The invention relates to a preparation method of nuclear-grade
graphite. The preparation method comprises the following steps: S1, mixing and kneading, S2, crushing, S3, isostatic pressing, S4,
roasting, S5, dipping, S6, graphitizing and S7, purifying. Nuclear-grade
graphite preparation equipment comprises a
roasting furnace and a purification furnace, the
roasting furnace comprises a sealed graphitization cavity, the front end and the rear end of the graphitization cavity are provided with a sealed feeding cavity and a sealed discharging cavity respectively, and the end of the feeding cavity and the end of the discharging cavity are each provided with an openable end sealing door; openable middle sealing
doors are arranged between the graphitization cavity and the feeding cavity and between the graphitization cavity and the discharging cavity,
backflow assemblies are arranged between the feeding cavity and the graphitization cavity and between the discharging cavity and the graphitization cavity, and each
backflow assembly comprises a
backflow pipe and a first sucking pump. The invention aims to solve or at least alleviate the defects in the prior art, and provides the nuclear-grade
graphite preparation method and preparation equipment, purification is carried out in the graphite roasting and purification process, and the method is simple and easy to operate, and is very suitable for large-scale production.