The utility model discloses a kind of low pressure preparation chromatogram
sample purification and automatic feeding device, it is related to the field of pharmaceutical synthesis experiment, and it includes: the upper end of extraction column
pipe is set open, lower end is connected and is provided with lower interface, and extraction column
pipe is filled with adsorption extraction filler layer above lower interface in;Adsorption extraction filler layer is flexible mechanical
compressible material with communicating type porous;
Vacuum evaporation heater is sleeved in the outside of extraction column
pipe, for the target reaction mixture is removed by vacuum heating
evaporation;Liquid channel is connected and is provided with in sample rod along the axial direction, and the outer periphery of one end of sample rod is circumferentially sleeved with sealing
assembly;The one end of sample rod setting sealing
assembly is pushed into extraction column pipe from upper end opening, for compressing adsorption extraction filler layer;The inner wall of extraction column pipe is tightly attached to the outer wall of sealing
assembly, for sealing extraction column pipe. The scheme not only does not need to operate the
silica gel micro
powder of health
threat, also greatly speeds up the purification speed of
chemical reaction mixture.