Patents
Literature
Patsnap Copilot is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Patsnap Copilot

34results about How to "Broaden research direction" patented technology

Method for preparation of high mud resistant polycarboxylic acid dispersant by unsaturated halogenated hydrocarbon copolymerization and grafting with cationic side chain

ActiveCN106188557AThe polymerization process is mild and stableLess side effectsAlcoholPolyethylene glycol
Belonging to the field of dispersants, the invention provides a method for preparation of high mud resistant polycarboxylic acid dispersant by unsaturated halogenated hydrocarbon copolymerization and grafting with a cationic side chain. The method consists of: employing an unsaturated carboxylic acid monomer, an unsaturated halogenated hydrocarbon monomer, an unsaturated cationic quaternary ammonium salt monomer, a polyethylene glycol compound and the like as the raw materials, firstly conducting main chain copolymerization, then polymerizing the cationic side chain, performing functionalization, and finally carrying out etherification grafting so as to synthesize the excellent performance high mud resistant polycarboxylic acid dispersant material with unsaturated halogenated hydrocarbon copolymerized and grafted with cationic side chain, i.e. taking unsaturated carboxylic acid and unsaturated halogenated hydrocarbon as the reactants, conducting free radical polymerization to obtain a carboxylic acid-halogenated hydrocarbon copolymer main chain, using high valence cerium salt-alcohol to initiate polymerization of an unsaturated cationic quaternary ammonium salt monomer so as to obtain a hydroxyl terminated cationic side chain, then modifying the hydroxyl terminated cationic side chain and the polyethylene glycol compound to obtain a functionalized side chain, and carrying out etherification grafting of the functionalized side chain on the carboxylic acid-halogenated hydrocarbon copolymer main chain. The method provided by the invention realizes high water reduction, slump loss resistance, high clay resistance and other multiple effects.
Owner:BEIJING UNIV OF TECH

Lipoic acid-modified ethyl cellulose film and preparation method thereof

ActiveCN111187433AEnhance performance and valueImprove flexibilityEthyl cellulosePolymer chemistry
The invention discloses ipoic a lacid-modified ethyl cellulose film and a preparation method thereof. The preparation method comprises the following steps: step 1, weighing ethyl cellulose, adding theweighed ethyl cellulose into a reaction container, adding an organic solvent, carrying out heating and continuous stirring until the ethyl cellulose is completely dissolved, and performing cooling toroom temperature so as to obtain an ethyl cellulose solution; 2, weighing solid lipoic acid, adding the solid lipoic acid into another reaction container, and adding an organic solvent for dissolvingof the solid lipoic acid to obtain a lipoic acid solution; and 3, weighing a proper amount of the lipoic acid solution, the ethyl cellulose solution and a polymerization inhibitor, carrying out blending and stirring until the formed mixed solution is clear, pouring the mixed solution into a mold, and putting the mold into an oven to form a film. Compared with a pure ethyecellulose film, the filmprovided by the invention has the advantages that the mechanical properties of the film are greatly improved, and the application range of the ethyecellulose film can be widened. Besides, the film prepared by taking ethyl cellulose which is wide in source and renewable as a raw material and taking non-toxic and environment-friendly lipoic acid as a modifier has the advantages of excellent performance, water resistance, degradability and the like.
Owner:INST OF CHEM IND OF FOREST PROD CHINESE ACAD OF FORESTRY

Water-based lubricant and preparation method thereof

The invention discloses a water-based lubricant and a preparation method thereof. The preparation method comprises the following steps: carrying out an epoxy open-loop reaction on rubber seed oil andepoxy chloropropane; carrying out a closed-loop reaction on sodium hydroxide and calcium oxide so as to obtain rubber seed oil-based epoxy; carrying out an open-loop reaction on the rubber seed oil-based epoxy with an alkylol amine compound in an inert organic solvent so as to obtain rubber seed oil-based multi-element alkylol amine; carrying out an esterification reaction on an alcohol or alcoholether with the rubber seed oil-based multi-element alkylol amine and a phosphoryl chloride compound in an inert organic solvent so as to obtain a rubber seed oil-based extreme pressure alcohol or a rubber seed oil-based extreme pressure ether; dissolving the rubber seed oil-based extreme pressure alcohol or the rubber seed oil-based extreme pressure ether into a solution, thereby obtaining a stable green environmental-friendly water-based lubricant under the coactions of hydrogen bonds. The green environmental-friendly water-based lubricant prepared by using the method disclosed by the invention has multiple effects of lubrication, environment protection and extreme pressure wearing resistance.
Owner:INST OF CHEM IND OF FOREST PROD CHINESE ACAD OF FORESTRY

Method for synthesizing cationic polycarboxylate superplasticizer based on Hoffmann rearrangement reaction

ActiveCN106117450AGood application effectExtended Design-Structure-PerformanceSide chainCerium
The invention discloses a method for synthesizing a cationic polycarboxylate superplasticizer based on a Hoffmann rearrangement reaction, and belongs to the field of water reducing agents. Unsaturated amide monomers are modified into unsaturated isocyanate, meanwhile, an oxidation-reduction initiating system is formed by high-valence cerate and alcohol to initiate polymeric unsaturated cation quaternary ammonium salt monomers, a hydroxyl-terminated cation side chain is obtained, then isocyanate reacts with the hydroxyl-terminated cation side chain and polyethylene glycol monomethyl ether to obtain cationic macromonomers and polyether macromonomers, then the cationic macromonomers, the polyether macromonomers and small carboxylic acid monomers are subjected to free radical copolymerization, and the cationic polycarboxylate superplasticizer is obtained. Based on the Hoffmann rearrangement reaction principle, unsaturated amide modified amide reacts with the cation side chain and a polyether side chain, the macromonomers with different structures and different functions are designed and synthesized, and the novel pectinated polycarboxylate superplasticizer with polycarboxylic acid as a main chain and cations and polyether as the side chain is obtained finally. The synthesis process is continuous and easy to control, and multiple effects of excellent water reduction, collapse protection, clay resistance and the like are shown.
Owner:中铁一局集团工业贸易有限公司

A signature authenticity identification system for signature pen

The invention discloses a signature authenticity identification system oriented to a signature pen. It includes information entry module, sample database module, feature model building module, feature extraction module, similarity measurement module and identification and output module. The identification process is that the feature model building module performs spatial modeling on the feature information collected by the information input module, and extracts the feature parameters of the relationship between the writing level pressure and the pen-holding posture with time and the length of the handwriting from the spatial geometric model, and constructs a matrix input system. The average information entropy of each type of feature is used to calculate its weight coefficient, and the comprehensive feature similarity between the information to be tested and the sample information is calculated by combining the method of matrix similarity measurement. In the identification and output module, the comprehensive similarity is compared with the similarity threshold corresponding to different signers, and the authenticity of the signature is verified and the final identification result is output. The signature verification and identity verification method proposed by the invention has objective and stable results.
Owner:HOHAI UNIV CHANGZHOU

Method for Synthesizing Cationic Polycarboxylate Water Reducer Based on Hoffmann Rearrangement Reaction

ActiveCN106117450BGood application effectExtended Design-Structure-PerformanceSide chainCerium
The invention discloses a method for synthesizing a cationic polycarboxylate superplasticizer based on a Hoffmann rearrangement reaction, and belongs to the field of water reducing agents. Unsaturated amide monomers are modified into unsaturated isocyanate, meanwhile, an oxidation-reduction initiating system is formed by high-valence cerate and alcohol to initiate polymeric unsaturated cation quaternary ammonium salt monomers, a hydroxyl-terminated cation side chain is obtained, then isocyanate reacts with the hydroxyl-terminated cation side chain and polyethylene glycol monomethyl ether to obtain cationic macromonomers and polyether macromonomers, then the cationic macromonomers, the polyether macromonomers and small carboxylic acid monomers are subjected to free radical copolymerization, and the cationic polycarboxylate superplasticizer is obtained. Based on the Hoffmann rearrangement reaction principle, unsaturated amide modified amide reacts with the cation side chain and a polyether side chain, the macromonomers with different structures and different functions are designed and synthesized, and the novel pectinated polycarboxylate superplasticizer with polycarboxylic acid as a main chain and cations and polyether as the side chain is obtained finally. The synthesis process is continuous and easy to control, and multiple effects of excellent water reduction, collapse protection, clay resistance and the like are shown.
Owner:中铁一局集团工业贸易有限公司

Method for preparing high mud-resistant polycarboxylic acid dispersant by grafting cationic side chains by copolymerization of unsaturated halogenated hydrocarbons

ActiveCN106188557BThe polymerization process is mild and stableLess side effectsAlcoholPolyethylene glycol
Belonging to the field of dispersants, the invention provides a method for preparation of high mud resistant polycarboxylic acid dispersant by unsaturated halogenated hydrocarbon copolymerization and grafting with a cationic side chain. The method consists of: employing an unsaturated carboxylic acid monomer, an unsaturated halogenated hydrocarbon monomer, an unsaturated cationic quaternary ammonium salt monomer, a polyethylene glycol compound and the like as the raw materials, firstly conducting main chain copolymerization, then polymerizing the cationic side chain, performing functionalization, and finally carrying out etherification grafting so as to synthesize the excellent performance high mud resistant polycarboxylic acid dispersant material with unsaturated halogenated hydrocarbon copolymerized and grafted with cationic side chain, i.e. taking unsaturated carboxylic acid and unsaturated halogenated hydrocarbon as the reactants, conducting free radical polymerization to obtain a carboxylic acid-halogenated hydrocarbon copolymer main chain, using high valence cerium salt-alcohol to initiate polymerization of an unsaturated cationic quaternary ammonium salt monomer so as to obtain a hydroxyl terminated cationic side chain, then modifying the hydroxyl terminated cationic side chain and the polyethylene glycol compound to obtain a functionalized side chain, and carrying out etherification grafting of the functionalized side chain on the carboxylic acid-halogenated hydrocarbon copolymer main chain. The method provided by the invention realizes high water reduction, slump loss resistance, high clay resistance and other multiple effects.
Owner:BEIJING UNIV OF TECH
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products