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34results about How to "Reduce oxygenation" patented technology

Method for preparing large powder metallurgy TZM blank with uniform carbon and oxygen distribution

The invention discloses a method for preparing a large powder metallurgy TZM blank with uniform carbon and oxygen distribution, which comprises the following steps of: 1, weighing raw materials; 2, mixing powder, namely mixing the weighed four raw materials twice under vacuum or the protection of inert gas, mixing titanium hydride powder, zirconium hydride powder and carbon black powder to prepare mixed powder, adding a volatile organic solvent into the mixed powder, uniformly stirring to prepare suspension, adding the weighed molybdenum powder into the suspension for uniform mixing, and adding residual molybdenum powder for uniform mixing; 3, performing cold isostatic pressing; and 4, sintering by keeping the temperature at stages, namely adopting a vacuum sintering furnace and sintering at three stages, wherein the process comprises the following steps of: raising the temperature at the first stage, raising the temperature at the second stage, and sintering at high temperature. The preparation method has the advantages of reasonable design, simple and convenient operation, and good using effect. The carbon content in the center and on the surface of the prepared larger-size TZM blank can be controlled to be approximately consistent, and the oxygen content in the center and on the surface of the TZM blank also can be reduced to a lower level.
Owner:NORTHWEST INSTITUTE FOR NON-FERROUS METAL RESEARCH

Oxygen control slag system for electroslag furnace and preparation method thereof

The invention relates to an oxygen control slag system for an electroslag furnace and a preparation method thereof, and belongs to the technical field of metallurgical smelting. In order to solve theproblems that the deoxidation capacity of the existing premelting slag is weak and the cost is high, the invention provides the oxygen control slag system for the electroslag furnace. The oxygen control slag system for the electroslag furnace is prepared from the following components in percentage by weight: 30 to 32 percent of self-made premelting slag, 43 to 45 percent of Al2O3, 20 to 22 percentof CaO and 3 to 5 percent of MgO, wherein the self-made premelting slag has the SiO2 content of less than or equal to 1.5 percent through desilicication treatment, and also contains 2 to 3 percent ofaluminum, so that a good deoxidation effect can be achieved; and the CaO, the Al2O3 and the MgO can further improve the deoxidation capacity of the slag system. The oxygen control slag system for theelectroslag furnace provided by the invention is low in cost, simple in preparation process, good in energy saving and consumption reducing effects, and stable in remelting chemical components. The oxygen control slag system provided by the invention is utilized for melting steel, which can make the internal quality of an electroslag steel ingot uniform, the surface of a cast ingot smooth, and detection indicators excellent.
Owner:建龙北满特殊钢有限责任公司

Beryllium-aluminum alloy powder and preparation method and application thereof

The invention provides beryllium-aluminum alloy powder and a preparation method and application thereof. The preparation method comprises the following steps of placing a beryllium-aluminum alloy rodin a vacuum environment; introducing inert gas into the vacuum environment to replace air, wherein the oxygen content in the replaced vacuum environment is smaller than 6 ppm; melting the end surfaceof the beryllium-aluminum alloy rod by means of arc to form a liquid film; crushing the liquid film to fine liquid drops by means of centrifugal force; and carrying out cooling to obtain the beryllium-aluminum alloy powder. The beryllium-aluminum alloy powder may comprise the beryllium-aluminum alloy powder prepared through the preparation method of the beryllium-aluminum alloy powder. The application may comprise application of the beryllium-aluminum alloy powder in the field of laser or electron beam additive manufacturing and / or in the field of laser or electron beam cladding. The inventionhas the beneficial effects that the preparation method is high in production efficiency and low in energy consumption; the prepared beryllium-aluminum alloy powder is good in degree of sphericity, free of hollow powder basically, low in oxygenation amount in the manufacturing process and good in flowability and is a good raw material for 3D printing.
Owner:西藏智材新材料有限公司

Method for treating sewage with low carbon nitrogen ratio

The invention belongs to the technical field of sewage treatment and discloses a method for treating sewage with a low carbon nitrogen ratio. The method comprises the following steps of (1) preparation of a solid carbon source filler bio-membrane reactor, specifically, the bio-membrane reactor is filled with a solid carbon source material, inoculated active sludge and sewage are poured into the bio-membrane reactor, the bio-membrane reactor is emptied after a period of time of standing, sewage is injected from the bottom of the bio-membrane reactor in an aerated state till biofilm formation succeeds; and (2) synchronous nitrification and denitrification of the sewage, specifically, the sewage is injected continuously from the bottom of the solid carbon source filler bio-membrane reactor inthe aerated state, the sewage is subjected to synchronous nitrification and denitrification when flowing through the solid carbon source material, and then water is discharged from the upper part ofthe solid carbon source filler bio-membrane reactor. The method effectively reduces the concentration of organic matter, reduces the aeration amount required for the aerobic reaction, and improves thesewage treatment efficiency. According to the method, the cost is low, the energy consumption of projects is reduced, the occupied space is small, and the characteristics of being flexible, economical, environmentally friendly and the like are achieved.
Owner:GUANGZHOU UNIVERSITY

Screening method of 3D printing powder

The invention discloses a screening method of 3D printing powder, and the method comprises the steps of screening powder prepared by gas atomization by using an air classifier, and removing ultrafinepowder with the granularity of -15 [mu]m to obtain powder with the granularity of 15-250 [mu]m; carrying out ultrasonic screening on the powder with the granularity of 15-250 [mu]m by using a glove box to obtain printing powder with the granularity of 15-45 [mu]m; and packaging the printing powder with the granularity of 15-45 [mu]m. According to the invention, ultrafine powder and large-particle-size powder in the powder are removed in sequence by continuously screening the powder prepared by gas atomization; and the quantity of the ultrafine powder is effectively reduced by controlling the rotating speed and the air input of the wind wheel of the air classifier, the ultrasonic frequency and the screening time of an ultrasonic vibration screening machine, the humidity and the oxygen increasing amount of the printed powder are effectively reduced by controlling the parameters such as the water content and the oxygen content of the glove box, and the gas-filled packaging prevents the vacuum packaging from causing powder agglomeration and adhesion to influence the flowability of the powder..
Owner:CHENGDU ADVANCED METAL MATERIALS IND TECH RES INST CO LTD

Multi-sectional hydrogenation dehydrogenation furnace and manufacturing method of low-oxygen-content titanium powder

The invention provides a multi-sectional hydrogenation dehydrogenation furnace which comprises a heating furnace, a reactor, a gas storage tank, a cooling device and a movable support, wherein the heating furnace and the reactor are horizontally placed. The reactor is a cylinder with two closed ends and formed by sequentially jointing a heating part section, a middle part section and a cooling part section, a material feeding and discharging port is formed in the end of the cooling part section and provided with a sealing cover, and a gas inflow and outflow port is formed in the sealing cover or the cylinder. The cooling device is provided with a first thermoelectric couple. The heating furnace is provided with a second thermoelectric couple. The gas storage tank is provided with a pressure gauge, a reactor joint, a vacuumizing joint and a hydrogen source joint. The reactor is installed on the movable support. The heating part section of the reactor is located in a hearth of the heating furnace. The cooling device is installed on the cooling part section of the reactor. The reactor joint on the gas storage tank is communicated with the gas inflow and outflow port of the reactor through a pipe. The invention further provides a manufacturing method of low-oxygen-content titanium powder. The oxygen content of the titanium powder manufactured through the method does not exceed 0.1wt%.
Owner:SICHUAN UNIV

A kind of beryllium aluminum alloy powder and its preparation method and application

The invention provides a beryllium aluminum alloy powder and a preparation method and application thereof. The preparation method may include the following steps: placing the beryllium aluminum alloy rod in a vacuum environment; passing an inert gas into the vacuum environment to replace the air, and after the replacement, the oxygen content in the vacuum environment is below 6 ppm; using an electric arc to make the beryllium aluminum alloy rod The end face is melted to form a liquid film; the liquid film is broken into fine droplets by centrifugal force; cooled to obtain beryllium aluminum alloy powder. The beryllium aluminum alloy powder may include beryllium aluminum alloy powder prepared by the above-mentioned preparation method of beryllium aluminum alloy powder. The applications may include applications in the field of laser or electron beam additive manufacturing, and / or applications in the field of laser or electron beam cladding. The beneficial effects of the present invention may include: the preparation method has high production efficiency and low energy consumption; the prepared spherical beryllium aluminum alloy powder has good sphericity, basically no hollow powder, low oxygen increase in the preparation process, good fluidity, and is 3D Good raw material for printing.
Owner:西藏智材新材料有限公司

Oxygen-controlled slag system for electroslag furnace and preparation method thereof

The invention relates to an oxygen control slag system for an electroslag furnace and a preparation method thereof, and belongs to the technical field of metallurgical smelting. In order to solve theproblems that the deoxidation capacity of the existing premelting slag is weak and the cost is high, the invention provides the oxygen control slag system for the electroslag furnace. The oxygen control slag system for the electroslag furnace is prepared from the following components in percentage by weight: 30 to 32 percent of self-made premelting slag, 43 to 45 percent of Al2O3, 20 to 22 percentof CaO and 3 to 5 percent of MgO, wherein the self-made premelting slag has the SiO2 content of less than or equal to 1.5 percent through desilicication treatment, and also contains 2 to 3 percent ofaluminum, so that a good deoxidation effect can be achieved; and the CaO, the Al2O3 and the MgO can further improve the deoxidation capacity of the slag system. The oxygen control slag system for theelectroslag furnace provided by the invention is low in cost, simple in preparation process, good in energy saving and consumption reducing effects, and stable in remelting chemical components. The oxygen control slag system provided by the invention is utilized for melting steel, which can make the internal quality of an electroslag steel ingot uniform, the surface of a cast ingot smooth, and detection indicators excellent.
Owner:建龙北满特殊钢有限责任公司
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