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30results about How to "Low cost recycling" patented technology

Method for recycling ilmenite from vanadium titano-magnetite iron dressing tailings

The invention discloses a method for recycling ilmenite from vanadium titano-magnetite iron dressing tailings. The method comprises the steps that the specific susceptibility of main gangue in the iron dressing tailings, the specific susceptibility of the ilmenite in the iron dressing tailings and the content of TiO2 in the iron dressing tailings are determined; when the iron dressing tailings meet the condition 1, the iron dressing tailings are subjected to first-section strong magnetic separation, first-section strong magnetism concentrates are subjected to one-time or multi-time reselection, and gravity concentrates are obtained; the gravity concentrates are subjected to first-time flotation and one-time or multi-time electric separation, and ilmenite concentrates are obtained, wherein the condition 1 can be shown in the formula: X1>(X2*60%), the total amount of the iron dressing tailings serves as a standard, the content of the TiO2 in the iron dressing tailings is lower than 5 wt%, X1 is the specific susceptibility value of the main gangue in the iron dressing tailings, and X2 is the specific susceptibility value of the ilmenite in the iron dressing tailings; and otherwise, the iron dressing tailings are subjected to a strict granularity classification method. By mean of the method, the production cost of the ilmenite is reduced, and the grade of the TiO2 of selected raw ore obtained after electric separation and flotation is improved.
Owner:PANGANG GRP MINING

Method for absorbing and recovering high-concentration oil vapor

The invention discloses a method for absorbing and recovering high-concentration oil vapor, which belongs to the technical field of oil vapor recovery, and comprises the following steps that: the high-concentration oil vapor flows through an absorption column filled with a mesopore absorbent and micropore absorbent double-layer fixed bed under normal temperature and normal pressure, the mesopore absorbent is arranged at the lower part of the absorption column, and the micropore absorbent is arranged at the upper part of the absorption column; and the absorbent absorbing organic substances is vacuumized and desorbed, and the desorbed oil vapor is condensed or absorbed and then returns to an oil tank. The concentration of the oil vapor at an outlet of the absorption column processed by the invention can be reduced to 25g/cm3, which can achieve the national control standard of oil vapor pollutant emission; and the oil product returning to the oil tank continues to be used, and the oil vapor recovery rate reaches more than 93 percent. According to the characteristics of the high-concentration oil vapor, the invention develops a double-layer fixed bed absorption process combined by the mesopore high molecular polymer absorbent and the micropore absorbent, and the high absorption capacity of the mesopore absorbent and the high absorption efficiency of the micropore absorbent are coupled, thereby achieving the efficient utilization of the high-concentration oil vapor.
Owner:NANJING UNIV

Treatment process of nickel-containing alloy powder in hydrochloric acid system

The invention provides a treatment process of nickel-containing alloy powder in a hydrochloric acid system. The treatment process comprises the following steps that (1) presoaking of the nickel-containing alloy powder is carried out, specifically, the nickel-containing alloy powder, concentrated hydrochloric acid and water are mixed, and then heated, stirred and presoaked; (2) high-pressure oxygen introduction and leaching is carried out, specifically, prepreg is poured into a high-pressure kettle, heating is carried out, oxygen is introduced to react for a certain time, cooling and liquid-solid separation are carried out, leaching residues are produced and stacked, and leaching liquid enters a next process; (3) neutralization and impurity removal are carried out, specifically, the pH value of the leaching liquid is adjusted by using nickel carbonate, a neutralization solution and neutralization slag are produced, and the neutralization slag returns to the leaching process; (4) cobalt extraction with resin is carried out, specifically, cobalt ions in the neutralization solution is adsorbed with the resin to produce cobalt carbonate precipitate and cobalt-extracted liquid; and (5) product preparation is carried out, specifically, nickel carbonate is prepared from a small part of cobalt-extracted liquid for a neutralization and impurity removal process, the rest liquid is concentrated and pyrolyzed, hydrochloric acid is produced for recycling, and nickel oxide is taken as a final product. According to the treatment process, the nickel oxide product is produced through the leaching, purifying and pyrolyzing processes, meanwhile, hydrochloric acid and a neutralizing and impurity-removing reagent are recycled, and the treatment process is clean and environmentally friendly.
Owner:金川镍钴研究设计院有限责任公司 +1

A waste sulfuric acid recycling device and process

The invention relates to a recovery and treatment method of waste sulfuric acid, comprising S1: performing defluorination pretreatment on waste sulfuric acid; S2: transferring waste sulfuric acid to a reaction kettle, adding magnesium oxide for reaction; S3: performing pressure filtration on the reaction solution, and transferring the waste residue to Waste residue storage tank, the filtrate is transferred to activated carbon filtration equipment; S4: The mother liquor of magnesium sulfate is separated from the first crystallization tank to detect the content of potassium bisulfate. According to whether the content of potassium bisulfate in the mother liquor reaches the predetermined threshold, it is decided whether the mother liquor should continue to circulate or recover sulfuric acid Potassium hydrogen is recycled. The method and device of the present invention can realize the recovery of potassium hydrogensulfate in waste sulfuric acid, and through the circular purification of the mother liquor, when the concentration of potassium hydrogensulfate in the mother liquor does not reach the threshold value, the mother liquor is returned to the reactor to continue to increase the potassium hydrogensulfate of the mother liquor Concentration, when the concentration of potassium bisulfate in the mother liquor reaches the threshold, the mother liquor is transferred to the crystallization tank, magnesium oxide is added to generate potassium magnesium sulfate and the material is separated and discharged, realizing the low-cost recovery of potassium bisulfate in waste sulfuric acid.
Owner:山东齐创石化工程有限公司

Device and process for recycling waste sulfuric acid

The invention relates to a method for recycling waste sulfuric acid. The method comprises the following steps: S1, carrying out defluorination pretreatment on waste sulfuric acid; S2, transferring thewaste sulfuric acid into a reaction kettle, and adding magnesium oxide for reaction; S3, carrying out filter pressing on a reaction liquid, transferring waste residues to a waste residue storage tank, and transferring filtrate to activated carbon filtering equipment; and S4, separating a magnesium sulfate mother liquor through a first crystallization kettle, detecting the content of potassium hydrogen sulfate, and determining whether the mother liquor is continuously circulated or recycled after potassium hydrogen sulfate is recycled according to whether the content of potassium hydrogen sulfate in the mother liquor reaches a preset threshold value or not. According to the method and the device, the recovery of potassium hydrogen sulfate in the waste sulfuric acid can be realized; the mother liquor is circularly purified, when the concentration of potassium hydrogen sulfate in the mother liquor does not reach a threshold value, the mother liquor flows back to the reaction kettle to continue to increase the concentration of potassium hydrogen sulfate in the mother liquor, and when the concentration of potassium hydrogen sulfate in the mother liquor reaches the threshold value, themother liquor is transferred to the crystallization kettle, the magnesium oxide is added, potassium magnesium sulfate is generated, separated and discharged, and the low-cost recovery of potassium hydrogen sulfate in the waste sulfuric acid is achieved.
Owner:山东齐创石化工程有限公司

Solid waste pelletizing process and efficient sintering method thereof

PendingCN114763581AHigh thermal strengthAvoid sinter productivity impactProcess efficiency improvementFine powderCorn starch
The invention discloses a solid waste pelletizing process and an efficient sintering method thereof, waste magnesium oxide powder, iron-containing solid waste and a binder are adopted as raw materials, and solid waste pellets are prepared after burdening, surface modification and pelletizing; and mixing the solid waste pellets and a mineral mixture prepared by adopting a mixing granulation process as sintering raw materials, and sequentially carrying out material distribution, ignition, sintering, cooling and whole grain screening to obtain a finished product of sintered ore, the binder is prepared from waste magnesium oxide sludge, municipal sludge, first quick lime and corn starch; the waste magnesium oxide powder and the waste magnesium oxide sludge are magnesium oxide wastes. According to the method, the magnesium oxide waste, the municipal sludge, the rotary hearth furnace fine powder and other solid wastes inside and outside the steel plant are fully recycled, local concentrated heterogeneous sintering of magnesium oxide is realized, the adverse effect of uniform distribution of MgO on the sintering productivity is avoided, the quality of solid waste pellets is improved, and the production cost is reduced. Therefore, the quality index and the heat energy utilization efficiency of the finished sinter are remarkably improved, and fuel consumption and CO2 emission are reduced.
Owner:BAOSHAN IRON & STEEL CO LTD

A method for recovering ilmenite from vanadium-titanium-magnetite iron beneficiation tailings

The invention discloses a method for recycling ilmenite from vanadium titano-magnetite iron dressing tailings. The method comprises the steps that the specific susceptibility of main gangue in the iron dressing tailings, the specific susceptibility of the ilmenite in the iron dressing tailings and the content of TiO2 in the iron dressing tailings are determined; when the iron dressing tailings meet the condition 1, the iron dressing tailings are subjected to first-section strong magnetic separation, first-section strong magnetism concentrates are subjected to one-time or multi-time reselection, and gravity concentrates are obtained; the gravity concentrates are subjected to first-time flotation and one-time or multi-time electric separation, and ilmenite concentrates are obtained, wherein the condition 1 can be shown in the formula: X1>(X2*60%), the total amount of the iron dressing tailings serves as a standard, the content of the TiO2 in the iron dressing tailings is lower than 5 wt%, X1 is the specific susceptibility value of the main gangue in the iron dressing tailings, and X2 is the specific susceptibility value of the ilmenite in the iron dressing tailings; and otherwise, the iron dressing tailings are subjected to a strict granularity classification method. By mean of the method, the production cost of the ilmenite is reduced, and the grade of the TiO2 of selected raw ore obtained after electric separation and flotation is improved.
Owner:PANGANG GRP MINING

A method for separating potassium chloride in flotation froth and a dissolution kettle

The invention discloses a method for separating potassium chloride in flotation froth and a stirring vessel. The method comprises the steps that the flotation froth is input into the stirring vessel which can enable the flotation froth to flow vertically and mixed with water and old brine, solid potassium chloride in the flotation froth is dissolved, sodium chloride solid particles are sedimented, a mother solution with potassium chloride is dried in air to be separated out, and the main component is secondary carnallite containing potassium chloride. The stirring vessel applying the method comprises a vessel body, a stirrer, a center barrel and a flow guiding barrel, wherein the stirrer, the center barrel and the flow guiding barrel are sequentially arranged from interior to exterior in a sleeved mode. A mother solution outlet is formed in the upper portion of the vessel body, a sedimentation outlet is formed in the lower portion of the vessel body, the first end of at least two feeding pipes arranged in the stirring vessel is arranged inside the center barrel. The stirring vessel is combined with the method, so that potassium chloride in reverse flotation froth can be efficiently extracted; compared with a traditional method for recycling potassium chloride in reverse flotation froth, the efficiency is higher, the process is shorter, the cost is lower, the fresh water consumption is smaller.
Owner:QINGHAI SALT LAKE IND
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