The invention relates to a
microwave absorption material with a periodic nanometer structure and a preparation method thereof. A wave absorber of the
microwave absorption material with the periodic nanometer structure is filled around the inner walls of holes of a substrate, and the middle parts of the holes of the substrate have hollow structures. The preparation method comprises the following steps: preparing a
sol precursor; and then preparing a porous template with a periodic nano-hole structure, dipping the porous template into
sol precursor solution, performing oil-bath heating to a temperature of between 80 and 160 DEG C for 1 to 5 hours under the protection of
nitrogen, taking out the template for
drying, then annealing at a temperature of between 300 and 800 DEG C for 1 to 20 hours under the protection of the
nitrogen, and finally obtaining the
microwave absorption material with the periodic nanometer structure. The microwave absorption material has the advantages of small density, relatively lighter weight, and relatively better wave-absorbing effectiveness, and has absorption characteristics of narrow frequency and high efficiency.