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40results about How to "Reduce entrapment" patented technology

Method for preparing silane coupling agent modified attapulgite surface molecular imprinting material aiming at bisphenol A

The invention discloses a method for preparing a silane coupling agent modified attapulgite surface molecular imprinting material aiming at bisphenol A. The method comprises the following preparation steps: preparing a molecular imprinting material carrier; adding silane coupling agent modified attapulgite into an HCl solution to be acidified, performing backflow reaction under the condition of heating and nitrogen-filled seal, and drying in vacuum; adding the attapulgite obtained in the second step into anhydrous methylbenzene, adding acryloyl chloride and triethylamine under the condition of nitrogen-filled seal, stirring to react under the condition of room temperature, performing suction filtration, subsequently washing, and drying in vacuum; and putting the attapulgite obtained in the third step into an acetonitrile solvent, further adding template molecules, functional monomers, cross-linking agents and initiators to perform polymerization reaction so as to form the expected attapulgite surface molecular imprinting material. The prepared attapulgite surface bisphenol A molecular imprinting material has the advantages of large adsorption capacity, high targeted adsorbability, high repeated utilization rate, long service life and the like.
Owner:SOUTHEAST UNIV

Preparation method of surface molecularly imprinted polymers in water phase application

The invention discloses a preparation method of surface molecularly imprinted polymers in water phase application. The preparation method comprises the following steps: polymerizing solutions containing MOGs, glycidyl methacrylate, ethylene glycol dimethacrylate and an initiator, and subsequently conducting washing and drying to obtain a macroporous carrier; reacting the macroporous carrier with a photoinitiator, and conducting washing and drying to obtain the macroporous carrier with the photoinitiator on the surface; pre-assembling template molecules and functional monomers, then mixing the pre-assembled template molecules and functional monomers with a crosslinker and the treated macroporous carrier, conducting photopolymerization and washing, removing the template molecules, and conducting drying to obtain the surface molecularly imprinted polymer material, wherein the molar ratio of the functional monomers to the crosslinker is 1:(20-30). According to the preparation method, the macroporous material prepared by using the MOGs as a pore-foaming agent is used as the carrier and synergistically matched with the crosslinker with a high addition proportion, thereby preparing the surface molecularly imprinted polymers SMIPs with good template molecule identifying selectivity, large adsorption capacity and high adsorption and desorption speed.
Owner:CENT SOUTH UNIV

Environmentally-friendly biological microbial inoculum for repairing soil pollution and preparation method of environmentally-friendly biological microbial inoculum for repairing soil pollution

The invention discloses an environmentally-friendly biological microbial inoculum for repairing soil pollution and a preparation method of the environmentally-friendly biological microbial inoculum for repairing soil pollution, and belongs to the technical field of soil repairing. The preparation method comprises the steps of modifying glucan, coating 1-ethyl-3-(3-dimethyl aminopropyl)carbodiimidehydrochloride and N-hydroxy succinimide with the modified glucan and polylactic acid so as to obtain modified microspheres; then mixing chitosan with agarose, and adding the modified microspheres soas to obtain semi-finished products; and finally, mixing the semi-finished products with a bacterial culture solution, adding trichoderma and acetobacter xylinum, performing mixed culture, and performing filtration so as to obtain the environmentally-friendly biological microbial inoculum for repairing soil pollution. After the prepared environmentally-friendly biological microbial inoculum for repairing soil pollution is used, the content of viable counts in soil can be effectively increased, and the content of effective state heavy metal ions in the soil is reduced.
Owner:NANJING INST OF ENVIRONMENTAL SCI MINIST OF ECOLOGY & ENVIRONMENT OF THE PEOPLES REPUBLIC OF CHINA

Flavored function konjac sauce rich in decanoyl acetaldehyde and preparation method of flavored function konjac sauce

The invention provides a flavored function konjac sauce rich in decanoyl acetaldehyde and a preparation method of the flavored function konjac sauce. The preparation method comprises the following steps of (1) preparing root and leaf juice from fresh heartleaf houttuynia roots and heartleaf houttuynia leaves, adding deacetylate konjac glucomannan to obtain heartleaf houttuynia herb konjac gum liquid, and performing refrigeration for standby application; (2) selecting entire soybeans, performing hulling, performing washing, performing soaking, performing draining, adding the heartleaf houttuynia herb konjac gum liquid in a certain weight ratio, and performing refining to obtain viscous heartleaf houttuynia herb konjac soybean milk; (3) making the viscous heartleaf houttuynia herb konjac soybean milk into heartleaf houttuynia herb konjac bean curd blanks, performing dicing, performing vacuum dehydrating, and controlling the water content; and (4) performing inoculating with aspergillus oryzae for culturing, performing aerobic fermentation to obtain konjac bean curd yeast blanks, putting the konjac bean curd yeast blanks in a preserving machine to making preserved blanks, performing inoculating with lactic acid bacteria and microzymes, and performing anaerobic fermentation, so as to obtain the konjac sauce. The flavored function konjac sauce has unique fishy fragrance and rich flavor, can diminish inflammation, resist bacteria, promote urination and reinforce immunity of human bodies. The content of the decanoyl acetaldehyde in the konjac sauce is greater than 0.1g/Kg, the content of methyl-nonyl-ketone is greater than 0.21g/Kg, and the content of total flavonoids is greater than 6.0g/Kg.
Owner:湖北顺溪生物食品股份有限公司

Oleanolic acid enriched flavored functional fermented bean curd and preparation method thereof

The present invention provides an oleanolic acid enriched flavored functional fermented bean curd and a preparation method thereof. The preparation method comprises the following steps: (1) rhizomes of akebia quinata of three years or more are used to prepare into akebia quinata rhizome juice; the akebia quinata rhizome juice is refrigerated for a standby application; and akebia quinata fruit fleshes are stirred and beaten into fruit slurry; (2) whole soybeans are selected; the selected soybeans are shelled; the shelled soybeans are soaked; the soaked soybeans are drained; the akebia quinata rhizome juice at a certain weight ratio is added; filtering and slurry boiling are conducted; and during curdling, the fruit slurry at a certain weight ratio is added to prepare fermented bean curd bases; (3) mixed micro-organisms containing mucor and monascus are taken to be inoculated into the fermented bean curd bases; the fermented bean curd bases are subjected to aseptic culture; the culturedfermented bean curd bases are put into a pickling device; salt bases are prepared; and inoculum containing yeasts is poured into the pickling device for fermentation; and (4) a flavoring agent is added into the fermented bean curd after the fermentation; and high-temperature sterilizing and sub-packaging are conducted to obtain a finished product. The flavored functional fermented bean curd is sticky, refreshing and moist in mouthfeel, unique in ester fragrance, rich in flavor and improved in health-care functions, and has an oleanolic acid content of more than 0.15g/100g, an organic acid content of more than 1.0g/100g and a Vc content of more than 30mg/100g.
Owner:湖北顺溪生物食品股份有限公司

Metallurgical machinery equipment capable of automatically screening ore

The invention discloses a metallurgical mechanical equipment capable of automatically sieving ore. The metallurgical mechanical equipment structurally includes bulk material conveying equipment, a feed inlet, a supporting frame, a repair cover and a power device. The bulk material conveying equipment is composed of a machine body, a sieved material conveying device, a power rotating disc, a driving gear transmission shaft, a conveying screen, an inclined material guide plate and a driven gear transmission shaft. The bulk material conveying equipment uses a vibration mechanism to vibrate the bottom end of the conveying screen so that soil on the surface of a material on the conveying screen can be sieved to fall on the sieved material conveying device and sent out through the sieved material conveying device, a material enclosing frame is used to prevent the soil from falling to the bottom of a machine, the conveying screen levels the material accumulated on the conveying screen by a material sweeping mechanism, a material sweeping plate uses a shovel strip to reduce the material clamping and pressing conditions on the conveying screen at the time of material leveling, and the damage to the conveying screen is avoided. The material can automatically screened when the material is conveyed.
Owner:武钢资源集团鄂州球团有限公司

A kind of preparation method of surface molecularly imprinted polymer applied in aqueous phase

The invention discloses a preparation method of surface molecularly imprinted polymers in water phase application. The preparation method comprises the following steps: polymerizing solutions containing MOGs, glycidyl methacrylate, ethylene glycol dimethacrylate and an initiator, and subsequently conducting washing and drying to obtain a macroporous carrier; reacting the macroporous carrier with a photoinitiator, and conducting washing and drying to obtain the macroporous carrier with the photoinitiator on the surface; pre-assembling template molecules and functional monomers, then mixing the pre-assembled template molecules and functional monomers with a crosslinker and the treated macroporous carrier, conducting photopolymerization and washing, removing the template molecules, and conducting drying to obtain the surface molecularly imprinted polymer material, wherein the molar ratio of the functional monomers to the crosslinker is 1:(20-30). According to the preparation method, the macroporous material prepared by using the MOGs as a pore-foaming agent is used as the carrier and synergistically matched with the crosslinker with a high addition proportion, thereby preparing the surface molecularly imprinted polymers SMIPs with good template molecule identifying selectivity, large adsorption capacity and high adsorption and desorption speed.
Owner:CENT SOUTH UNIV

A kind of preparation method and application of PD ion imprinted silica gel adsorbent

The invention discloses a preparation method and application of a Pd ionic imprinting silica gel adsorbent. The preparation method comprises the following steps: firstly, dispersing Pd (II) salts and silica gel activated by acid in an alcohol solvent; secondly, enabling chlorosilane to react with KI, then adding 2-aminothiazole, and reacting under the action of alkali; thirdly, carrying out mixed reaction on a product obtained in the first step and a product obtained in the second step; fourthly, filtering and washing the product in the third step, extracting the washed product, washing to neutral and drying, thus obtaining a finished product. Meanwhile, the invention discloses the application of the adsorbent in adsorption of Pd ions. According to the preparation method and the application disclosed by the invention, a Pd ionic imprinting polymer is prepared by using an ionic imprinting technology, using the silica gel as a substrate, using 3-chloropropyltriethoxysilane as a cross-linking agent and using 2-aminothiazole as a functional monomer through a polymerization reaction; the Pd ionic imprinting polymer is applied to the research on adsorption of Pd and has the advantages of high mechanical stability, good adsorption selectivity, uniform distribution of particle size, and the like; identification and elution of template ions are facilitated, and an embedding phenomenon can be reduced.
Owner:SOUTH CHINA NORMAL UNIVERSITY
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