novel technique and unique technology, the prepared health-care food has the efficacies of tonifying and building the body, prolonging life, reducing fat to lose weight, moistening the intestines to relax the bowels, eliminating toxins to nourish the face, adjusting the internal secretion and enhancing the immunity and has good curative effect, and clinic applications prove that the effective rate reaches 100%. The preparation method is simple and easy to operate, the problem of crushing fineness of oily materials is solved, the oily materials can be crushed into fine powder or ultrafine powder, the formulation requirement is achieved, the effect of the health-care product is improved, and the bioavailability is increased.
Owner:SHENGQUAN HEALTANG

Clathrate compound of perphenazine cyclodextrin derivative, and preparation method thereof

The invention relates to a clathrate compound of a perphenazine cyclodextrin derivative, and a preparation method of the clathrate compound, aiming at solving the problems that perphenazine can not be dissolved in the water, and the medicine effect is low. The cyclodextrin derivative selected by the invention is hydroxypropyl-beta-cyclodextrin. The preparation method of the perphenazine hydroxypropyl-beta-cyclodextrin clathrate compound is simple in technology, easy to control, mild in clathration condition, short in production period and high in medicine content of the clathrate compound; and the clathrate compound can be mixed with pharmaceutic adjuvant to prepare any pharmaceutically acceptable oral administration preparation such as common tablets, orally disintegrating tablets, buccal tablets, etc.
Owner:CHINA PHARM UNIV

Device and method for preparing multiscale fiber reinforced composite material through electrostatic wire separating method

The invention discloses a device and a method for preparing a multiscale fiber reinforced composite material through the electric wire separating method. The device comprises a rack, a forming device,an electrostatic wire separating device and a powder paving device, wherein the electrostatic wire separating device comprises a wire separating table, a first press cake and a second press cake, wherein a wire pressing groove is formed in the upper part of the wire separating table; a wire separating table through hole is coaxial with a working table through hole; two groups of wire separating grooves are formed in the two sides of the wire pressing groove and are oppositely formed in the two sides of the wire separating table through hole; each group of wire separating groove comprises a plurality of parallel wire separating grooves; the first press cake and the second press cake are hinged to the bottom surface of the wire pressing groove; the forming device comprises a forming die anda convex die coaxially arranged; and the convex die is arranged in the forming die. The device can prepare multiscale fiber composite material and can prepare continuous fiber and chopped fiber reinforced composite materials simultaneously. The preparation method and the process are continuous, rapid and efficient, and the performance features of the continuous fiber and chopper fiber reinforcedcomposite materials can be taken into account.
Owner:SHAANXI UNIV OF SCI & TECH

Method for preparing transparent clay

The invention provides a method for preparing transparent clay, belongs to the technical field of a building material and can simulate physico-mechanical properties of the clay. The method is characterized in that the void fluid having a certain refractive index is obtained by mixing the white oil and the solvent oil according to a certain volume ratio, and a certain mass fraction of the vapor white carbon black powder is added to form slurry-like transparent soil; the alternating condition of the vacuum condition and the normal pressure, bubbles in the slurry-like transparent soil are removed; lastly, through pressured consolidation, the transparent clay having desired transparency is obtained. The method is advantaged in that the obtained transparent clay is simple and convenient to prepare, has fewer bubbles and has excellent cohesion and transparency, the clay can be used to study deformation characteristics of clay formations in the geotechnical engineering field, moreover, the transparent clay has good stability, can be used for simulating the natural clay and has good promotion value.
Owner:SHANGHAI CONSTRUCTION GROUP +1

Preparation method for high purity reactive black used for digital ink-jet printing

The invention discloses a preparation method for high purity reactive black used for digital ink-jet printing, which belongs to the technical field of the fine chemical industry. According to the method, reactive black is used as a raw material, the processes of removal of particle impurities by using a microfiltration membrane, desalination and purification by using a charged mosaic membrane and condensation by using a nanofiltration membrane are utilized, and therefore, a high purity liquid dye is prepared for preparation of digital ink-jet printing ink; to facilitate preservation and transport, the high purity liquid dye can undergo spray drying so as to prepare a high purity solid dye. A product in the invention has low content of impurities; in terms of the solid dye obtained after spray drying, Cl<-> is no more than 200 ppm, SO4<2-> is no more 400 ppm, Ca<++> is no more 800 ppm, Mg<++> is no more 400 ppm, and Fe<++> is no more 100 ppm; the product is applicable to preparation of digital printing ink. The method provided in the invention is simple and feasible, is convenient for industrial production and is easy to popularize and apply; the product prepared by using the method can substitute imported products, thereby reducing cost for enterprises and promoting development of the domestic digital printing industry.
Owner:ZHENGZHOU UNIV +1

Directly blendable seawater-based variable viscosity fracturing fluid and preparation method thereof

Belonging to the field of fracturing fluid, the invention particularly relates to a directly blendable seawater-based variable viscosity fracturing fluid and a preparation method thereof. The fracturing fluid comprises a seawater-based slickwater fracturing fluid and a seawater-based high-viscosity slickwater fracturing fluid; the seawater-based slickwater fracturing fluid comprises the followingcomponents, in terms of the total amount of the seawater-based slickwater fracturing fluid, 0.05%-0.15% of a thickening agent, 0.01%-0.03% of a synergist, 0.1%-0.2% of a bactericide and the balance seawater. The invention solves the problems of small fracturing scale and unsatisfactory fracturing effect caused by limited water storage space in offshore fracturing. Seawater resources are rich, thefracturing fluid can be prepared and used immediately during fracturing construction, thus effectively lowering the water consumption, storage and transportation cost of the fracturing fluid, and greatly shortening the construction period.
Owner:DAGANG OIL FIELD GRP +1

Yanlixiao capsule and preparation method thereof

The invention discloses a Yanlixiao capsule and a preparation method thereof. The Yanlixiao capsule is prepared from clove leaves through processing and is a pharmaceutical composition. The pharmaceutical composition does not contain any other raw and accessory materials except for components from the clove leaves. The preparation method for the pharmaceutical composition is characterized by comprising the following steps: (1) extracting clove leaves with water and concentrating the obtained water extract into clear paste with relative density of 1.23 to 1.27 (80 DEG C); (2) crushing clove leaves and then carrying out screening with a sieve No. 5 so as to obtain fine powder; and (3) uniformly mixing the fine powder prepared in the step (2) with the clear paste prepared in the step (1) anddrying the mixture so as to obtain the pharmaceutical composition. The Yanlixiao capsule provided by the invention is a purely traditional Chinese medicine, has substantial curative effect and small side-effect, and can overcome the problem of abuse of antibiotics; and the Yanlixiao capsule is free of any accessory material and has substantial better dissolution and stability than commercially available Yanlixiao capsules.
Owner:黑龙江迪龙制药有限公司

Solid preparation containing insoluble thienopyridine composition and preparation method thereof

The invention discloses a solid preparation containing an insoluble thienopyridine composition and a preparation method thereof. The preparation is low in impurity content and can be rapidly dissolvedout. According to the solid preparation containing the insoluble thienopyridine composition, the composition comprises a compound with a structure shown in a formula I and a compound with a structureshown in a formula II, wherein the mass ratio of the compound shown in the formula II to the compound shown in the formula I is smaller than or equal to 1: 100.
Owner:CHENGDU SHIBEIKANG BIOLOGICAL MEDICINE TECH CO LTD

Cholagogic pain-relieving capsule as well as preparation method and quality test and control method thereof

The invention discloses a cholagogic pain-relieving capsule as well as a preparation method and a quality test and control method thereof. In the invention, the existing cholagogic pain-relieving tablets are improved significantly by adding prescription dosage, adopting reduced pressure low temperature concentration technology or reduced pressure low temperature concentration plus spray drying, reducing moisture in the extract to increase the medicament concentration, thus satisfying the requirement for the medicament preparation and optimizing the preparation technique. Meanwhile, the invention also provides a qualitative and quantitative method for product quality test and control, wherein TLC method is selected for authenticating five drugs, HPLC method is adopted for detecting the content of naringin, thus the cholagogic pain-relieving capsule is secure and effective and has controllable quality.
Owner:YUNNAN YONGZITANG PHARMA

Compositions containing cationic compound, preparation method of skin external preparation, skin external preparation and application of compositions

The invention discloses compositions containing a cationic compound, a preparation method of a skin external preparation, the skin external preparation and an application of the compositions. One composition includes the following components: the cationic compound and a surfactant I; and a structural general formula of the surfactant I is R1-(M1)m-(N1)n-A1, wherein R1 is C10-C18 alkyl, M1 is a polyethylene glycol chain, N1 is a polypropylene glycol chain, m is any integer of 2 to 10, n is any integer of 0 to 10, and A1 is a dibasic acid ester salt or a polybasic acid salt. After the compositions containing the cationic compound provided by the invention are added to an anionic system, especially an anionic polymer system, a transparent and non-precipitating system can be obtained; and theprepared skin external preparation is still transparent and stable after being left for 3 months under accelerated test conditions, can meet the requirements of skin external preparations, has good antiseptic ability and no irritation to skin, and is safe to use.
Owner:上海尤文化工有限公司

Preparation method of integrated plastic gravure alcohol-soluble aqueous composite ink resin

ActiveCN102010485BPolarity can be effectively adjustedStrong adhesionInksSolubilityFunctional monomer
The invention relates to a resin for plastic gravure composite ink, in particular to an integrated plastic gravure alcohol-soluble aqueous composite ink resin and a preparation method thereof. In the preparation method of the integrated plastic gravure alcohol-soluble aqueous composite ink resin for gravure, the integrated plastic alcohol-soluble aqueous composite ink resin is obtained by polymerizing the raw materials of a polymerizable polyurethane macromonomer, (methyl) acrylic ester, vinylacetate and active functional monomer through solution radicals. Due to the introduction of a polyurethane chain, the ink has favorable adhesive force on various plastic film substrates (BOPP (Biaxially-oriented Polypropylene), PET (Polyethylene Terephthalate), PA (Polyamide), PVC (Polyvinyl Chloride), PE (Poly Ethylene), PC (Polycarbonate) and the like), good printing adaptability and high composite strength, adapts to various laminating glues (ester-soluble type, alcohol-soluble type), and can be boiled in water with the high temperature of 98 DEG C. The preparation method of the plastic gravure composite ink resin is simple, the prepared ink has good printing effect and strong adaptability, realizes the integrated adaption of the substrates and the laminating glues, and can be used for printing various plastic substrates; without using crosslinking components, the ink can be boiled in water with the high temperature of 98 DEG C and has the advantages of convenience in operation and high composite strength; the resin has alcohol solubility, economy, environmental protection and wideapplication prospect in the field of plastic gravure composite inks.
Owner:CHENGDU XINJIN TUOZHAN PRINTING INK

Multifunctional enemator

The invention provides a multifunctional enemator, and relates to the technical field of medical instrument cleaning. Comprising a liquid storage box, a material storage box, a liftable crushing box communicated with the liquid storage box and the material storage box, a liquid collection box arranged on the periphery of the crushing box and communicated with the crushing box in a filtering mode, a standby box communicated with the liquid collection box and a sausage filling pump communicated with the standby box, and at least part of pipelines, communicated with the crushing box, of the liquid storage box and the material storage box are flexible pipes. A crushing motor is arranged at the top of the crushing box, a crushing shaft extending into the crushing box is fixed to a main shaft of the crushing motor, crushing blades are arranged on the portion, extending into the crushing box, of the crushing shaft, a lifting electric pole is arranged at the bottom of the crushing box, and the liquid collecting box and the crushing box are in flexible sealing connection. And a heating evaporation device is arranged in the standby box. According to the invention, the sausage filling operation is changed from manual operation to mechanical operation, so that the workload is greatly reduced, the labor intensity is reduced, and the working efficiency is improved.
Owner:THE FIRST AFFILIATED HOSPITAL OF ARMY MEDICAL UNIV

Preparation method of polyacrylate-polyurethane resin binder for single-fluid general plastic gravure alcohol-soluble and water-soluble composite ink

ActiveCN101921374BPolarity can be effectively adjustedStrong adhesionInksEnvironmental resistanceFunctional monomer
The invention relates to a resin binder for the plastic gravure composite ink, in particular to a preparation method of a resin binder for the single-fluid general plastic gravure alcohol-soluble and water-soluble composite ink. The invention provides a preparation method of a polyacrylate-polyurethane resin binder for the single-fluid general plastic gravure alcohol-soluble and water-soluble composite ink. The method uses (methyl) acrylate, vinyl acetate, polymerizable polyurethane macromonomer and activated functional monomer as raw materials and is prepared by the radical polymerization ofsolution. As polyurethane branch chains are introduced, the composite ink has good adhesive force to various plastic film substrates such as BOPP, PET, PA, PVC, PE and PC, good printing adaptability and high combined strength, and can adapt to various laminating adhesives such as fat-soluble laminating adhesives and alcohol-soluble laminating adhesives. The preparation method of the resin binder for the ink is easy, the prepared ink has good printing effect and high adaptability and can be used for printing various plastic substrates; crosslinking component is not needed to use, the resin binder has convenient operation and high combined strength; the resin binder is alcohol-soluble, water-soluble, economical and environmentally friendly, and has wide application prospect in the plastic gravure composite ink field.
Owner:CHENGDU XINJIN TUOZHAN PRINTING INK

Device and method for preparing multi-scale fiber-reinforced composite materials by electrostatic filament separation

The invention discloses a device and a method for preparing a multiscale fiber reinforced composite material through the electric wire separating method. The device comprises a rack, a forming device,an electrostatic wire separating device and a powder paving device, wherein the electrostatic wire separating device comprises a wire separating table, a first press cake and a second press cake, wherein a wire pressing groove is formed in the upper part of the wire separating table; a wire separating table through hole is coaxial with a working table through hole; two groups of wire separating grooves are formed in the two sides of the wire pressing groove and are oppositely formed in the two sides of the wire separating table through hole; each group of wire separating groove comprises a plurality of parallel wire separating grooves; the first press cake and the second press cake are hinged to the bottom surface of the wire pressing groove; the forming device comprises a forming die anda convex die coaxially arranged; and the convex die is arranged in the forming die. The device can prepare multiscale fiber composite material and can prepare continuous fiber and chopped fiber reinforced composite materials simultaneously. The preparation method and the process are continuous, rapid and efficient, and the performance features of the continuous fiber and chopper fiber reinforcedcomposite materials can be taken into account.
Owner:SHAANXI UNIV OF SCI & TECH

Cephalosporin ester drug particle in non-gel state after meeting water, and preparation method and application of drug particle

The invention relates to a cephalosporin ester drug particle in a non-gel state after meeting water, and a preparation method and an application of the drug particle, and belongs to the technical field of pharmaceutical preparations. The drug particle comprises the following raw and auxiliary materials: a cephalosporin ester drug with the bulk density of 0.1-0.3g / ml, and the following auxiliary materials accounting for the mass percentage of the cephalosporin ester drug as follows: 2-4.5% of micropowder silica gel, 2-4.5% of anti-gel adjuvant, and 12-16% of disintegrating agent, wherein the anti-gel adjuvant is a glidant and / or a lubricant with the bulk density greater than 0.50g / ml. According to the cephalosporin ester drug particle in the non-gel state after meeting the water, and the preparation method and the application of the drug particle, the problem that the dissolution rate is relatively low due to the fact that gelatinization is severe when the cephalosporin ester drug is dissolved out in the water in the prior art is solved, the dispersity and the hydrophilicity in a dissolution-out process are good, no gelatinization exists, and the dissolution rate is increased greatly.
Owner:SUZHOU CHUNGHWA CHEM & PHARMA IND

A track-changing anti-twist wire rope braiding machine

The invention relates to the field of wire rope braiding for power transmission line pay-off, in particular to a track-changing anti-twist wire rope braiding machine. It is composed of machine base, gear transmission part, roller walking track part, shift fork part, and drum winding part: the machine base part has a machine base, and the outer peripheral part of the circular steel plate of the machine base is evenly distributed with the first transmission shaft, which is installed in the center. A group of central gear shafts, two sets of second transmission shafts distributed in the middle; the gear transmission part includes a large gear, a small gear, an incomplete gear, a central gear, a first transmission shaft, a second transmission shaft, a central gear shaft and a transmission The motor; the roller walking track part is composed of a track installation base, a fixed track, a movable track and a movable track fork; the fork part has a fork, and the fork is installed at the end of the first transmission shaft evenly distributed on the frame; the drum is wound The part includes bogie mechanism, support seat, roller and brake tensioning mechanism; the roller is installed on the upper part of the bogie mechanism, and the roller is equipped with a brake tensioning mechanism.
Owner:WUXI VOCATIONAL & TECHN COLLEGE

Stachyose health food

The invention relates to the technical field of health products, and particularly relates to a stachyose health food. The health food is prepared from the following components in parts by weight: 15-25 parts of stachyose, 10-15 parts of rhizoma atractylodis macrocephalae, 13-18 parts of apricot kernels, 8-12 parts of ginkgo seeds, 1-5 parts of acorn nut kernels and 3-8 parts of hazelnut kernels. The health food has a precise formula, novel technology and unique process, has the effects of nourishing and building bodies, prolonging lives, reducing lipid, reducing weight, relaxing bowels, removing toxicity, nourishing skin, regulating internal secretion and enhancing immunity, has a good curative effect, and has an effective rate of 100 percent in clinical verification; and the preparation method is simple and easy to operate, can be used for solving the problem for the crushing fineness of oily materials, can be used for crushing oily materials into fine powder or ultrafine powder to meet the requirement of preparations, so that the effect of the health food is improved, and biological utilization is improved.
Owner:威海紫光科技园有限公司

Preparation method for high purity reactive black used for digital ink-jet printing

The invention discloses a preparation method for high purity reactive black used for digital ink-jet printing, which belongs to the technical field of the fine chemical industry. According to the method, reactive black is used as a raw material, the processes of removal of particle impurities by using a microfiltration membrane, desalination and purification by using a charged mosaic membrane and condensation by using a nanofiltration membrane are utilized, and therefore, a high purity liquid dye is prepared for preparation of digital ink-jet printing ink; to facilitate preservation and transport, the high purity liquid dye can undergo spray drying so as to prepare a high purity solid dye. A product in the invention has low content of impurities; in terms of the solid dye obtained after spray drying, Cl<-> is no more than 200 ppm, SO4<2-> is no more 400 ppm, Ca<++> is no more 800 ppm, Mg<++> is no more 400 ppm, and Fe<++> is no more 100 ppm; the product is applicable to preparation of digital printing ink. The method provided in the invention is simple and feasible, is convenient for industrial production and is easy to popularize and apply; the product prepared by using the method can substitute imported products, thereby reducing cost for enterprises and promoting development of the domestic digital printing industry.
Owner:ZHENGZHOU UNIV +1

Large size ni-cr electrothermal alloy billet and hot working method

The invention discloses a large-sized Ni-Cr electrothermal alloy blank and a hot working method, belonging to the technical field of metallurgical production technology. Provided are a large-sized Ni-Cr electrothermal alloy blank and a hot working method with relatively high finished product quality and significant reduction in subsequent use costs. The large-sized Ni-Cr electrothermal alloy blank is a superalloy blank containing the following components in parts by weight, and the components in parts by weight are C≤0.05%, Si 0.9-1.60%, Al≤0.50%, Cr 20.0‑22.0%, Mn≤0.3%, Fe≤1.0%, P≤0.010%, S≤0.010%, Ti≤0.01%, Zr 0.1‑0.25%, Re≤0.2%, the balance is Ni and inevitable impurities , Among them, the tensile strength of the finished superalloy material is ≥760MPa, and the elongation rate is ≥55%. The thermal processing method first adopts vacuum induction melting + electroslag remelting to prepare Ni-Cr electrothermal alloy electroslag round ingots with a unit weight exceeding 1.2 tons according to the above-mentioned components in parts by weight, and then sequentially processes the electroslag round ingots. Forging and precision forging, and finally hot rolling to obtain material with a single weight of more than 800kg.
Owner:CHENGDU ADVANCED METAL MATERIALS IND TECH RES INST CO LTD

Synthesis method of electrolyte sample for sodium expansion rate test

The invention relates to a synthesis method of an electrolyte sample for sodium expansion rate test. The method comprises: proportioning cryolite, sodium fluoride, calcium fluoride and aluminum oxideaccording to a certain ratio, uniformly mixing the mixture, pouring the mixture into a graphite crucible, heating the mixture to a melting temperature, keeping the temperature for a certain time, andcontinuously stirring to escape bubbles during the period; and scooping out a melt by using a proper sampling tool, cooling the melt, and pouring the melt into a mold to form an electrolyte sample block, coarsely crushing a sample block to be less than 3mm by using a jaw crusher, dividing the sample into two parts, crushing one part to be about 1mm-2mm by using a double-roll crusher, grinding theother part by using a sample grinding machine to substances that can completely pass a 0.075 mm test sieve, and mixing the two parts of samples according to a certain ratio to obtain an electrolyte sample meeting the measurement of the sodium expansion rate. According to the method, the electrolyte sample for sodium expansion rate test is prepared by melting and particle size mixing, and the finalelectrolyte reagent can replace imported ones, is more economical and applicable, and can meet the preparation requirements of crucibles with different sizes.
Owner:GUIZHOU BRANCH CHINA ALUMINUM IND

Solid preparation containing insoluble thienopyridine composition and preparation method

The invention discloses a solid preparation containing an insoluble thienopyridine composition and a preparation method. The preparation is low in impurity content and can be rapidly dissolved out. According to the solid preparation containing the insoluble thienopyridine composition, disclosed by the invention, the composition comprises a compound with a structure represented by a formula I and acompound with a structure represented by a formula II, wherein a mass ratio of the compound II to the compound I is smaller than or equal to 1: 100.
Owner:CHENGDU SHIBEIKANG BIOLOGICAL MEDICINE TECH CO LTD

Preparation method of high-performance printing ink resin

ActiveCN102040726BPolarity can be effectively adjustedStrong adhesionInksEnvironmental resistanceWater based
The invention relates to plastic gravure printing ink resin, in particular to high-performance alcohol-water based printing ink resin and a preparation method thereof. The high-performance alcohol-water based printing ink resin in the invention is polyurethane grafted polyacrylate copolymer obtained by reaction of polyacrylate with a hydroxyl and polyurethane prepolymer with the end group of isocyanate. A polyurethane chain is introduced, thus the resin has good adhesive force to various plastic film substrate (BOPP (biaxially oriented polypropylene), PET (polyethylene terephthalate), PA (polyamide), PVC (polyvinyl chloride), PE (poly ethylene), PC (polycarbonate) and the like), adapts to various laminated adhesives (ester soluble ones and alcohol soluble ones) and has high combined strength. The preparation method of the plastic gravure printing ink resin in the invention is simple, and the prepared printing ink has good printing effect and strong adaptability, thus realizing integrated adaptation to the substrate and laminated adhesive and being capable of using for printing of various plastic substrates; no crosslinking component is required, tolerance to poaching at high temperature of 98 DEG C is achieved, operation is easy, and combined strength is high; and the resin is alcohol soluble, economic and environment-friendly and has a wide application prospect in the plastic gravure printing ink field.
Owner:CHENGDU XINJIN TUOZHAN PRINTING INK

Large-specification Ni-Cr electrothermal alloy blank and hot working method

The invention discloses a large-specification Ni-Cr electrothermal alloy blank and a hot working method, and belongs to the technical field of metallurgical production processes. According to the large-specification Ni-Cr electrothermal alloy blank and the hot working method, the finished product quality is relatively high, and the subsequent use cost is remarkably reduced. The large-specification Ni-Cr electrothermal alloy blank is a superalloy blank comprising the following components in parts by weight: less than or equal to 0.05% of C, 0.9-1.60% of Si, less than or equal to 0.50% of Al, 20.0-22.0% of Cr, less than or equal to 0.3% of Mn, less than or equal to 1.0% of Fe, less than or equal to 0.010% of P, less than or equal to 0.010% of S, less than or equal to 0.01% of Ti, 0.1-0.25% of Zr, less than or equal to 0.2% of Re and the balance being Ni and inevitable impurities, wherein tensile strength of a finished high-temperature alloy material is larger than or equal to 760 MPa, and ductility is larger than or equal to 55%. The hot working method comprises the following steps: firstly, preparing a Ni-Cr electrothermal alloy electroslag round ingot with the piece weight exceeding 1.2 tons by adopting vacuum induction melting and electroslag remelting according to the components in parts by weight; then carrying out quick forging and precision forging on the electroslag round ingot in sequence; and finally, carrying out hot rolling to obtain a material with the piece weight exceeding 800 kg.
Owner:CHENGDU ADVANCED METAL MATERIALS IND TECH RES INST CO LTD

A kind of purification method of bendamustine hydrochloride

The present invention relates to a purification method of bendamustine hydrochloride. The method comprises the following steps: (1) adding hydrochloric acid aqueous solution to the crude product of bendamustine hydrochloride, stirring and dissolving, and then adding activated carbon for decolorization; (2) adding Adding an inorganic alkali solution to the solution obtained in step (1) to adjust the pH of the solution to 1-4, then cooling, recrystallizing, and filtering to obtain a filter cake; (3) washing and drying the filter cake obtained in step (2) to obtain Bendamustine hydrochloride. By adopting the purification method of the present invention, the crude product of bendamustine hydrochloride can be obtained at low temperature and normal temperature to obtain high-purity bendamustine hydrochloride, avoiding the generation of new impurities under high temperature conditions, the product purity is above 99.8%, and all single impurities The content is all lower than 0.10%. The method has simple process, short cycle, a refining yield of more than 90%, good product quality, can meet preparation requirements, and is suitable for industrial production.
Owner:南京力成药业有限公司

A kind of synthetic method of the electrolyte sample that is used for sodium expansion rate test

The invention relates to a method for synthesizing an electrolyte sample used for sodium expansion rate testing, comprising: firstly mixing cryolite, sodium fluoride, calcium fluoride and alumina according to a certain ratio, then mixing the mixture and pouring it into graphite Heat the crucible to the melting temperature and keep it warm for a certain period of time, stirring constantly to make the bubbles escape. Then use a suitable sampling tool to scoop out the melt and cool it down to form an electrolyte sample block. The sample block is roughly crushed to less than 3mm with a jaw crusher, and the sample is divided into two parts: one part is crushed with a pair of rollers Machine crushed to about 1mm-2mm, one part of the sample ground by a sample mill completely passed through the 0.075mm test sieve, and the two parts of the sample were mixed in a certain proportion to obtain an electrolyte sample that meets the determination of the sodium expansion rate. The invention uses melting and particle size mixing to prepare electrolyte samples for the sodium expansion rate test, and the final electrolyte reagent can replace imports, is more economical and applicable, and can meet the preparation requirements of crucibles of different sizes.
Owner:GUIZHOU BRANCH CHINA ALUMINUM IND
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