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417results about How to "Shape adjustable" patented technology

Method for preparing hollow ball and hollow ball with complex structure by template method

The invention belongs to the field of materials with a hollow structure, in particular to a method for preparing hollow spheres of minerals, metals and organic matters and hollow spheres with compound structures as well as hollow spheres with photic, electrical, magnetic and catalytic properties and hollow spheres with compound structures thereof by taking a polymer hollow sphere as a template. The invention prepares the hollow spheres with compound structures by taking the polymer hollow sphere as the template and combining sol-gel, settlement reaction and redox process through the method of forcing interface or surface settlement, removes the template polymer through high sintering or selective extraction of a solvent to obtain the hollow spheres of minerals, metals and organic matters. The structure and the size of the hollow sphere can be controlled through controlling the reagent activity, the feeding mode, the reagent concentration and a circulation reaction method; besides, compounding of various matters can be realized; the hollow sphere of the invention not only has good dispersing performance, but also has excellent strength and size stability. The invention relates to the application of the materials with a hollow structure.
Owner:INST OF CHEM CHINESE ACAD OF SCI

Method for preparing hollow ball with polymer complex structure by swelling polymerization

The invention belongs to the field of materials with a hollow structure, in particular to a method for preparing hollow spheres of minerals, metals and organic matters and hollow spheres of compound structures as well as hollow spheres with photic, electrical, magnetic and catalytic properties and hollow spheres with compound structures thereof by taking a polymer hollow sphere as a template through a swelling polymerization method. The invention prepares the compound hollow spheres by taking the polymer hollow sphere as a template and combining sol-gel, settlement reaction and redox process through the method of forcing interface or surface settlement, removes the template polymer through high sintering or selective extraction of a solvent to obtain the hollow spheres of minerals, metals and organic matters. The structure and the size of the hollow sphere can be controlled through controlling the reagent activity, the feeding mode, the reagent concentration and a circulation reaction method; besides, compounding of various matters can be realized; the hollow sphere of the invention not only has good dispersing performance, but also has excellent strength and size stability. The invention relates to the application of the materials with a hollow structure.
Owner:BEIJING NEW BUILDING MATERIALS PLC

Method for preparing starfruit-shaped SnO2/C micro-nano particles through electrostatic spinning and prepared product

InactiveCN105668617ANarrow scale distributionUnique shape of the productTin oxidesDimethyl formamideElectrospinning
The invention discloses a method for preparing starfruit-shaped SnO2/C micro-nano particles through electrostatic spinning and a prepared product. The method comprises steps as follows: PVP (polyvinyl pyrrolidone), TBAB (tetrabutylammonium bromide), liquid paraffin and tin salt are dissolved in a mixed solvent of ethanol and DMF (dimethyl formamide) and stirred, and a transparent solution is obtained; the transparent solution is treated with an electrostatic spinning method, precursor fibers are obtained and calcined under the condition of inert gas protection, and the starfruit-shaped SnO2/C micro-nano particles are obtained. The starfruit-shaped SnO2/C micro-nano particles with adjustable sizes are prepared with the combination of a simple electrostatic spinning technology and the heat treatment process under the condition of inert gas protection, the technological process is simple, the synthesis condition is easy to control, the operability is high, the product morphology is unique, the controllability is high, the repeatability is good, the particle size distribution range is narrow, the particle sizes are adjustable, and the method is suitable for industrial production. The obtained starfruit-shaped SnO2/C micro-nano particles have potential application value in the aspects of a supercapacitor, a lithium ion battery and the like.
Owner:UNIV OF JINAN

Single-incision laparoscopic surgery system based on flexible arms

ActiveCN106175851AGuaranteed implementabilityMeet size constraintsSurgical robotsDegrees of freedomSingle incision laparoscopic
The invention relates to a single-incision laparoscopic surgery system based on flexible arms. The single-incision laparoscopic surgery system comprises flexible surgery tools, an imaging tool, a catheter and a driving body. Each flexible surgery tool comprises the first flexible arm, a surgery performer and a first driving transmission unit. The imaging tool comprises the second flexible arm, an imaging lighting module and a second driving transmission unit. The catheter comprises a catheter body and a multi-cavity catheter main body. The driving body comprises a framework linked with the catheter, and a plurality of driving modules connected to the framework in a fastened mode and linked with the first driving transmission units and the second driving transmission unit. The overall feed degrees of freedom, the overall rotation degrees of freedom and the turn degrees of freedom of the first flexible arms are achieved through the driving modules via the first driving transmission units linked with the driving modules, and the overall feed degrees of freedom and the turn degrees of freedom of the second flexible arm are achieved through the driving modules via the second driving transmission unit linked with the driving modules. According to the single-incision laparoscopic surgery system, the flexible surgery tools and the imaging tool can enter the human body through the same multi-cavity catheter main body to perform surgery.
Owner:BEIJING SURGERII TECH CO LTD

Blue-jewel-crystal multi-crucible melt growth technolgoy

ActiveCN101024898AThe structure of the temperature field is stableAdjustable temperature gradientPolycrystalline material growthFrom frozen solutionsFurnace temperatureHearth
The invention provides a multi-pot melt growth technique for growing sapphire crystals, comprising: (1) pretreating aluminum oxide raw material; (2) placing the pretreated aluminum oxide blocks and the oriented seed crystals into pots and moving into high temperature descending furnace, sealing the whole system and power-on to raise temperature, starting mechanical pump and diffusion pump in turn, vacuumizing to 10-3-10-4Pa, and when the furnace temperature up to 1500-1800deg.C, charging inert gas and continuing raising temperature to the set temperature (2100-2250deg.C); (3) when the furnace temperature up to the set temperature, preserving heat for 4-8 hours, regulating hearth temperature and pot positions to smelt raw material and seed crystal top to implement inoculation growth and setting solid-liquid interface temperature gradient at 10-50deg.C/cm and controlling pot descending rate at 0.1-3.0mm/h; and (4) after the crystal growth ends, making in-situ annealing treatment. And the process has features of raw material pretreatment, special temperature field design, multi-pot technique, in-situ annealing treatment, etc, and advantages of stable temperature field, adjustable temperature gradient, operating convenience, low average energy consumption, high yielding by one furnace, and beneficial to industrialized production.
Owner:苏州晶生新材料有限公司

SO3H-SBA-15 molecular sieve catalyst for catalyzing isobutene and carboxylic acid to synthesize carboxylic acid tert-butyl ester and preparation method and application thereof

The invention discloses a SO3H-SBA-15 molecular sieve catalyst for catalyzing isobutene and carboxylic acid to synthesize carboxylic acid tert-butyl ester. The molecular sieve catalyst is prepared by adopting a template agent, a morphology regulator, a silicon source, a sulfonic acid source and an oxidizing agent through a one-step co-condensation method or a two-step sulfonic acid group post-synthesis method. In the SO3H-SBA-15 molecular sieve catalyst, by the molar ratio of a sulfonic acid group to silicon oxide, the sulfonic acid group supporting amount accounts for 30%-50%. The invention further discloses a method of using the SO3H-SBA-15 molecular sieve catalyst to catalyze the isobutene and the carboxylic acid for carboxylic acid tert-butyl ester synthesis. The molecular sieve catalyst is adjustable in shape, orderly in mesoporous pore passage and capable of efficiently and stably catalyzing the isobutene and the carboxylic acid to selectively synthesize the carboxylic acid tert-butyl ester under the conditions of higher temperature and polymerization inhibitor absence, meanwhile the separation energy consumption and equipment investment of reaction products are reduced, and the SO3H-SBA-15 molecular sieve catalyst has an important significance on development and utilization of atomic economic reaction.
Owner:NANJING UNIV OF TECH +1
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