34results about How to "Adjustable specific surface area" patented technology

The invention relates to a preparation method of continuous SiO2 aerogel fibers. The method comprises the following steps: processing silicate or silanol sol to prepare a spinning stock solution; adding an acidic solution to a coagulation tank to form a coagulation bath; and injecting the spinning stock solution to the coagulation bath, carrying out reaction wet spinning to obtain orthosilicic acid / silicate fibers, reeling the orthosilicic acid / silicate fibers, immersing the reeled fibers in an ageing solution, ageing the immersed fibers at normal temperature for 2-10d, washing the aged fibers with deionized water until the aged fibers are neutral, carrying out solvent displacement, and drying the obtained fibers to obtain the continuous SiO2 aerogel fibers. The method has the characteristics of cheap and easily available raw materials, simple reaction process and good spinnability, and solves the problem of difficult production of fibers through spinning SiO2 aerogel. The inorganic SiO2 aerogel fibers prepared in the invention have the characteristics of abundant holes, high specific surface area, high temperature resistance, chemical corrosion resistance and adjustable specific surface area, and can be applied in the fields of catalyst carriers and adsorbing filtration.

The invention discloses a method for preparing an open-tube electrophoretic column coated with nanometer titanium dioxide, as well as application thereof. In an etched capillary column, an open-tube capillary electrophoretic column coated with the nanometer titanium dioxide is prepared by a water (solvent) thermal method. The preparation method is characterized in simplicity, coatings insusceptible to fall off, and the like, and is suitable for the selective enrichment and separation of functionalized phosphorylated polypeptide and protein in complex biological samples. Titanium dioxide molecules are combined with silicon hydroxyl on the surface of the inner wall of a capillary through chemical bonds, and nanometer titanium dioxide particles are uniform in grain, complete in coatings and capable of effectively reducing the nonspecific adsorption effect to the protein and other macromolecule samples. The surface properties and micropore structures of the coatings can be conveniently controlled by changing the categories and proportion of middle pore-forming agents in hydrothermal mixtures, so as to obtain a phosphorylated polypeptide capillary column with adjustable pore diameter and specific surface area.

The invention provides a continuous cellulose aerogel fiber and a preparation method thereof. The preparation method comprises the following steps: dispersing cellulose into a dispersing agent so as to obtain a spinning stock solution; extruding the spinning stock solution into a coagulating bath for wet-method spinning so as to obtain cellulose aerogel fiber; winding the cellulose aerogel fiber in the coagulating bath, and soaking into an aging liquid for aging; washing the aged cellulose aerogel fiber till the pH is neutral, and drying, so as to obtain the continuous cellulose aerogel fiber. The preparation method provided by the invention has the characteristics that raw materials are cheap and easy to obtain, the preparation process is simple, green and pollution-free, the continuous cellulose aerogel fiber is good is spinnability, and the problem that cellulose aerogel is hard to spin into fiber is solved. The diameter of the cellulose aerogel fiber provided by the invention is smaller than 120 [mu]m, the cellulose aerogel fiber has the characteristics of high specific surface area (greater than or equal to 88m<2> / g), high porosity (greater than or equal to 85%), and low density (less than or equal to 0.2 / cm<3>), meanwhile the fiber specific surface area can be adjusted, and the cellulose aerogel fiber can be used in fields such as functional clothes, sensing, catalyst loading and adsorption filtration, cosmetics and biological treatment.