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45results about How to "Cause poison" patented technology

Detection and analysis method for trans-2-nonenyl aldehyde potentiality in wort

The invention relates to a detection and analysis method for trans-2-nonenyl aldehyde potentiality in wort, which employs headspace solid phase micro-extraction and gas chromatography / mass spectrometry method, the method comprises the following steps: 1) sample pretreatment: placing wort in a headspace bottle for heat treatment; 2) ageing of a SPME extraction head: inserting the extraction head in a gas chromatography sample introduction for aging; 3) headspace solid phase micro-extraction: employing a solid phase extraction column to absorb a detected ingredient in upper space of the wort sample; 4) gas chromatography / mass spectrometry: editing a program, inserting the extraction head to an sample introduction port; vaporizing; introducing the ingredient from the sample introduction port to a capillary column for separating; and 5) detection: introducing the ingredient to be detected in a detector for detecting. A detection and analysis method of the present invention has the advantages of rapidity, less sample amount, accuracy, high sensitivity, no requirement of an extraction solvent and a derivative agent, no environmental pollution is generated, the environmental protection performance is good, and the detection and analysis method has no toxicity on testing staff body, and the security is high.
Owner:广州南沙珠江啤酒有限公司 +1

Method for preparing silk fibroin/hyaluronic acid double-network hydrogel capable of realizing three-dimensional loading of cells

The invention discloses a method for preparing silk fibroin / hyaluronic acid double-network hydrogel capable of realizing three-dimensional loading of cells. The method comprises the following steps that (1) materials are sterilized; (2) a silk fibroin solution and a modified hyaluronic acid solution are mixed to form a prepolymer solution, and a photoinitiator is added to the prepolymer solution;(3) the prepolymer solution obtained in the step (2) is subjected to ultrasonic treatment, and after the ultrasonic treatment, the solution has fluidity and is translucent; (4) the solution obtained after being treated in the step (3) is mixed with the cells to obtain a cell prepolymerization solution, and the cell prepolymerization solution is further added to a cell culture plate; and (5) the culture plate obtained in the step (4) is placed under ultraviolet light and subjected to photo-crosslinking into gel, and then placed in an incubator at 37 DEG C until the prepolymerization solution becomes milky white, and the silk fibroin / hyaluronic acid double-network hydrogel is obtained. The method can realize the three-dimensional culture of the cells in the high-strength and high-tough double-network hydrogel, and is beneficial to the three-dimensional construction of the load-bearing soft tissue such as cartilage in vitro.
Owner:CHONGQING UNIVERSITY OF SCIENCE AND TECHNOLOGY

Method for quickly analyzing total diketone content of beer semi-finished product

ActiveCN103884668ADetection speedGood quantitative detection effectColor/spectral properties measurementsChemistryKetone
The invention discloses a method for quickly analyzing total diketone content of a beer semi-finished product. The method comprises the following steps: 1) preparing certain concentration of peroxide solution; 2) adding certain volume and certain concentration of peroxide solution to a sample before distillation; 3) distilling the sample for about 6 minutes to finish distillation by adopting a direct heating and distilling mode; 4) adding certain volume and certain concentration of hydrochloric acid solution to a 25ml distillate collecting volumetric flask before distillation, wherein the PH when the distillate is metered to the full scale is about 1.2, so that the diketone completely reacts with o-phenylenediamine to generate 2,3-dimethyl quinoxaline; and 5) carrying out colorimetric determination by using a spectrophotometer, and calculating the total diketone content. The quick analysis method disclosed by the invention has the advantages of being quick, simple to operate, convenient, accurate, high in sensitivity and the like, the variable coefficients of the repeatability and the reproducibility are smaller than 5% respectively, the recovery rate achieves over 80%, the analysis time is shortened to 30 minutes from 120 minutes in an electron beam curing (EBC) method, and the detection efficiency is improved by three times in comparison with that of the EBC method.
Owner:东莞市珠江啤酒有限公司

Weeding composition containing pyroxasulfone and flumetsulam

The invention discloses a weeding composition containing pyroxasulfone and flumetsulam, belongs to the technical field of farm chemical preparation, and solves the problems that at present, weeds in a wheat field are various in variety and different in characteristics, a single herbicide is limited in herbicide controlling spectrum and cannot kill various weeds at the same time, existing farm chemicals are poor in adhesive force on plant leaves, and existing farm chemical synergists cannot be degraded. The weeding composition comprises the following raw materials in percentage by mass: 4-50% of pyroxasulfone, 2-60% of flumetsulam, and 1-2% of a synergist, with the balance being auxiliaries and excipients. While the weeding composition is prepared, the synergist is also prepared, the synergist contains a biquaternary ammonium salt structure, diester groups, diacetal, diglucose molecules and alkyl chains, has relatively low micelle concentration, and can be spread and wet on crops when being used as a farm chemical additive and a spraying solution, so that the rain wash of the spraying solution is reduced, the wetting time of the spraying liquid is prolonged, the absorption of plants to the spraying liquid is increased, and the control effect of the farm chemicals is improved.
Owner:安徽喜田生物科技有限公司

Acid mist inhibitor performance test method

The invention discloses an acid fog inhibitor performance test method. Neutral gas which does not react with acid fog is used for bringing out acid fog produced in an electrodeposition process, and isfed into water; after the water absorbs the acid fog, the pH value is reduced; the amount of the acid fog produced in the electrodeposition process is calculated by measuring a variation of the pH value of the water before and after the electrodeposition; the acid fog inhibition rate is calculated by comparing the amounts of the acid fog produced before and after the adding of an acid fog inhibitor into electrodeposition liquid. An acid fog test device comprises a gas source, an electrodeposition tank, an acid fog absorption unit and a vacuum pump which are connected in sequence through gas pipes; the acid fog absorption unit comprises multiple serially connected closed water accommodating containers; the water accommodating containers are also connected through gas pipes; gas flowmetersare arranged on the gas pipe between the gas source and the electrodeposition tank and the gas pipe between the acid fog absorption unit and the vacuum pump. The used device is small in size and simple in structure, can be placed in a fuming cupboard of a laboratory, and is harmless; the quantity of required samples is very small, and steps are simple; the data reproducibility is high, and a result is accurate and reliable.
Owner:CHONGQING KOOPPER CHEM IND

A landscape garden ecological maintenance device

The invention discloses a landscape garden ecological maintenance device. The landscape garden ecological maintenance device comprises a supporting frame mechanism, a power switching mechanism, a ropling mechanism and a feeding mechanism, wherein the power switching mechanism, the ropling mechanism and the feeding mechanism are arranged in the supporting frame mechanism; the power switching mechanism is located at the bottom position of the feeding mechanism, and the ropling mechanism is located at the position between the feeding mechanism and the power switching mechanism; the supporting frame mechanism comprises a fixing base, a first supporting column and a second supporting column, wherein the fixing base is used for being installed on a ship deck, and the first supporting column andthe second supporting column are fixedly arranged at the top of the fixing base; the power switching mechanism comprises an upper plate body, a lower plate body, an inclined guiding sliding rod and anadjusting sliding block, wherein the inclined guiding sliding rod is fixedly arranged between the upper plate body and the lower plate body, and the adjusting sliding block is arranged on the inclined guiding sliding rod in a sliding-fit connection mode; and a first motor is fixedly arranged at the right side end of the adjusting sliding block, and a power driving disk is connected to the right side end of the first motor in a power-fit mode. According to the landscape garden ecological maintenance device, the structure is simple, the operation is convenient, the labor amount of workers is reduced, and the throwing efficiency and the spreading efficiency are improved.
Owner:昆山天坤园林景观工程有限公司

Wide-temperature vanadium-free denitration catalyst as well as preparation method and application thereof

The invention discloses a wide-temperature vanadium-free denitration catalyst preparation method, which comprises: 1, dissolving a chromium-containing precursor, an iron-containing precursor and a copper-containing precursor in deionized water, and stirring in a water bath at a temperature of 20-30 DEG C for 30-60 min to obtain a mixed solution; step 2, adding a pretreated HY molecular sieve into the mixed solution obtained in the step 1, and heating in a water bath to 70-80 DEG C under a stirring condition to obtain a viscous mixture; and step 3, sequentially carrying out ultrasonic oscillation, room-temperature aging, drying, roasting and cooling treatment on the obtained viscous mixture to obtain the catalyst, the mass ratio of the HY molecular sieve to the Fe precursor is (1.33-2.67): 1. The prepared wide-temperature vanadium-free denitration catalyst is wide in active temperature range, low in activation temperature and high in denitration efficiency, the composite desulfurization catalyst can be arranged in equipment behind a dust remover and a desulfurization tower, the service mechanical life of the catalyst is prolonged, and the denitration efficiency can reach 95% or above within the range of 200-360 DEG C under the sulfur-free working condition.
Owner:XIAN RES INST OF CHINA COAL TECH& ENG GROUP CORP

Detection and analysis method for trans-2-nonenyl aldehyde potentiality in wort

The invention relates to a detection and analysis method for trans-2-nonenyl aldehyde potentiality in wort, which employs headspace solid phase micro-extraction and gas chromatography / mass spectrometry method, the method comprises the following steps: 1) sample pretreatment: placing wort in a headspace bottle for heat treatment; 2) ageing of a SPME extraction head: inserting the extraction head in a gas chromatography sample introduction for aging; 3) headspace solid phase micro-extraction: employing a solid phase extraction column to absorb a detected ingredient in upper space of the wort sample; 4) gas chromatography / mass spectrometry: editing a program, inserting the extraction head to an sample introduction port; vaporizing; introducing the ingredient from the sample introduction port to a capillary column for separating; and 5) detection: introducing the ingredient to be detected in a detector for detecting. A detection and analysis method of the present invention has the advantages of rapidity, less sample amount, accuracy, high sensitivity, no requirement of an extraction solvent and a derivative agent, no environmental pollution is generated, the environmental protection performance is good, and the detection and analysis method has no toxicity on testing staff body, and the security is high.
Owner:广州南沙珠江啤酒有限公司 +1

Method for detecting and analyzing content of polyphenol in beer semi-finished product and bear finished product

The invention discloses a method for detecting and analyzing the content of polyphenol in a bear semi-finished product and a bear finished product. The method comprises the following steps of: (1) preparing a tea polyphenol stock solution preparation: soaking tea leaves by using heated distilled water, filtering, taking a clear solution, adding the clear solution into a beer, and mixing for later use; (2) detecting the polyphenol value of a tea polyphenol stock solution sample; (3) analyzing by using a chemical automatic analyzer: editing a program, uniformly mixing reagents, putting the sample into a reaction tank from a sample inlet, and reacting and analyzing by using a detector; (4) making a standard curve: diluting the tea polyphenol stock solution sample according to a certain concentration, and making a standard curve for a detection polyphenol module of the chemical automatic analyzer; (5) pre-treating a sample: degassing, filtering or centrifuging a sample to be detected; and (6) performing detection: detecting the sample to be detected in the detector. By adopting the detection and analysis method disclosed by the invention, an unstable polyphenol detection result caused by the fact that a standard substance is not provided for making a polyphenol standard curve for the chemical automatic analyzer can be avoided, and the method has the advantages of fastness, large sample amount, accuracy, high sensitivity and the like.
Owner:广州南沙珠江啤酒有限公司 +1
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