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30results about How to "Adjustable content" patented technology

Preparation method of silicon carbide nanowire enhanced C/C-SiC-ZrB2 ceramic-based composite material

The invention relates to a preparation method of a silicon carbide nanowire enhanced C/C-SiC-ZrB2 ceramic-based composite material. A pretreated carbon fiber prefabricating body is thermally treated to obtain a silicon carbide nanowire. The silicon carbide nanowire prepared by a sol-gel carbon-thermal reaction method is evenly distributed at the inner part of a porous carbon/carbon composite material. Subsequently, pyrolytic carbon deposited in an isothermal chemical vapor deposition furnace is coated at the surface of the silicon carbide nanowire, thus the dropping, growing and rupture of the silicon carbide nanowire in the following reaction and infiltration processes are effectively avoided. A ceramic-based composite material carbon fiber, a silicon carbide nanowire and a pyrolytic carbon middle layer after reaction and infiltration are not eroded by a high-temperature metal bath and are well preserved; thus the physical performance of the composite material can be improved. Compared with the C/C-SiC-ZrB2 ceramic-based composite material without adding the silicon carbide nanowire, the bending strength and the fracture toughness property of the silicon carbide nanowire enhanced C/C-SiC-ZrB2 ceramic-based composite material are improved by 26.9-41.3% and 45.2-59.1% respectively.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Method for preparing SSZ-39 molecular sieve by taking fluorine-modified Y-type molecular sieve as raw material

The invention discloses a method for preparing an SSZ-39 molecular sieve by taking a fluorine-modified Y-type molecular sieve as a raw material. The method comprises the following steps: dipping a Y-type molecular sieve in a fluorine-containing aqueous solution, and drying and roasting the Y-type molecular sieve to obtain a fluorine-doped Y-type molecular sieve; mixing and stirring deionized water, an alkali source, a template agent and a silicon source well in proportion, and adding the fluorine-doped Y-type molecular sieve to prepare sol; and transferring the sol into a crystallization kettle, filtering, washing and drying the crystallization product after complete crystallization, carrying out ion exchange, and carrying out roasting to obtain a hydrogen type SSZ-39 molecular sieve. According to the invention, the Y-type molecular sieve raw material is modified by a fluorine doping method, so that the SSZ-39 molecular sieve can be prepared by complete crystal transformation in a short time under the condition of relatively low silica-alumina ratio, and the raw material and production costs can be obviously reduced. The SSZ-39 molecular sieve prepared by the method has the characteristics of short crystallization time, high crystallinity, controllable grain size, good grain dispersity and the like, and can be applied to the fields of methanol-to-olefin reaction, carriers of selective catalytic reduction catalysts and the like.
Owner:CHINA CATALYST HLDG CO LTD

Micro-needle capable of being rapidly dissolved based on water-soluble small molecules as well as preparation and application of micro-needle

The invention belongs to the technical field of drug administration appliances and discloses a micro-needle capable of being rapidly dissolved based on water-soluble small molecules as well as a preparation and application of the micro-needle. The preparation method specifically comprises the following steps: firstly, taking a water-soluble small molecular material as a solute to prepare a small molecular water solution; then loading the small molecular water solution into a micro-needle mould; drying and de-molding so as to obtain the micro-needle capable of being rapidly dissolved based on the small molecules. According to the preparation method provided by the invention, a whole technological flow design and conditions and parameters (such as small molecule types and the concentration of water solutions of the small molecules) of each step are improved, so that the small molecular water-soluble micro-needle with an extremely rapid dissolving speed and good mechanical properties canbe prepared; compared with the prior art, the problems of a current high molecular water-soluble micro-needle that the time of a preparation process is long, the dissolving speed of the micro-needle is slow and the like can be effectively solved.
Owner:武汉楚颜生物科技有限公司

Steric compound crystal controlled polylactic acid/hydrogenated polybutadiene supermolecular elastomer

The invention relates to the technology of macromolecular thermoplastic elastomers, and aims to provide a steric compound crystal controlled polylactic acid/hydrogenated polybutadiene supermolecular elastomer. The product is composed of two compounds which are UPy-PLLA-PEB-PLLA-UPy and UPy-PDLA-PEB-PDLA-UPy respectively; in the UPy-PLLA-PEB-PLLA-UPy, chiral carbon in a PLLA block is of a left-handed structure; in the UPy-PDLA-PEB-PDLA-UPy, chiral carbon in a PDLA block is of a right-handed structure; and in the two compounds, the UPy-PLLA-PEB-PLLA-UPy occupies 10% to 90%, and the UPy-PDLA-PEB-PDLA-UPy occupies 90% to 10%. The UPy bonded PLA/PEB supermolecular polymer elastomer is prepared by adopting steric compound crystallized PLLA/PDLA as a hard area and PEB as a soft segment, and the hard segment of the obtained elastomer can be crystallized, and the elastomer is high in melting point, strength and modulus; the content of steric compound crystal can be adjusted by changing the mixed proportion of the two compound, so that the strength, modulus and heat resistance of the elastomer are convenient to control; and by adopting the biology base and biology degradable PLLA and PDLA as the hard segment of the supermolecular elastomer, the pollution generated to the environment is little, the elastomer is green and environment-friendly, and the resources are saved.
Owner:ZHEJIANG UNIV

System device and method for synchronously realizing organic waste disposal and synthesis gas quality improvement

ActiveCN105645581AAchieve anaerobic digestionAchieve gas upgradingGaseous fuelsWaste based fuelSyngasMethanation
The invention discloses a system device and a method for synchronously realizing organic waste disposal and synthesis gas quality improvement. A core part of the system device is an anaerobic synthesis integrated reactor, wherein the anaerobic synthesis integrated reactor sequentially comprises a sludge discharge area, an aeration buffer area, a gas liquid mixing area, a microbial synthesis reaction area, a gas solid liquid separation area and a gas phase pressure stabilizing area from bottom to top. By adopting the system device, organic waste disposal and recycling production of methane in the anaerobic synthesis integrated reactor can be realized, and methanation quality improvement of synthesis gas also can be realized simultaneously. Compared with the prior art, the system device and the method have the advantages that by adopting a microbial technology, while the synthesis gas is led into the anaerobic synthesis integrated reactor to dispose organic waste, gas quality improvement and purification are realized, under normal temperature and normal pressure, most components, except methane, in the synthesis gas can be converted into methane, and a new method is provided for solving the problems of resource shortage, environment pollution, unreasonable energy structure, and the like in the energy field in China.
Owner:BEIJING UNIV OF CHEM TECH +1

A method for preparing SSZ-39 molecular sieve using fluorine-modified Y-type molecular sieve as raw material

The invention discloses a method for preparing SSZ‑39 molecular sieves by using fluorine-modified Y-type molecular sieves as raw materials. Y-type molecular sieve is impregnated with fluorine-containing aqueous solution, dried, and roasted to obtain fluorine-doped Y-type molecular sieve; mix and stir deionized water, alkali source, template agent, and silicon source according to the ratio, and add the above-mentioned fluorine-doped Y-type molecular sieve. Sol: transfer the sol to a crystallization kettle, after the crystallization is complete, the crystallized product is filtered, washed, dried, ion-exchanged, and then roasted to prepare a hydrogen-type SSZ‑39 molecular sieve. The present invention modifies the raw material of Y-type molecular sieve by fluorine doping method, so that it can completely transform crystal to prepare SSZ-39 molecular sieve in a relatively short period of time under the condition of relatively low silicon-aluminum ratio, so that the raw material and Cost of production. The SSZ-39 molecular sieve prepared by the invention has the characteristics of short crystallization time, high crystallinity, controllable grain size, good grain dispersion, etc., and can be applied to the fields of methanol-to-olefin reaction, carrier of selective catalytic reduction catalyst, and the like.
Owner:CHINA CATALYST HLDG CO LTD

A silicon carbide nanowire reinforced c/c-sic-zrb 2 Preparation method of ceramic matrix composite material

The invention relates to a preparation method of a silicon carbide nanowire enhanced C / C-SiC-ZrB2 ceramic-based composite material. A pretreated carbon fiber prefabricating body is thermally treated to obtain a silicon carbide nanowire. The silicon carbide nanowire prepared by a sol-gel carbon-thermal reaction method is evenly distributed at the inner part of a porous carbon / carbon composite material. Subsequently, pyrolytic carbon deposited in an isothermal chemical vapor deposition furnace is coated at the surface of the silicon carbide nanowire, thus the dropping, growing and rupture of the silicon carbide nanowire in the following reaction and infiltration processes are effectively avoided. A ceramic-based composite material carbon fiber, a silicon carbide nanowire and a pyrolytic carbon middle layer after reaction and infiltration are not eroded by a high-temperature metal bath and are well preserved; thus the physical performance of the composite material can be improved. Compared with the C / C-SiC-ZrB2 ceramic-based composite material without adding the silicon carbide nanowire, the bending strength and the fracture toughness property of the silicon carbide nanowire enhanced C / C-SiC-ZrB2 ceramic-based composite material are improved by 26.9-41.3% and 45.2-59.1% respectively.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Method for adjusting and controlling structure and shape of calcium oxalate crystals by using colibacillus secretion

The invention relates to a method for adjusting and controlling the structure and shape of calcium oxalate crystals by using colibacillus secretion. The method comprises the following steps of: mixing the colibacillus secretion with a matrix solution of which the ratio of [Ca2<+>] to [C2O4<2->] is (19.5-20.5):1, wherein the volume ratio is 1:(8-80); performing constant temperature incubation, and staying overnight; and washing and drying to obtain pure acalculous type calcium oxalate dehydrate crystals or a mixture of the calcium oxalate dehydrate crystals and calcium oxalate monohydrate crystals, wherein the colibacillus secretion is prepared through the steps of inoculating TOP10 single colonies of colibacillus to an LB liquid culture medium, performing low-speed oscillation on the culture medium at a constant temperature, staying the culture medium overnight, and performing high-speed centrifugation on the original bacterium liquid to obtain the colibacillus secretion. The method has the advantages that the calcium oxalate dehydrate crystals formed through colibacillus secretion adjustment and control have the characteristics of uniform size and consistent shape, the content of the calcium oxalate dehydrate crystals can be adjusted according to different additions, and the preparation condition is simple and non-hazardous, so that the method can be widely used in various fields.
Owner:TONGJI UNIV

A kind of purification method and device of graphene oxide/graphene solution

The invention discloses a method and a device for purifying an oxidized graphene / graphene solution. The method comprises the following steps: pumping the oxidized graphene / graphene solution to be purified into a channel consisting of at least one filtering and discharging pipe, arranging the at least one filtering and discharging pipe between at least one group of negative and positive electrodes of an electrolytic tank, and forming auxiliary liquid channels between the negative and positive electrodes and the at least one filtering and discharging pipe; performing electrode migration on ions and charged particles in the oxidized graphene / graphene solution to be purified under the action of an electrical field between the negative and positive electrodes, filtering impurities out of the filtering and discharging pipes, taking away the impurities by auxiliary liquid, and pumping the residual purified oxidized graphene / graphene solution into another water tank from the at least one filtering and discharging pipe to form filtering circulation. According to the method and the device, the process is simple, the cost is low, the speed that the impurities are filtered out of the at least one filtering and discharging pipe can be increased, efficient purification of the oxidized graphene / graphene solution is realized, and the method is very suitable for industrial production.
Owner:CHANGSHA SAIWEI ENERGY TECH

A system device and method for synchronously realizing organic waste treatment and syngas upgrading

ActiveCN105645581BRealize in-situ upgrading and purificationAddress resource shortagesGaseous fuelsWaste based fuelGas solidSyngas
The invention discloses a system device and a method for synchronously realizing organic waste disposal and synthesis gas quality improvement. A core part of the system device is an anaerobic synthesis integrated reactor, wherein the anaerobic synthesis integrated reactor sequentially comprises a sludge discharge area, an aeration buffer area, a gas liquid mixing area, a microbial synthesis reaction area, a gas solid liquid separation area and a gas phase pressure stabilizing area from bottom to top. By adopting the system device, organic waste disposal and recycling production of methane in the anaerobic synthesis integrated reactor can be realized, and methanation quality improvement of synthesis gas also can be realized simultaneously. Compared with the prior art, the system device and the method have the advantages that by adopting a microbial technology, while the synthesis gas is led into the anaerobic synthesis integrated reactor to dispose organic waste, gas quality improvement and purification are realized, under normal temperature and normal pressure, most components, except methane, in the synthesis gas can be converted into methane, and a new method is provided for solving the problems of resource shortage, environment pollution, unreasonable energy structure, and the like in the energy field in China.
Owner:BEIJING UNIV OF CHEM TECH +1
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