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279results about How to "Change mechanical properties" patented technology

Method for extracting gas in low air permeability coal layer by pulse fracture anti-reflection

The invention relates to a method for extracting gas in low air permeability coal layer by pulse fracture anti-reflection, comprising the following steps: firstly using the blast-proof pulse-type coal layer high pressure water injector with adjustable frequency and pressure from the coal layer, high tunnel or low tunnel; using the pulse water effect generated by the periodical change of high pressure pulse water inside the drill hole of coal body, wherein the maximum pulse pressure is 35 MPa, the flow is about 300 L / min, and the pulse frequency is 0-1460 times / min; forcing the macroscopic fracture in the coal layer to be expanded and communicated; promoting the micro-pore fracture to be formed and extended; forming a new regeneration fracture net; providing a permeable channel of water inthe coal layer so as to achieve the effects of improving the mechanical property of the coal body, reducing the stress of the coal body in front of the working face and improving the discharge rate of the gas. Through the method, the pressure releasing range of the coal layer is enlarged, the whole pressure is adequately released, the radius of influence range of fracture can reach 10-40 m, and the air permeability of the coal body can be improved by 100-1000 times; and the method is simple, easy to operate and good in effect.
Owner:CHINA UNIV OF MINING & TECH

Preparation method of graphene based reinforced and flame-retarded recycled polyester staple fiber

The invention provides a preparation method of a graphene based reinforced and flame-retarded recycled polyester staple fiber. The method comprises the following steps: preparing graphene master batch; preparing phosphate based halogen-free flame retardant master batch; weighing the graphene master batch and the phosphate based halogen-free flame retardant master batch, mixing with a recycled polyester raw material, drying, feeding molten dried raw materials into an impurity removal stirrer under the action of a screw extruder by a melt pump for carrying out homogenization impurity-removal treatment, feeding a homogenized and impurity-removal polyester melt into a secondary filter by the melt pump, enabling a filtered melt to pass through a mixed melt on a pipeline to enter a spinning manifold, carrying out drafting processing on a spun fiber to obtain the reinforced and flame-retarded recycled polyester fiber, cutting off bundles and packaging. The reinforced and flame-retarded recycled polyester chip has the good spinning forming property, the fiber quality is high, the using amount of a fire retardant can be effectively reduced under the synergistic effect of grapheme and the phosphate based flame retardant, the cost is reduced, the reinforcement effect can be achieved and the mechanical property of the fiber is effectively improved.
Owner:NANJING UNIV OF AERONAUTICS & ASTRONAUTICS

Biodegradable resin material applied to oil and gas fields and preparation method for biodegradable resin material

InactiveCN104987682ANew mechanical propertiesChange mechanical propertiesDrilling compositionWell drillingAlloy
The invention provides a biodegradable resin material applied to oil and gas fields and a preparation method for the biodegradable resin material. According to the preparation method for the biodegradable resin material applied to the oil and gas fields, two or three polymers of polyglycolic-colactic acid, polycaprolactone and polylactic acid and a chain extender are subject to melt mixing reaction to obtain a resin alloy, namely the biodegradable resin material applied to the oil and gas fields. The biodegradable resin material applied to the oil and gas fields is prepared from the method, can be prepared into the shapes of sheets, powder, granules, spheres and the like, or can be prepared into the shapes of the sheets, the powder, the granules, the spheres and the like by one of the polyglycolic-colactic acid, the polycaprolactone and the polylactic acid, is used for temporarily blocking filtrate to protect a reservoir, temporarily blocking a blast hole, a constructed layer section and the like in various construction (well drilling, well completing, well repairing, and acidizing and fracturing) operations of the oil and gas fields, and has the advantages of complete degradation and zero damage to stratum.
Owner:CHINA UNIV OF PETROLEUM (BEIJING) +1

High-strength magnesium alloy and preparation method thereof

The present invention relates to a high intensity magnesium alloy and the preparation method. Magnesium, aluminum, zinc and neodymium are adopted as raw materials, which are melted in a melting furnace, under the protection of the mixed gases, and are melted down at the temperature of 720 plus or minus 10 degrees Celsius system, magnesium- neodymium alloy is added at the temperature of 780 plus or minus 10 degrees Celsius system, refined and the heat is preserved at the temperature of 740 plus or minus 10 degrees Celsius system and then the magnesium-aluminum-zinc-neodymium melt is obtained. When the temperature is lowered to 680-700 degrees Celsius system, the magnesium-aluminum-zinc-neodymium melt is discharged and cut into shapes after being moulded and cooled and then made into high intensity aluminum-magnesium alloy ingots after an 8-channel equal channel rotor angle pinch. The raw material mixture ratio of magnesium, aluminum, zinc and neodymium is 82 to 15 to 2 to 1 and aluminum makes up 15 percent. The aluminum material is abundant in resource, low in price and more economical and the lanthanon neodymium can change the metallurgical structure and mechanical property. The method has a short process flow and a slight pollution to the environment. The tensile strength, yield strength and elongation of the magnesium alloy ingots can be increased by 147.4 percent, 210.6 percent and 448.3 percent respectively. The metallurgical structure is compact and even and the average crystal grain size is less than or equal to 2 micrometers.
Owner:TAIYUAN UNIV OF TECH

Copolymer of polyarylether nitrile containing chian element of iso-benzene and preparation method

This invention relates to arylether-nitrile copolymer with isobenyl units. This invention can facilitate easy breakage of structural symmetry, easy control over the synthesis process, and easy increase of the product molecular weight by copolymerization reaction. This invention can control the structure and properties of the product by adjusting the ratio of resocin to the other dihydric phenol as well as its variety. This method can change the mechanical and thermal properties of the copolymer by changing the variety of the dihydric phenol, and improve the mechanical and thermal properties by increasing the amount of the dihydric phenol. This invention has such advantages as low raw material cost, abundant raw materials, low product price, high cost performance, and wide applications.
Owner:UNIV OF ELECTRONIC SCI & TECH OF CHINA

Outburst coal bed hydraulic phase change cracking cross-cut coal uncovering method

The invention provides an outburst coal bed hydraulic phase change cracking cross-cut coal uncovering method, which is applicable to high-gas-outburst coal bed cross-cut coal uncovering operation. The minimum normal distance from the cross-cut coal uncovering working face to the coal bed is greater than or equal to 7m position, a plurality of holes are respectively drilled in the coal uncovering region, a conventional capsule hole sealing coal bed water injection technology is adopted for injecting water into the coal bed through the drilled holes, after the water injection completion, a conventional refrigeration freezing technology is adopted for freezing the coal bed around the water injection hole, in the freezing process, free water in the coal bed is gradually converted from the liquid state into the solid state, and the volume of the water expands for 9.1 percent in the phase change process; after the freezing completion, the freezing coal bed absorbs the underground environment head and gradually thaws. After the freezing thawing completion, the water injection hole and a gas extraction pipeline are connected for gas extraction, or the gas extraction drilling is implemented on the coal bed in the phase change cracking region for gas extraction. When the coal bed gas content is less than 8m<3> / t, the gas extraction is stopped, the water is injected into the water injection hole again, the secondary freezing of the coal bed is completed, and then, the coal bed is uncovered according to a conventional coal uncovering method.
Owner:CHINA UNIV OF MINING & TECH

Polyamide 66 membrane covered nickel-titanium alloy intravascular scaffold and preparation method thereof

The invention relates to a polyamide 66 membrane covered nickel-titanium alloy intravascular scaffold and a preparation method thereof. The intravascular scaffold comprises a nickel-titanium alloy scaffold and a polyamide 66 membrane, and is provided with a tubular blood vessel shaped structure or a cylindrical blood vessel shaped structure, wherein the surfaces of an inner wall and an outer wallof the scaffold are covered by thin membranes with the thickness between 0.2 and 5 millimeters. The preparation method comprises the following steps of: preparing 1 to 20 percent of polyamide 66 solution by using formic acid as a solvent; coating a layer of the polyamide 66 solution on a glass rod and volatizing the solvent; sleeving a nickel-titanium shape memory alloy expanding scaffold on the glass rod; coating another layer of the polyamide 66 solution on the glass rod and volatizing the solvent; and peeling off the polyamide 66 membrane and the nickel-titanium alloy intravascular scaffold from the glass rod, and performing vacuum drying to obtain the polyamide 66 membrane covered intravascular scaffold. The intravascular scaffold prepared by the method has a stable structure, good mechanical property, transportability and anti-seepage property, overcomes the performance defects of a single material, and has a simple preparation process.
Owner:DONGHUA UNIV

Core-shell type pre-charged chemotherapy medicine embolization microsphere and preparation method thereof

The invention provides a core-shell type pre-charged chemotherapy medicine embolization microsphere and a preparation method thereof. The method comprises the following steps of using water/oil/water(W/O/W) complex emulsion type or oil/water/oil (O/W/O) complex emulsion type emulsified micro liquid drips as templates; coating tiny liquid drips containing medicine into outer layer liquid drips; high molecular polymers in the inner and outer layer liquid drips are converted through measures such as physical measures and chemical measures to form an inner layer core and an outer layer shell. Theformed core-shell structure medicine microsphere is formed by polymers of two-layer structures; the inner core contains medicine; the outer shell is favorable for maintaining the activity of the inner core medicine; the stable medicine release is realized; the sudden release is prevented; the safety is enhanced. The medicine carried microsphere prepared by the method has the advantages that the particle diameter range is 10 to 1000 micrometers; the sphere degree is good; the particle diameter is uniform; (the dimension deviation is 5 percent); the medicine encapsulation rate is high; the structure/carried medicine is controllable; meanwhile, the preparation method of the pre-charged chemotherapy medicine embolization microsphere can provide a novel idea for the clinic application study ofthe transcatheter arterial embolization.
Owner:ENERGY RES INST OF SHANDONG ACAD OF SCI

Chemically mechanical polishing solution

The present invention belongs to the field of chemical and mechanical polishing technology in microelectronic processing, and is especially chemical and mechanical polishing fluid for multilayer insulating film in superlarge scale integrated circuit manufacture. The polishing fluid has nanometer spherical mesoporous powder as grinding material and contains nanometer spherical mesoporous powder as grinding material, stabilizer, surfactant, pH regulator to regulate pH to 8.5-12.5, and high purity deionized water. The present invention utilizes the grinding material with rich surface hydroxy groups and excellent dispersivity in water in polishing interlayer medium of integrated circuit, and has no submicron scratches, high levelness, easy cleaning and high polishing rate.
Owner:INST OF METAL RESEARCH - CHINESE ACAD OF SCI

Cellulose-reinforced polyurethane/epoxy resin interpenetrating polymer network hard composite foam material and preparation method thereof

The invention discloses a cellulose-reinforced polyurethane / epoxy resin interpenetrating polymer network hard composite foam material and a preparation method thereof, relates to a foam material and a preparation method thereof and aims at solving the problems that existing polymer formed through mutual interpenetrating of two types of polymer, namely polyurethane and epoxy resin, is poor in sound absorption property and low in mechanical property. The sound absorption property of the composite foam material ranges from 80% to 92%, and the composite foam material is prepared from polyether polyol, isocyanate, water, a foaming agent, foam stabilizer, initiator, hydrosol of nano-crystalline cellulose with the mass percentage being 1%, chain extender, a cross-linking agent and epoxy resin. The preparation method comprises the steps of firstly, mixing the polyether polyol, the foam stabilizer, the initiator, the foaming agent, the chain extender and the water with cellulose obtained after pretreatment, then adding the epoxy resin and the cross-linking agent, and obtaining a mixture; then mixing the isocyanate with the mixture, conducting stirring till bubbles are generated, leaving the mixture standing still, obtaining a foamed mixture, finally, conducting curing on the foamed mixture at the room temperature, and then conducting curing at the high temperature.
Owner:NORTHEAST FORESTRY UNIVERSITY

Freezing-type stone door cross-measure coal uncovering method based on hydraulic seam cutting

A freezing-type rock cross-measure coal uncovering method based on hydraulic seam cutting is suitable for a rock cross-measure coal uncovering operation in a high-gas outburst coal seam. The method includes following steps: (1) constructing a plurality of water injection holes into a coal uncovering operation surface at a position of the coal uncovering operation surface, wherein a minimum normal distance from the coal seam to the position is not less than 7 m; (2) performing hydraulic seam cutting to the water injection holes through a conventional hydraulic seam cutting technology; (3) when the hydraulic seam cutting is finished, connecting the water injection holes to a gas extraction pipe network to perform gas extraction; (4) when the content of gas in the coal seam is less than 8 m<3> / t, stopping the gas extraction; (5) constructing a freezing holes and a temperature measuring hole respectively at the two sides of the water injection holes; (6) sealing the holes through a capsule hole-sealing device; (7) injecting water into the coal seam through the water injection holes and closing valves when the water injection process is finished to enable the water injected into the coal seam to gradually seep into micro cracks in coal; (8) freezing the coal seam around the water injection holes through a conventional freezing technology to enable free water in the micro cracks in the coal seams to gradually convert from liquid phase into solid phase during the freezing process, so that a strength and an anti-impact performance of the coal are increased and an effect of solidification of the coal seam is achieved; and (9) uncovering the coal seam through a conventional coal uncovering method.
Owner:CHINA UNIV OF MINING & TECH

High-temperature high-power rare earth resistance paste and preparation method thereof

The invention discloses a high-temperature high-power rare earth resistance paste and a preparation method thereof. The high-temperature high-power rare earth resistance paste comprises a functional phase, an inorganic adhesive phase, a burning promoter and an organic carrier, wherein the functional phase is composite powder consisting of micrometer silver powder and bismuth ruthenate powder; the inorganic adhesive phase is lead-free pyroceram powder consisting of SiO2, MgO, B2O3, ZnO, Bi2O3, rare earth oxides and a nucleation agent; and the organic carrier is a mixture consisting of a solvent, resin, a dispersing agent, a deforming agent and a thixotropic agent. The resistance paste has the advantages that firstly, the damages of lead on the environment and human bodies can be avoided; secondly, the resistance paste is high in compatibility, wettability, thermal performance, electrical performance, manufacturability and adaptability; thirdly, the resistance paste is high in binding performance with ceramic and stainless steel substrates; and fourthly, the resistance paste is high in printing performance, burning performance and compatibility. The preparation method comprises preparation of the inorganic adhesive phase, preparation of the functional phase, preparation of the organic carrier and preparation of the resistance paste in sequence, and the resistance paste can be produced and prepared effectively.
Owner:DONGGUAN COREHELM ELECTRONICS MATERIAL TECH CO LTD

Polysiloxane and glycidol-containing strong-hydrophobicity gelatin leather finishing agent and preparation method

The invention relates to a polysiloxane and glycidol-containing strong-hydrophobicity gelatin leather finishing agent and a preparation method. The preparation method comprises the following steps: dissolving gelatin in water to prepare aqueous solution with mass concentration of 2-20 percent; adding glycidol into a first reaction flask under the conditions of temperature of 40-70 DEG C and pH of 6-12 to obtain solution 1; adding a surfactant into a second reaction flask, continuously stirring, and meanwhile adding Si-O-Si repetitive unit-containing epoxypolysiloxane in batches or continuously to obtain solution 2, wherein the using amount of the surfactant is 0.5-20 percent of the mass of the gelatin; mixing the solution 1 and the solution 2 in different proportions, weighing 15-20 g of the mixed solution to be placed in a mold of polytetrafluoroethylene, adding 5-10 mL of one or two or three of ethanol, tetrahydrofuran and methanol and drying in a normal pressure drying oven at the temperature of 40-80 DEG C to obtain the gelatin leather finishing agent with a superior function. The finishing agent has the characteristics of strong hydrophobicity, super extensibility, heat resistance, oxidation resistance, wet scrubbing resistance and the like.
Owner:QILU UNIV OF TECH

Method for improving dispersibility of single-walled carbon nanotube in aqueous solution

The invention belongs to the field of materials chemistry and in particular relates to a method for improving the dispersibility of a single-walled carbon nanotube in aqueous solution. The method comprises the following detailed steps of: dispersing a single-walled carbon nanotube purification sample in the aqueous solution of ethanol, and performing ultrasonic dispersion on the sample to uniformly suspense the sample in the solution; quickly cooling the obtained solution by using liquid nitrogen as a cooling medium and continuously supplying the cooling medium to guarantee that the cooling temperature of the sample reaches -50 to -190 DEG C; at normal temperature and under normal pressure, placing the solid sample in a closed device in which a high-speed blade rotates, wherein the rotation speed is 22,500rpm, the rotation time is 1 minute and the crushing process is repeated for 1 to 7 times; and filtering and drying the obtained sample to obtain the single-walled carbon nanotube aqueous solution with relatively good water solubility finally. In the invention, a physical method is adopted at normal temperature and under normal pressure, so that the structure of the single-walled carbon nanotube in aqueous solution is not damaged in a treatment process; the ethanol serving as a raw material is simple and available and causes no pollution to environment; and the method has the advantages of simple process and easy processing, so that the method is suitable for commercial production.
Owner:TONGJI UNIV

Sweet potato collecting equipment

The invention discloses sweet potato collecting equipment. The sweet potato collecting equipment comprises an equipment body, rollers, a tractor connection arm, a digging shovel, a soil sieving mechanism, a conveying mechanism and a sweet potato collecting box, wherein the rollers are rotationally arranged on the lower part of the equipment body; one end of the tractor connection arm is hinged to the equipment body; the digging shovel is arranged below the front part of the equipment body, and is used for digging out planted sweet potatoes; the soil sieving mechanism is arranged on the back part of the equipment body, and is used for sieving soil from the dug sweet potatoes; the sweet potato collecting box is used for collecting sweet potatoes from which soil is sieved by the soil sieving mechanism. Through adoption of the sweet potato collecting equipment, the current situation that mechanical digging and manual collection are adopted at present can be improved, and the aims of digging, soil sieving and collecting of the sweet potatoes from a growing underground environment are fulfilled at a time.
Owner:YANCHENG INST OF TECH
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