143 results about "Cyclobutene" patented technology

The present invention discloses novel compounds which have HCV protease inhibitory activity as well as methods for preparing such compounds. In another embodiment, the invention discloses pharmaceutical compositions comprising such compounds as well as methods of using them to treat disorders associated with the HCV protease.

The invention relates to a manufacturing method for a soft magnetic core spiral micro-inductor, which is characterized by integrating a NiFe-AlOx soft magnetic core spiral micro-inductor and comprising the following steps: 1) preparing lower-layer metal of an inductor; 2) preparing a first benzo-cyclobutene BCB dielectric layer; 3) preparing a NiFe-AlOx film; 4) preparing a second benzo-cyclobutene BCB dielectric layer; 5) preparing a benzo-cyclobutene BCB dielectric through hole; and 6) preparing upper-layer metal of the inductor. The manufacturing method has the advantages that the soft magnetic core spiral micro-inductor for an RF / MMIC (Radio Frequency / Monolithic Microwave Integrated Circuit) is prepared by integrating a soft magnetic material with an MMIC micro-inductor. Compared with the micro-inductor free from the magnetic core, the soft magnetic core spiral micro-inductor has the advantages: (1) the inductance volume is greatly increased; (2) the quality factor is certainly increased; and (3) the whole technology is compatible with the manufacturing technology of a GaAs and GaN MMIC.

Provided is a dielectric / barrier rib composition for a plasma display panel, comprising a compound 1 of the formula or at least one compound belonging to a polyhedral oligosilsesquioxane (compound 2) having R6SiO1.5 as a repeating unit, or comprising inorganic / organic hybrid materials having compounds 1 and 2 as a monomer, wherein X is an integer inclusive 0, R1, R2, R3, R4, R5 and R6 are independently a linear, branched or cyclic C1-C12 hydrocarbon group containing one or more alkyl, alkoxy, ketone, acryl, methacryl, allyl, aromatic, halogen, amino, mercapto, ether, ester, sulfone, nitro, hydroxyl, cyclobutene, carbonyl, carboxyl, alkyd, urethane, vinyl, nitrile, hydrogen, or epoxy functional group, and A is oxygen or NH. The inorganic / organic hybrid materials can be a material composed of an extended matrix, containing silicon and oxygen or nitrogen atoms, and having at least one silicon fraction directly bonded to a substituted or unsubstituted hydrocarbon atom.

The present invention provides methods of making low energy polymerizable monomers and resins for use in making dielectric materials. The methods comprise deprotecting or deacylating an organic alkali cleavable protecting group containing addition polymerizable, amine containing aromatic monomer or oligoaromatic phenol resin containing an organic alkali cleavable protecting group, such as a C2 to C9 alkanoyl group, preferably, an acyl group, by hydrolyzing to remove the protecting group in organic alkali in a polar solvent containing an excess of alkali C1 to C7 alkoxide and form a hydroxyl functional monomer or resin, followed by; reacting via nucleophilic substitution the resulting hydroxyl functional monomer or resin with an alpha-halide (α-halide) or strong acid conjugate leaving group containing arylcyclobutene compound in a polar solvent, to yield a product an arylcyclobutene-containing addition polymerizable or amine containing aromatic monomer or oligoaromatic phenol resin having an ether linkage from the cyclobutene ring to an aromatic group of the addition polymerizable aromatic monomer, aromatic amine or oligoaromatic phenol.

The invention relates to a high molecular material and discloses an adamantyl benzocyclobutene monomer and a synthesizing method of a polymer of the adamantyl benzocyclobutene monomer. According to the adamantyl benzocyclobutene monomer and the synthesizing method of the polymer of the adamantyl benzocyclobutene monomer, the structural formula of the adamantyl benzocyclobutene monomer is shown as the specification, wherein a formula in the specification is adamantane; a formula in the specification is benzocyclobutene; O is oxygen and Si is silicon; m and n are the quantities of substituent groups on 1, 3, 5 and 7 sites of the adamantane; the sum of the m and the n is smaller than or equal to 4; the n is more than or equal to 1 and less than or equal to 4; R1 is a first fat substituent group or a first aromatic substituent group; R2 is a second fat substituent group or a second aromatic substituent group; R3 is a third fat substituent group or a third aromatic substituent group. The adamantyl benzocyclobutene monomer prepared by the invention is used for carrying out a polymerization reaction to obtain an adamantyl benzocyclobutene monomer polymer. According to the adamantyl benzocyclobutene monomer and the synthesizing method of the polymer of the adamantyl benzocyclobutene monomer, the adamantyl benzocyclobutene monomer and the polymer thereof have low dielectric constants and low dielectric losses; the dielectric properties are good; meanwhile, the adamantyl benzocyclobutene monomer and the polymer thereof have higher hydrophobic property and heat resistance.

The invention relates to novel cycloalkyl- or cycloalkenyl-substituted pyrazolopyrimidinones of formula (I), wherein A is selected from the group A1 consisting of a C3-C8-cycloalkyl group or a C4-C8-cycloalkenyl group, whereby the members of C3-C8-cycloalkyl group being selected from the group of cyclopropyl, cyclobutyl, cyclopentyl, cyclohexyl, cycloheptanyl and cyclooctanyl; and the members of the C4-C8-cycloalkenyl group, being selected from cyclobutenyl, cyclopentenyl, cyclohexenyl, cycloheptenyl, cyclooctenyl, cyclopentadienyl, cyclohexadienyl, cycloheptadienyl, cyclooctadienyl, cycloheptatrienyl, cyclooctathenyl, cyclooctatetraenyl. The new compounds shall be used for the manufacture of medicaments, in particular medicaments for improving perception, concentration, learning and / or memory in patients in need thereof. Chemically, the compounds are characterised as pyrazolopyrimidinones with a cycloalkyl-moiety directly bound to the 1 position of the pyrazolopyrimidinone and a second substituent in the 6 position which is bound via an optionally substituted methylene-bridge. Further aspects of the present invention refer to a process for the manufacture of the compounds and their use for producing medicaments.

The characteristics is that this kind of monomer includes two new monomers. Benzo cyclobutane-4-boracic acid or the ester, or benzo cyclobutane-4-boracic acid or the ester and 4-bromo-benzo cyclobutane, or dihalogeno arene and benzo cyclobutane-4-boracic acid or the ester, or arylhypoboric acid or the ester and 4-bromobenzene cyclobutane are used as reaction material to be stirred with catalytic agent, inorganic alkali dissolvant more than 3 hours on room temp. in the air or nitrogen gas, then monomer I or / and monmer II is produced by a series of reprocessing.

An OLED device including a cathode, an anode, and having therebetween a light-emitting layer and further comprising a first layer between the light-emitting layer and the cathode containing a cyclobutene compound comprising a cyclobutene nucleus substituted in the 1-position with a five- or six-membered heteroaromatic ring group containing at least one trivalent nitrogen atom; substituted in the 2-position with an aromatic ring group; and substituted with a first methylene group in the 3-position and a second methylene group in the 4-position, provided said first and second methylene groups are further disubstituted in the 1′,1′-positions and the 1″,1″-positions with independently selected aromatic groups.

The invention relates to a preparation method of hexafluorobutadiene, which comprises the following steps: respectively dehydrating a 3, 4-dichlorohexafluoro-1-butene raw material and an organic solvent, adding the dehydrated 3, 4-dichlorohexafluoro-1-butene raw material and the dehydrated organic solvent into a dechlorination reaction kettle together with zinc powder, carrying out a dechlorination reaction to obtain a dechlorination product, and carrying out rectification and catalytic conversion on the dechlorination product to obtain a hexafluorobutadiene product. Compared with the prior art, the method has the advantages that the by-product is rearranged into hexafluorobutadiene by using a catalyst, and rectification purification is combined, so that the purity of the obtained hexafluorobutadiene product is high, the content of impurities such as hexafluoro-2-butyne and hexafluorocyclobutene in the hexafluorobutadiene product is remarkably reduced, the difficulty of downstream production of high-purity hexafluorobutadiene can be reduced, and the purity requirement on 3, 4-dichlorohexafluoro-1-butene raw material is reduced from 99.95% to 99%, the requirement on the purity of the 3, 4-dichlorohexafluoro-1-butene raw material is reduced, the pressure of upstream production and investment is greatly reduced, and the height of a rectifying tower for producing the 3, 4-dichlorohexafluoro-1-butene can be greatly reduced.

Disubstituted 3,4-diamino-3-cyclobutene-1,2-dione compounds are disclosed that are represented by general formula (I). Also disclosed, are pharmaceutical compositions including these compounds and methods of using these compounds and compositions for the treatment of chemokine-mediated pathologies.

The invention belongs to the technical field of polymer dielectric materials and in particular relates to benzocyclobutene monomers containing siloxane and imide structure and a synthesis method and application of the Benzocyclobutene monomers. Hydrosilylation reaction is allowed to take place between hydrogen-terminated polysiloxane / siloxane and 5-norbornylene-2,3-dianhydride in the presence of platinum catalysts to produce an intermediate compound, and imidization reaction is allowed to take place between the intermediate compound and 4-aminobenzocyclobutene to obtain the target monomers. The monomers have good solubility, and can be directly formed by thermal polymerization or dissolved in solvents to make films by spin-coating, followed by curing. The polymerization process is simple and free of byproducts. The cured resins have the characteristics of good heat resistance, low dielectric constant and low hydroscopicity; and the mechanical properties of the cured resins can be regulated by changing siloxane structure.

The invention discloses a cyclobutenone compound with an antioxidant effect and a preparation method thereof, and belongs to the technical field of synthesis of functional organic molecules. Key points of the technical scheme of the invention comprise that the cyclobutenone compound has a structure. The cyclobutenone compound with a novel structure is obtained through efficient competitive [2+2] cycloaddition reaction; antioxidant detection is carried out through a DPPH method to find that the target compound has a good antioxidant effect, so that the compound is expected to be applied to thefields of polyolefin material synthesis and the like, and is used as an oxidant for inhibiting oxidative degradation of the polyolefin material.

The present invention provides methods of making low energy polymerizable monomers and resins for use in making dielectric materials. The methods comprise deprotecting or deacylating an organic alkali cleavable protecting group containing addition polymerizable, amine containing aromatic monomer or oligoaromatic phenol resin containing an organic alkali cleavable protecting group, such as a C2 to C9 alkanoyl group, preferably, an acyl group, by hydrolyzing to remove the protecting group in organic alkali in a polar solvent containing an excess of alkali C1 to C7 alkoxide and form a hydroxyl functional monomer or resin, followed by; reacting via nucleophilic substitution the resulting hydroxyl functional monomer or resin with an alpha-halide (α-halide) or strong acid conjugate leaving group containing arylcyclobutene compound in a polar solvent, to yield a product an arylcyclobutene-containing addition polymerizable or amine containing aromatic monomer or oligoaromatic phenol resin having an ether linkage from the cyclobutene ring to an aromatic group of the addition polymerizable aromatic monomer, aromatic amine or oligoaromatic phenol.

The invention discloses a method for synthesizing a 4-cyclobutyl biphenyl fluorine-containing compound. The method comprises the following steps: by taking chlorine benzene halide as an initial raw material, performing a Grignard reaction; performing a coupling reaction on the chlorine benzene halide with cyclobutanone so as to generate cyclobutanol chlorobenzene; performing a dehydration reactionso as to generate cyclobutene chlorobenzene; performing a one-pot method reaction to generate 4-cyclobutene phenylboronic acid; performing a coupling reaction with fluorine-containing benzene halideso as to generate a 4-cyclobutene biphenyl fluorine-containing compound; performing a hydrogenation reaction, thereby obtaining a 4-cyclobutyl biphenyl fluorine-containing compound IX. The method hasthe characteristics of being high in conversion rate, low in cost, safe and stable in process, short in reaction step, green and environmental-friendly in process route and small in pollutant emission.