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807results about How to "Facilitate continuous production" patented technology

Method for preparing polyimide fiber

The invention relates to a preparation method of polyimide fiber. The procedures and conditions of the preparation method are as follows: (1) precursor acid polyamine solution used for spinning is made by fasculating diamine and dianhydride monomer; (2) the preparation of the polyimide fiber adopts dry-wet spinning process; (3) the polyimide fiber is imidized; and (4) the polyimide fiber undergoes the heat drawing under the temperature of 300 to 500 DEG C, and the drawing multiple of the fiber is 1 to 7 times. Imide process adopts a gradient heating-up thermal treatment furnace so as to overcome the defects of the inaccurate temperature control and the non-feasibility of the prior double thermal furnace process. The preparation method has simple process and is easy for continuous production. The prepared polyimide fiber has stronger strength and high modulus and can be used under the temperature of over 300 DEG C. In addition, the polyimide fiber has UV irradiating resistance property, a higher limited oxygen index and corrosion resistance, so the polyimide fiber can be widely applicable for the reinforced fiber of composite materials, a cable sheath, a cable reinforcing core, the mooring rope of vehicle and vessel and the filtering materials of high temperature or radioactive substance, etc.
Owner:CHANGCHUN INST OF APPLIED CHEMISTRY - CHINESE ACAD OF SCI

Fluororesin mixture, copper-clad plate prepared therefrom and manufacturing method thereof

The invention relates to a fluororesin mixture, a copper-clad plate prepared therefrom and a manufacturing method thereof. The fluororesin mixture contains the following two substances as necessary components in 100 parts by weight of an organic solid substance: 90-99 parts of polytetrafluoroethylene (PTFE) emulsions and 1-10 parts of polytetrafluoroethylene perfluoroalkyl vinyl ether (PFA) emulsions. The copper-clad plate prepared from the fluororesin mixture comprises a plurality of superimposed varnished cloths and copper foil coating one or two surfaces of the varnished cloths, and each varnished cloth comprises a glass fiber cloth and the fluororesin mixture attached to the dipped and dried glass fiber cloth. The fluororesin mixture is prepared by using the PTFE emulsions as main resins and can dip the glass fiber cloths many times under the condition that the PTFE sintering temperature is330 DEG C to prepare the vanished cloths, and the vanished cloths prepared from the fluororesin mixture has the advantages of good gum dipping quality, level surface, flexibility and easy operation; and besides, the copper-clad plate made from the fluororesin mixture has excellent dielectric performance which meets the dielectric performance requirement of the high-frequency communication field for a base plate material, and has simple making method and process and is beneficial to industrial continuous production.
Owner:GUANGDONG SHENGYI SCI TECH

Automatic assembling machine of hinge spring shafts

The invention belongs to an assembling machine for manufacturing spectacle frames, in particular to an automatic assembling machine of hinge spring shafts, which can continuously and automatically complete the integral assembly of spectacle hinge spring shafts. The traditional assembly of the spectacle hinge spring shafts completely depends on manual operation of workers and has the defects of low assembly speed, long period and low production efficiency due to one-by-one serial connection, and the assembled spectacle hinge spring shafts have great difference and unstable quality due to the limitations of the technical level of the workers, which greatly influences the later actual use of the spectacle frames. Aiming at the defects, the invention provides an automatic assembling machine of hinge spring shafts, which has the technical characteristic that one large rotary table and one small rotary table which are mutually perpendicular are arranged, the rotary tables are provided with a plurality of corresponding through holes and card slots for installing corresponding parts, and the two rotary tables rotate and are mutually matched according to a set beat so as to continuously and automatically assemble the hinge spring shafts. Compared with the traditional manual operation, the invention has high speed and high efficiency, and the finished hinge spring shafts assembled by the machine have uniform specifications, small difference and stable quality.
Owner:浙江康华眼镜有限公司 +1

Preparation method of thermotropic liquid crystal polyarylester fiber

The invention discloses a preparation method of a thermotropic liquid crystal polyarylester fiber, relates to a preparation method of thermotropic liquid crystal polyarylester, and aims to solve the problems that the existing method for preparing the thermotropic liquid crystal polyarylester is complex and the polyarylester fiber is low in tensile strength. The preparation method of the thermotropic liquid crystal polyarylester fiber comprises the following steps: step one, adding p-hydroxybenzonic acid, 2-(4-hydroxyphenyl)-5-carboxylbenzimidazole, acetic anhydride, 4-diethylaminopyridine and an antioxidant into a polymerization kettle for carrying out melt condensation polymerization to prepare a pre-polymer of thermotropic liquid crystal polyarylester; step two, putting the pre-polymer in a rotary kiln under the condition with nitrogen protection for carrying out solid phase polycondensation reaction to obtain high-molecular-weight polymer powder; step three, mixing the high-molecular-weight polymer powder, then cooling and drawing to prepare primary polyarylester fiber; and step four, carrying out heat treatment on the primary polyarylester fiber. The preparation method of the thermotropic liquid crystal polyarylester fiber is simple to operate; the tensile strength of the polyarylester fiber which is finally obtained can reach 4.0-4.5GPa.
Owner:HEILONGJIANG JUXIANG TECH DEV CO LTD

Reaction system and preparation method for nitrous alkyl ester

The invention relates to a reaction system for alkyl nitrite and a preparation method for the alkyl nitrite. The preparation method comprises the following steps that: a trickle-bed reactor is adopted and porcelain ring filler is filled into the trickle-bed reactor; liquid added into the reactor forms liquid membranes on the filler; alkyl alcohol is taken as a liquid-phase raw material and nitric monoxide, oxygen and nitrogen are taken as gas-phase raw materials; and gas and liquid phases are reacted in the trickle-bed reactor by means of co-current flow or countercurrent flow under the condition of nitrogen protection so as to generate the alkyl nitrite. The mol ratio of the alkyl alcohol to NO is between 2 to 1 and 7 to 1, and the mol ratio of the NO to O2 is between 4 to 1 and 8 to 1; the reaction temperature is between 40 and 100 DEG C, and the reaction pressure is between 0.1 and 1.0 MPa; and the retention time of continuous feeding of liquid-phase alkyl alcohol in the trickle-bed reactor is between 10 and 500 minutes, and the retention time of continuous feeding of gas phase in the trickle-bed reactor is between 0.02 and 1 minute. The reaction system and the preparation method have the advantages that: the operating condition is mild; the reaction time is short; the conversion rate of the raw materials, and the selectivity and the yield of products are high; and the whole reaction system is convenient for realizing continuous production, etc.
Owner:TIANJIN UNIV

Preparation method of PTFE (polytetrafluoroethylene) copper-clad plate with high elastic modulus

The invention provides a preparation method of a PTFE (polytetrafluoroethylene) copper-clad plate with a high elastic modulus, which comprises the following steps of: preparing copper foil and glass fiber cloth with a low dielectric constant, and preparing a fluororesin mixture; soaking the glass fiber cloth with the prepared fluororesin mixture, transferring the soaked glass fiber cloth into a baking oven for baking and drying, and repeating the steps to enable the glass fiber cloth to be soaked, baked and dried many times, thereby obtaining soaking pieces the resin content of which is about 60-70%; and superposing the soaking pieces, coating the copper foil on two sides, and laminating to obtain the PTFE copper-clad plate. The baking and drying process comprises three stages, wherein the temperature of the baking oven in the first stage is 50-100 DEG C, the temperature of the baking oven in the second stage is 200-320 DEG C, and the temperature of the baking oven in the third stage is 380-400 DEG C. The plate prepared by the method provided by the invention not only has a lower dielectric constant but also has a higher elastic modulus, and the plate has the advantages of consistent internal structure and good dimensional stability.
Owner:GUANGDONG SHENGYI SCI TECH

A high-performance cooper-coated aluminum rectangle section compound conductive bus bar and its making technology

ActiveCN101241778AMeet the requirements of multiple specificationsGreat widthSingle bars/rods/wires/strips conductorsMeasuring devicesCopperAluminum composites
The present invention provides a high-performance copper-clad aluminum cross section composite conductive bus-bar and the preparing technique thereof, and the invention relates to a rectangle-cross section bimetal composite material and the preparation thereof. The copper-clad aluminum rectangular cross section composite conductive bus-bar is compounded by the core-part aluminum and the coating layer copper. The area proportion of the coating copper layer is 15to 50 The technique comprises the following procedures: Adopting horizontal continuous casting for directly compounding and forming the copper-clad aluminum composite blank. Commonly flat-roller rolling and finish drawing-pulling the copper-clad aluminum blank according to requirement or rolling with the flat roller provided with a vertical roller, the range of the rolling speed is 3-50m / min, and the single-pass relative reduction is between 15and 40 The speed range of finish drawing-pulling is 1-20m / min and the single-pass cross section scalage is 10%. When the multiple-pass relative reduction is up to 70%, the low-temperature intermediate annealing is executed to the copper-clad aluminum composite conductive bus-bar. The annealing temperature is between 250 and 450 DEG C and the annealing time is between 0.5 and 3h. The annealed composite conductive bus-bar is executed with hole-form rolling or drawing. The invention not only can produce the high-performance copper-clad aluminum cross section composite conductive bus-bar, but also has the advantages of short process flow and high efficiency of the producing method.
Owner:UNIV OF SCI & TECH BEIJING

Fluoro-resin mixture, copper-clad plate made of same and making method thereof

The invention relates to a fluoro-resin mixture, a copper-clad plate made of the same and a making method thereof. The fluoro-resin mixture comprises the following two substances as necessary components: 90-99 parts by weight of polytetrafluoroethylene (PTFE) emulsion and 1-10 parts by weight of fluorinated ethylene propylene (FEP) based on 100 parts by weight of an organic solid matter. The copper-clad plate made of the fluoro-resin mixture comprises a plurality of pieces of superimposed varnished cloth and copper foils covering one side or two sides of the varnished cloth, wherein each piece of varnished cloth comprises glass fiber cloth and a fluoro-resin mixture adhered thereon through dipping drying. The fluoro-resin mixture is prepared by taking the PEFE emulsion as base resins, the glass fiber cloth can be dipped for many times in the mixture under the condition of below PTFE sintering temperature (330 DEG C) to obtain the varnished cloth. The varnished cloth made from the fluoro-resin mixture has favorable gum dipping quality, uniform gum content, smooth surface, softness and easy operation. The copper-clad plate made from the fluoro-resin mixture has favorable comprehensive properties, excellent dielectric properties, simple making method and process, satisfies the dielectric property requirements on substrate materials in the field of high frequency communication and is beneficial to industrial continuous production.
Owner:GUANGDONG SHENGYI SCI TECH

Preparation method for waterborne polyurethane synthetic leather Bass

The invention discloses a preparation method for a waterborne polyurethane synthetic leather Bass. The method comprises the following steps of: adding a dispersing agent, a polypropylene powder and a talcum powder to waterborne polyurethane under a stirring condition; after sufficiently dispersing these materials, adding a thickening agent to these materials to stir the materials, so as to obtain a waterborne polyurethane synthetic leather paste; before coating, adding a foam stabilizer to the waterborne polyurethane synthetic leather paste under a stirring condition; bubbling the paste by using compressed air, wherein the bubbling speed is 0.2-0.8 m3 / h; and stirring and bubbling the paste for 5-10 minutes at a speed of 600-1000 rpm; and then coating a waterborne polyurethane synthetic leather foaming paste to a base fabric, which is treated by a base fabric treating liquid and ironed by an ironing roller, wherein the coating quantity is 300-600 g / m2; and finally, drying the waterborne polyurethane synthetic leather foaming paste, so as to obtain the waterborne polyurethane synthetic leather Bass. According to the invention, a foaming material has the advantages of rapidness in foaming and good foam stabilizing property; and the preparation method disclosed by the invention has the advantages of simplicity, easiness and easiness for continuous production and is very suitable for large-scale industrial production.
Owner:HEFEI KETIAN WATERBORNE TECH CO LTD

Method for recovering nickel and molybdenum from waste nickel-molybdenum catalyst

The invention discloses a method for recovering nickel and molybdenum from a waste nickel-molybdenum catalyst. The method comprises the concrete steps of firstly carrying out primary low-temperature roasting, then carrying out secondary high-temperature alkali roasting, and transforming molybdenum and aluminum components in the waste catalyst into water-soluble sodium molybdate and sodium metaaluminate; then carrying out water leaching and solid-liquid separation to obtain a nickel slag and an alkaline filter liquor containing molybdenum and aluminum; carrying out acid leaching, evaporative crystallization and solid-liquid separation on the nickel slag to obtain a nickel sulfate product; and adding a barium salt precipitant into the filter liquor to separate the aluminum and the molybdenum, obtaining a refined aluminum-containing solution, adopting a chemical precipitation method to obtain an aluminum hydroxide precipitate, and calcining to obtain an aluminum oxide product. According to the method for recovering the nickel and the molybdenum from the waste nickel-molybdenum catalyst provided by the invention, valuable metals in the catalyst is comprehensively recycled, three products such as nickel sulfate, barium molybdate and aluminum oxide are obtained, the valuable metal recovery rate is high, the product added value is high, and the method has a certain application value.
Owner:XUZHOU GUOMAO VALUABLE & RARE METAL COMPREHENSIVE UTILIZATION INST +1

Vacuum insulated panel core material and manufacturing method thereof

The invention relates to a vacuum insulated panel core material and a manufacturing method thereof. the core material is small in heat conductivity coefficient and low in cost and comprises 70wt% to 100wt% of short chopped glass fiber strands with diameters in a range of 6 microns to 13 microns and lengths in a range of 4 millimeters to 20 millimeters and 0wt% to 30wt% of glass fiber cotton with diameters in a range of 1.0 microns to 4 microns and lengths in a range of 1 millimeters to 5 millimeters, wherein the short chopped glass fiber strands are produced through a strand drawing method, and the glass fiber cotton is produced through a flame method flame method. According to the manufacturing method for core panels, multi-layer liquid adding and multi-layer vacuum dewatering are used, the heat conductivity coefficient of the vacuum insulated panel core material is below 0.03W/m.k, and the heat conductivity coefficient of the vacuum insulated panel is below 0.0025 W/m.k, the heat conductivity coefficient is lower than that of a glass fiber cotton core material 100% produced through the flame method, the insulating effect is good, the manufacture cost of the vacuum insulated panel core material is saved greatly simultaneously, and the quality is stable and controllable.
Owner:CHANGZHOU SANYOU DIOR INSULATION MATERIALS MFG
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