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277 results about "Ultra high purity" patented technology

Production process of ultra-high-purity isopropanol

The invention discloses a production process of ultra-high-purity isopropanol, which comprises the following process steps of: (1) delivering a feed stream containing at least 98% of industrial grade isopropanol into a molecular sieve adsorption tower from the bottom of the molecular sieve adsorption tower, dehydrating through a molecular sieve, and then flowing out of the top of the tower to obtain high-purity isopropanol of which the moisture content is less than 100ppm; (2) filtering the high-purity isopropanol taken out of the molecular sieve adsorption tower by using a filter so as to remove particles of which the sizes are more than 1mum; and (3) transferring the high-purity isopropanol which is qualified by filtering into a distillation tower and a rectification column for rectifying, then transferring the rectified high-purity isopropanol into a condenser to be condensed into high-purity liquid isopropanol, enabling the condensed high-purity liquid isopropanol after rectifying to pass through a deionized resin tank, and deionizing through ionic resin so as to obtain ultra-high-purity isopropanol of which the metallic impurity is less than 0.1ppb. The production process disclosed by the invention is carried out under the normal pressure, and has the advantages of mild reaction conditions, simple operation processes and good safety performance.
Owner:JIANGSU DENOIR TECH CO LTD

Method for preparing vacuum zone melting high resistant silicon single crystal

The invention discloses a method for preparing vacuum zone melting high resistant silicon single crystal, comprising the two sequential major processes: polysilicon purification and crystal forming of silicon single crystal, wherein, the process of polysilicon purification comprises the steps of cleaning fire, charging, evacuating, preheating, melting materials heat sealing, growing narrow necks, shouldering, shoulder circuiting, equating diameter, ending and repeating; the process of crystal forming of silicon single crystal comprises the steps of cleaning fire, charging, evacuating, preheating, processing of chemicals, crystal seeding, shouldering, shoulder circuiting, equating diameter, ending and blowing out. With the method of the invention adopted to prepare silicon single crystal, electric resistivity, ultra-high purity, resistivity profile, uniformity of cross-section electric resistivity and minority carrier lifetime are greatly improved; purity of the silicon single crystal is above 11N, electric resistivity reaches 8000 omega/cm-30000omega/cm, uniformity of cross-section electric resistivity is less than 15%, and minority carrier lifetime is more than 600-1000Mus, thus greatly improving performance, stability and safety of the devices while realizing mass production of vacuum zone melting high resistant silicon single crystal.
Owner:峨嵋半导体材料研究所

Process method for ultra-high purity alumina preparation by utilizing coal ash and comprehensive utilization of ultra-high purity alumina

The invention discloses a process method for ultra-high purity alumina preparation by utilizing coal ash and comprehensive utilization of ultra-high purity alumina. In the process method, mechanical activation, flotation decarbonization, magnetic separation iron removal sulfuric acid aluminum lixiviation, solid-liquid separation, resin absorption iron removal, low-iron aluminum sulfate concentration, organic alcohol alcoholization acid washing, aluminum sulfate dehydration drying and aluminum sulfate high-temperature calcination are carried out on the coal ash so as to obtain ultra-high purity alpha-Al2O3, wherein the content of the Fe2O3 in the ultra-high purity alpha-Al2O3 is less than 2 ppm. By using the process method, the complicated purification problem that intermediate aluminum sulfate in the process of coal ash reclamation is necessarily subjected to a called Bayer circulation process is avoided, thereby simplifying the process flow, reducing the energy consumption, reducing the resource consumption and solving the technical problem of over-large secondary residue quantity accumulation. The process method has the advantages that the extraction efficiency is high, and the circulation recovery of organic alcohol and sulfuric acid and comprehensive utilization of byproducts such as resin and the like are achieved. In the invention, the process is simple, the process flow is short, the production process is easy to control, the content of the impurity in the product is low, and the quality of the product is stable.
Owner:内蒙古昶泰资源循环再生利用科技开发有限责任公司 +2

Method for treating stainless steel surfaces

The invention relates to a method for treating stainless steel surfaces, comprising the following steps of: burnishing, degreasing, decontaminating and cleaning the surfaces of stainless steel parts to be treated; carrying out electrochemical polishing to the burnished, degreased, decontaminated and cleaned stainless steel parts; passivating the electrochemically polished stainless steel parts; precisely cleaning the passivated stainless steel parts; purifying, drying and baking the precisely cleaned stainless steel parts; and inspecting the stainless steel parts in a dust-free room and carrying out double-layer anti-static packaging and vacuum sealing to the stainless steel parts. The stainless steel parts treated with the method meet the use requirements of high-end industries comprising semiconductor processing and equipment manufacturing, solar energy, micro-electronics, electric industry, restaurant and food, biological pharmaceutics, medicine and medical treatment, analytical instruments, petrifaction industries, aerospace and the like and completely accord with the regulations of the standards comprising SEMI (Semiconductor Equipment and Materials International), ASTM (American Society for Testing Material) and the like on the high cleanness and ultra-high purity (UHP) of the stainless steel surfaces.
Owner:BEIJING SEVENSTAR ELECTRONICS CO LTD

Continuous producing technique for ultra-high pure nitric acid

The invention relates to a process for continuously producing extra high purity nitric acid, which comprises the following steps: first, industrial grade 80-90% nitric acid raw material and double allyl 18-crown-6 ether organosilicon macromolecular complexing agent accounting for 0.2-2% of the weight of nitric acid raw material are mixed in a pretreater, then, the mixture is filtered by a micro-filtration membrane under a working pressure of 0.1-0.2 Mpa, the filtrate enters a rectification tower, and the semi-finished product going through the rectification tower is diluted by ultra pure water in a dilution device; after the dilution is finished, the dissociative NO2 is expelled by high pure nitrogen in a whitening device, and the obtained finished product is filtered by a nanometer filter membrane and enters a finished product receiver under the working pressure of 0.5-0.8 Mpa; wherein, the aperture of the micro filtration membrane is 0.2 to 0.8 Mu m, and the aperture of the nanometer filter membrane is 0.5 to 1.5 nm. In the prepared ultra high purity nitric acid, the content of single cation is lower than 1 ppb, the content of single anion is lower than 100 ppb, and the content of the dust particle larger than 0.5 Mu m is lower than 5 per milliliter. The production process for extra high purity nitric acid has the advantages of simple technique, low production costs, high purity of products, low content of impurity ions, and applicability for large-scale mass production.
Owner:JIANGYIN RUNMA ELECTRONICS MATERIAL

Method for preparing micron-sized ultra-high-purity aluminum oxide powder by virtue of full-process regulation control

The invention relates to high-purity aluminum oxide powder and in particular relates to a method for preparing micron-sized ultra-high-purity aluminum oxide powder by virtue of full-process regulation control. The method comprises the following steps: melting a high-purity aluminum ingot, repeatedly vacuumizing at a high temperature, filling nitrogen gas for protection, performing ultrasonic pneumatic nebulization, centrifuging, quenching and dispersing of a high-speed pure aluminum turntable and quick cooling of high-purity de-ionized water on molten aluminum by virtue of a ceramic liquid guide pipe to obtain high-activity aluminum slurry, producing an active hydrolysis reaction to generate aluminum hydroxide, repeatedly diluting and filtering through the high-purity de-ionized water to further remove impurities, drying and grinding products, and calcining at 1000-1300 DEG C to obtain the micron-sized (less than 2 microns) aluminum oxide powder with the purity of 99.999%. According to the method, the processes in different stages are optimized, so that the purity of active aluminum powder, the aluminum hydroxide and the final aluminum oxide are well controlled and the cost is reduced; the pollution is avoided, the operation is convenient, and the industrial production is facilitated.
Owner:NANJING CHANGJIANG IND FURNACE TECH GRP CO LTD
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