The invention belongs to the technical field of
sulfur hexafluoride production, and particularly relates to a rectification device for electronic-grade
sulfur hexafluoride and a control method thereof. The rectification device comprises a rectification mechanism and a separation mechanism, wherein the rectification mechanism comprises a first-stage rectification
tower, a second-stage rectification
tower and a third-stage rectification
tower; the first-stage rectification tower, the second-stage rectification tower and the third-stage rectification tower are cylindrical cavity type rectification towers; the middle part of the first-stage rectification tower is fixedly connected with a feeding
pipe; and the feeding
pipe is externally connected with a molding press and a precooler. According to the device, a separation wheel and an
evaporation cavity are arranged, the separation wheel is driven to rotate through
impact of fed materials, then a fluid is divided by an
evaporation cavity, a small part of liquid integrally separated from
sulfur hexafluoride liquid is rapidly evaporated under continuous heat conduction effect, and due to the fact that the content of the liquid in the
evaporation cavity is small, temperature change is obvious, and pure
sulfur hexafluoride liquid is effectively separated by utilizing different boiling points of the liquid.