The invention discloses a method for preparing MXene through
fluoride-free
etching of an ultrasonic-assisted
supercritical carbon dioxide flash explosion technology, and relates to the field of MXene preparation, MXene is prepared through a one-pot method by utilizing the synergistic effect of a high-frequency power
ultrasonic technology, a flash explosion technology and a
supercritical carbon dioxide fluid medium, and the MXene is prepared through a high-frequency power
ultrasonic technology, a flash explosion technology and a
supercritical carbon dioxide fluid medium. Putting the
fluoride-free
etching agent and the MAX phase into a supercritical reaction kettle; introducing
carbon dioxide to enable the
carbon dioxide to reach a supercritical state, and applying continuous or discontinuous high-frequency power ultrasonic treatment to carry out supercritical state
etching reaction; after the reaction is finished, carrying out instantaneous supercritical flash explosion treatment; releasing the pressure of the flash explosion area and the buffer area, collecting the product, centrifuging, washing and
drying to obtain an MXene product; according to the method, the production of
fluorine-containing waste liquid is avoided, the etching efficiency and the product yield are remarkably improved by virtue of high permeability and
mass transfer characteristics of supercritical
carbon dioxide, and a new way is provided for large-scale preparation of various MXene materials.