The invention relates to the technical field of
consumer goods detection, and discloses a detection method for rapidly determining the content of twenty-two
flame retardants in
consumer goods, which comprises the following steps: S1, preparing a liquid sample; s2, putting a
solid sample to be detected into a
reaction tube, and adding a liquid sample; step S3, extracting; and S4, analyzing the sample solution by adopting a liquid chromatograph-
mass spectrometer. The method can simultaneously detect the content of twenty-two organic
flame retardants, utilizes ultrasonic extraction and LCMSMS analysis, makes up the disadvantages of
gas chromatography, can rapidly determine the content of twenty-two organic
flame retardants, is simple in operation and short in analysis time, and has very high
test efficiency. According to the method, the
repeatability is 0.3%-3.8%, the reproducibility is 1.3%-2.7%, the
detection limit of the method is as low as 0.02 mg / kg, and the method completely meets the control requirements of all countries and the
test requirements of customers.