The invention belongs to the technical field of light-emitting materials and particularly relates to a preparation method of
zinc-doped
lutetium aluminum garnets. The preparation method comprises thefollowing steps: (1) adding high-purity
lutetium trioxide powder and aluminum
trioxide powder into absolute ethyl
alcohol, carrying out ultrasonic cleaning for 20-50 minutes, and
drying, so as to obtain a mixture; (2) adding the mixture into a
hydrochloric acid solution, and stirring until the mixture is completely dissolved, so as to obtain a
mixed solution; (3) adding
zinc chloride and hydroxy propyl
cellulose into the
mixed solution, and uniformly stirring, so as to obtain a dispersed
mixed solution; (4) slowly introducing
carbon dioxide into the dispersed mixed solution until no precipitate is generated, introducing
ammonia gas until no precipitate is generated, carrying out ultrasonic
filtration, repeatedly washing with absolute ethyl
alcohol, and
drying, so as to obtain a mixed precipitate; and (5) carrying out constant-temperature
drying on the mixed precipitate for 4-8 hours, cooling, crushing into
powder through ball milling, and calcining, so as to obtain the
zinc-doped
lutetium aluminum garnets. According to the preparation method, the technical blank of the zinc-doped lutetium aluminum garnets is solved, and a new
doping manner for lutetium aluminum garnets is provided.