This invention relates to a aluminium-scandium alloy standard spectrum sample and preparation method, <0}wherein, the sample comprises: Si 0.045~0.27%, Fe 0.07~0.37%, Cu 0~0.11%, Mn 0.13~1.2%, Mg 4.3~7.8%, Cr 0~0.27%, Ni 0~0.11%, Zn 0~0.17%, Sc 0.03~0.54%, Ti 0~0.18%, Zr 0.025~0.22%, Be 0.00005~0.0035% and B 0.0005~0.010%. The preparation relates to smelting, casting, homogenizing, lathing surface, and extruding. This invention meets practical demand, and provides foundation for production of 5A70 and 5A71 series Al-alloy.