The invention relates to a preparation method of a high-performance sintered Nd-Fe-B permanent
magnet material, belonging to the field of
rare earth permanent
magnet material. The
quaternary and abovequaternary
rare earth alloy films are deposited on the surface of pretreated Nd-Fe-B
magnet by magnetron
sputtering. The homogenization,
grain boundary diffusion and low temperature
tempering are used as
diffusion sources to improve the
boundary structure of the magnet, so that the
coercivity of the magnet is greatly increased and the
remanence is kept basically unchanged. The composition of thequaternary and above
quaternary rare earth alloy film is LRE 100-X-Y-ZHRExMyAlz (1 <= x <= 40, 1 <= y <= 20, 1 <= z <= 20), wherein LRE is one or more of the light rare earth elements such as Y, La, Ce, Pr, Nd, HRE is one or more of the heavy rare earth elements such as Tb, Dy, Ho, and M is one or more of the
alloy elements such as Cu, Fe, Co, Ga, Zr, Zn, Mn, and Mg. The rare earth alloy thin filmprepared by the invention is uniform, compact and strong in adhesion as
diffusion source, the quantity is continuously controllable, and the consistency of magnetic properties of the magnet after diffusion treatment is good; It can reduce the amount of rare earth and is suitable for industrial production.