The invention discloses a preparation method for a nonmetallic element-doped MxFe3-xO4@TiO2
magnetic composite material. A double-cavity
polytetrafluoroethylene-lining stainless steel reaction kettle is used for synthesizing the target
composite material under high temperature and
high pressure. The method comprises the following steps: taking water-soluble metallic M<2+> salt, Fe<3+> salt,
titanium salt and inorganic nonmetallic salt as raw materials, and stirring and dissolving M<2+> salt, Fe<3+> salt and a surfactant into an
ethanol solution, and synthesizing magnetic MxFe3-xO4 nano-particles under an alkaline condition by virtue of a solvothermal method; ultrasonically dispersing and uniformly mixing the MxFe3-xO4 nano-particles, nonmetallic salt and
titanium salt in the
ethanol solution, performing reaction for 8 to 15 hours by adopting a high-temperature high-pressure vapor-thermal method, and performing separation, washing,
drying and
grinding to obtain the target product. The
composite material is doped with nonmetallic elements, so that the photoeffect
wavelength response range of TiO2 can be widened; by MxFe3-xO4, the forbidden bandwidth of TiO2 can be effectively reduced; in addition, by the magnetic property, the catalytic material can be efficiently recycled; the whole preparation method is simple in flow, and has the advantages of safety, high efficiency, low cost, environment friendliness and the like.