An embodiment of the present application discloses a method for detecting the
lithium intercalation content of a negative
electrode sheet. The detection method does not require the production of a button
cell. After the
battery cell is charged or discharged, the
battery cell is disassembled to take the negative
electrode sheet for XRD testing, avoiding the problem of large deviation in the detection result caused by the loss of material during the
cutting of the negative
electrode sheet for the production of the button
cell. Through the XRD spectrum information, from the LiC6 stage of the negative electrode sheet to the
peak intensity change of the LiC 12 stage, combined with the theoretical specific capacity per
gram of the carbon material, the graphitization degree of the carbon material, and the N / P value of the
battery cell, the actual specific capacity of the carbon material is calculated. The
lithium intercalation content of the negative electrode sheet is calculated based on the actual specific capacity of the carbon material. It is not affected by the polarization during the
charge and discharge of the battery
cell, and the result deviation is within the range of 0-5%. The test method is simple to operate, removing the unstable factors in the button cell test. By utilizing the
phase change that occurs during the
lithium intercalation process of
graphite, the intrinsic change of the
crystal structure is characterized by XRD testing, the test result is more intuitive, the detection accuracy is high, the detection time is short, and the detection efficiency is high.