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61results about How to "Avoid supplements" patented technology

Weight-losing nutrition bar and preparation method thereof

The invention provides a weight-losing food with balanced nutrition, containing the following components of: soybean isolate protein expanded grains, maltitol liquid, water-soluble dietary fiber, concentrated lactalbumin, glycerol, fish collagen protein, phytosterol, quick-freezing blueberry grains, Arabic gum, sodium caseinate and compound vitamin. The weight-losing bar has the advantages of good taste and high protein content; the weight-losing food bar can enhance the satiety and also can supplement the protein; and meanwhile, functional food raw materials including the fish collagen protein, the phytosterol and the like, the compound vitamin and the like are added, so as to achieve the aim of healthily losing the weight of a consumer.
Owner:浙江诺特健康科技股份有限公司

Automatic medicine packaging machine with door lock unit

An automatic medicine packaging machine with door lock unit that prevents the supplement and outflow of tablets by an unauthorized person and makes tablets kept and treated more safely is disclosed. The automatic medicine packaging machine comprising a plurality of tablet cassettes and a door includes; a door lock unit that is established on a body of the automatic medicine packaging machine and locks or unlocks the door; a button operation unit that is established on the front of the body and that operation is inputted by a user; and a lock controller that controls the operation of the door lock unit according to a lock or unlock signal inputted by the button operation unit, in which the lock controller includes a user authentication unit that authenticates user of the door lock unit.
Owner:JVM CO LTD

Helium cooling magnetic resonance superconducting magnet

The invention discloses a helium cooling magnetic resonance superconducting magnet which comprises a vacuum vessel, an accommodating cavity used for arranging a cryogenic vessel is formed inside the vacuum vessel, and a cold shield which is used for reducing radiation heat leakage of room temperature to the cryogenic vessel is further arranged in the accommodating cavity; a superconducting coil is arranged in the cryogenic vessel; a refrigerating machine is fixed on the vacuum vessel; a first stage cold head of the refrigerating machine is connected with the cold shield, a second stage cold head of the refrigerating machine is located in the cryogenic vessel, the helium cooling magnetic resonance superconducting magnet further comprises a helium gas pipe which is used for filling gaseous helium into the cryogenic vessel, the helium gas pipe comprises a stretching end which stretches out of the vacuum vessel, and a sealing ball valve which is used for preventing gaseous helium leaking when the helium cooling magnetic resonance superconducting magnet operates or the superconducting coil is invalid. The gaseous helium in the cryogenic vessel is specifically gaseous helium with 1-10 atmospheric pressure in room temperature. According to the helium cooling magnetic resonance superconducting magnet, the helium gas utilization ratio can be improved, and the maintenance process of the superconducting magnet can be simplified.
Owner:NINGBO JANSEN SUPERCONDUCTING TECH CO LTD

Microbiological incubator

The invention discloses a microbiological incubator. A first motor is fixedly mounted at the bottom of a box body by a motor mounting seat, and a rotary disc is fixedly arranged at an output end of the first motor; a culture vessel mounting seat is fixedly arranged on the surface of the rotary disc; a hydraulic cylinder I is fixedly arranged in the center of a supporting plate; a baffle is weldedon each of the two sides of the supporting plate; a rotary shaft is fixedly connected at the other end of each of the baffles; a first tong arm and a second tong arm are symmetrically arranged on therotary shaft; the first tong arm and the second tong arm are fixed on the rotary shaft by shaft sleeves; an arc-shaped clamping plate is arranged at the corresponding ends of the first tong arm and the second tong arm respectively; a connecting rod is connected at the other corresponding ends of the first tong arm and the second tong arm respectively in an articulation manner; the other ends of the connecting rods are welded on a piston rod of the hydraulic cylinder I.
Owner:浙江品创知识产权服务有限公司

Calcium supplement health food and preparation method thereof

The invention relates to a calcium supplement health food and a preparation method thereof. Primary raw materials of the calcium supplement health food comprise 10-20wt% of a calcium-containing compound, 10-30wt% of , 5-20wt% of an edible fungus extract, 5-20wt% of a tremella extract, 5-20wt% of pearl powder and 0.1-0.5wt% of vitamin D3, and 0-35wt% of auxiliary materials allowed in health foods can be added in the health food to prepare a tablet, a soft capsule, a capsule or a granule, wherein the calcium-containing compound is one of or a combination containing above two of calcium citrate malate, calcium lactate, L-calcium aspartate, calcium gluconate and calcium citrate. The calcium supplement health food has the advantages of natural components, scientific burdening, safety, no toxic side effect, high calcium content and high bioavailability, and is a good novel calcium supplement agent.
Owner:WEIHAI BAIHE BIOTECH

Energy cable having a crosslinked electrically insulating layer, and method for extracting crosslinking by-products therefrom

An energy cable includes, at least one cable core including an electric conductor, a crosslinked electrically insulating layer, and zeolite particles placed in the cable core. The zeolite particles are able to extract and absorb, very efficiently and irreversibly, the by-products deriving from the cross-linking reaction, so as to avoid space charge accumulation in the insulating material during cable lifespan. A method for extracting crosslinking by-products from a cross-linked electrically insulating layer of an energy cable core, which includes manufacturing the energy cable core containing zeolite particles, heating the energy cable core up to a temperature causing migration of the crosslinking by-products from the crosslinked electrically insulating layer; and then placing a metal screen around the energy cable core.
Owner:PRYSMIAN SPA

Vacuum drying oven

The invention relates to the technical field of displaying, and discloses a vacuum drying oven. The vacuum drying oven is used for drying an ink-jet printing device. The vacuum drying oven comprises acavity, a hot plate, a solvent trough and a cold plate, wherein an exhaust port is formed in the top of the cavity, the hot plate is arranged in the cavity, a bearing face used for placing the ink-jet printing device is formed on the surface, facing the exhaust port, of the hot plate, the solvent trough is arranged on the periphery of the hot plate, the temperature of the solvent trough can be independently controlled, solvent trough openings used for diffusing a solvent are formed in the surface of the side, facing the exhaust port, of the solvent trough, and the cold plate is arranged in the cavity and located between the hot plate and the exhaust port. According to the vacuum drying oven, parts on the surface of the ink-jet printing device are evenly dried by creating the same atmosphere on the surface of the ink-jet printing device which is placed in the vacuum drying oven.
Owner:BOE TECH GRP CO LTD

Method for separating MEOH-DMC (methanol-dimethyl carbonate) through vapor permeation

The invention discloses a method for separating MEOH-DMC (methanol-dimethyl carbonate) through vapor permeation, which belongs to the technical field of separation of methanol-dimethyl carbonate. The method comprises the following steps: firstly, with Na2O.n, SiO2, Al (OH)3 and Zn (OH) 2 as raw materials and a porous a-Al2O3 supporting membrane tube or a porous mullite membrane tube as a supporting membrane tube, preparing a NaY-Zn molecular sieve membrane through hydrothermal synthesis, and then, conveying MEOH-DMC saturated mixed vapor with temperature of 121-140 DEG C and pressure of 0.63-1.08 Mpa into a molecular sieve membrane separator equipped with the NaY-Zn molecular sieve membrane, and maintaining the vacuum absolute pressure of the permeation side of the molecular sieve membrane separator to 28-95 Kpa through a vacuumizing method, wherein the MEOH in the mixed vapor preferentially permeates through the molecular sieve membrane to be enriched on the permeation side of the membrane and is condensed into liquid under low vacuum degree, and the mixed vapor on the retentate side is further separated by multiple levels of serially connected molecular sieve membrane separators. The method disclosed by the invention can be used for effectively improving the separating performance of the MEOH-DMC and has the advantages of small investment, low operation cost and the like.
Owner:BEIJING ZHONGHUA DINGSHENG ENERGY SAVING TECH

Repetitive pulse high-intensity magnetic field generation device and method

The invention provides a repetitive pulse high-intensity magnetic field generation device and method, and belongs to the field of high-intensity magnetic fields. The device comprises a magnet coil anda plurality of independent power supply units, wherein the plurality of independent power supply units are connected to the two ends of the magnet coil in parallel; each power supply unit comprises an energy supply element, a follow current loop and an electrical switch, wherein the follow current loop is connected with the energy supply element in parallel and then is connected with the electrical switch in series, and the follow current loop comprises a follow current resistor and a one-way conduction element which are connected in series with each other. According to the invention, a scheme that multiple sets of power supplies discharge to a single magnet is adopted, a repeated pulse strong magnetic field can be generated by controlling the connection mode of multiple power supply units and the magnet coil and the discharge time sequence of the electrical switch, and the advantages of simple circuit topology and control system, diversified magnetic field waveforms and random controllable magnetic field polarity, magnetic field intensity and repetition frequency are achieved.
Owner:HUAZHONG UNIV OF SCI & TECH

Selenium-rich tea planting method

The invention relates to the field of tea planting, in particular to a selenium-rich tea planting method. The method comprises the following steps of treating a cultivated land, planting, topdressing,spraying a nutrient solution and preventing and curing diseases; by a series of operations, the selenium content of the planted tea is high, the selenium content in 500g of tea can reach more than 30micrograms, the method can improve the tea planting environment, change the selenium content of the soil, adjust the fertilizer structure of the tea, except that nutritional requirements of tea are met, the tea can be effectively replenished with organic selenium and inorganic selenium, the selenium content of the tea is effectively improved, when a sea seedling is replenished with selenium, thesupplementation of chemical synthesized selenium is avoided, the tea can absorb the selenium more effectively, on the other hand, the tea can supply natural selenium to the tea, guarantee the safety,improve the quality of the tea, and meet a great demand for the selenium-rich tea.
Owner:松桃鑫山农业科技开发有限公司

Method for preparing hydrocarbon fuel from grease raw materials

The invention relates to a method for preparing hydrocarbon fuel from grease raw materials. The method comprises the steps: performing a reaction through contact of the grease raw materials with a hydrogenation catalyst, performing separation on hydrogenation reaction effluents so as to obtain liquid hydrocarbon, water and gas matter, performing a reaction through contact of the liquid hydrocarbonwith a hydroisomerization catalyst, and performing separation and fractionation on hydroisomerization reaction effluents so as to obtain a diesel fraction and a naphtha fraction. The prepared dieselfraction contains no sulfur, has a low freezing point and a high cetane number, and is a high-quality diesel product and a diesel cetane number additive.
Owner:CHINA PETROLEUM & CHEM CORP +1

Scrubber integrated system capable of circularly filtering and recycling sewage

ActiveCN113440076AHigh circulation filtration efficiencyImprove filtering effectCarpet cleanersFloor cleanersWater flowSewage
The invention discloses a scrubber integrated system capable of circularly filtering and recycling sewage. The scrubber integrated system is characterized by comprising a shell, a roller assembly, a dust collection assembly, a water tank and a water circulation assembly are arranged in the shell, the roller assembly is arranged at the front end of the shell and used for sweeping garbage and collecting the garbage into the dust collection assembly, the water tank abuts against the roller assembly, a closed cavity for water to pass through is formed between the water tank and the roller assembly and communicated with the water circulation assembly through a liquid inlet pipeline and a liquid outlet pipeline, and the water circulation assembly can drive water to flow through the closed cavity, sewage flowing out of the liquid outlet pipeline enters the water circulation assembly to be purified and then flows into the closed cavity through the liquid inlet pipeline to achieve water circulation utilization. The system has the advantages of being exquisite in structure, capable of achieving product miniaturization, good in cleaning effect, good in use experience, low in production and manufacturing cost and beneficial to saving water, and the market application prospect is good.
Owner:GUANGDONG YUNHAN INTELLIGENT TECH CO LTD

Mud cyclic purification system and mud purification method during drilling

The invention discloses a mud cyclic purification system during drilling and a mud purification method thereof. The mud cyclic purification system is characterized in that a swirler (7) comprises a cylinder body (7.1), an inverted cone body (7.2) and an inverted cone hopper (7.3); a sand outlet (7.5) in the bottom of the inverted cone body (7.2) is in threaded connection with the inverted cone hopper (7.3) through an upper flange plate (8) and a lower flange plate (9); a sand outlet pipe (19) is fixed to the bottom end of the inverted cone hopper (7.3) of the swirler (7); and a first flow regulating valve (20) is arranged on the sand outlet pipe (19). The method comprises the key steps that mud in the swirler (7) is classified under the action of centrifugal force; and most drilling slags are thrown to the cylinder wall of a working cylinder, and rotate downwards to pass through the sand outlet (7.5), the inverted cone hopper (7.3) and the sand outlet pipe (19) to be completely discharged from the mud circulation. According to the purification system and the purification method, the energy consumption can be reduced, and the hole cleaning and deslagging efficiency is improved.
Owner:NINGBO ETONE CONSTR CO LTD

Power electrical cabinet

The invention belongs to the technical field of electrical cabinets, and particularly relates to a power electrical cabinet. The cabinet comprises a cabinet body and a cabinet door; the cabinet door is mounted on the cabinet body, and a handle is arranged on the cabinet door; a mounting cavity is formed in the cabinet body; a plurality of placing plates are fixedly mounted in the mounting cavity;an electrical element is fixedly mounted on the placing plate; a heat dissipation pipe is fixedly installed on the upper surface of the cabinet body; a storage cavity is formed in the cabinet body; the storage cavity is located above the mounting cavity; a heptafluoropropane fire extinguishing agent is compressed and stored in the storage cavity; the storage cavity is communicated with the mounting cavity through a switch module; after the temperature borne by the switch module exceeds a certain limit, the switch module is automatically started to communicate the mounting cavity with the storage cavity. The cabinet is simple in structure, dust can be effectively prevented from entering the cabinet body, meanwhile, when a fire occurs in the cabinet body, a channel for outside air to enter the cabinet body can be blocked, and oxygen supply of an ignition point in the cabinet body is blocked.
Owner:左建军

Synchronous biochemical advanced oxidation liquid waste treatment method and device

The invention discloses a synchronous biochemical advanced oxidation liquid waste treatment method and device. The device comprises a biological reaction tower and a gas dissolution pump. The gas dissolution pump is communicated with a water suction pipe on the top of the biological reaction tower and a through hole water pipe at the bottom of the biological reaction tower. The gas dissolution pump is used for pumping liquid waste from a water collection pool into the biological reaction tower to drive water circulation inside the tower. Two packing layers are arranged inside the biological reaction tower, wherein granular catalysis biological packing is placed on the upper layer, and suspension packing is placed on the lower layer. The granular catalysis biological packing is placed in the middle of the biological reaction tower, the water through water pipe is arranged at the bottom of the tower, and an ultrasonic transducer amplitude-change pole is placed above the biological reaction tower; the processing capacity is high, organic loads are high, the processing effect is 2-3 times higher than that of processing technologies of the same kind, the device has the advantages of being low in investment, small in occupied land and the like, the advanced oxidation technology, the ultrasonic decomposition technology and microbiological degradation technology are integrated, and the device has the advantages of being easy and convenient to operate and maintain, high in purification efficiency, low in investment and operation cost and the like, and is particularly applicable to processing organic liquid waste hard to degrade on the condition of intensified land occupation.
Owner:东莞市环境科学研究所 +1

Full-automatic multi-layer board double machine production line

The invention discloses a full-automatic multi-layer board double machine production line. The full-automatic multi-layer board double machine production line comprises a single board I vertical splicing and horizontal splicing mechanism, a finished product viewing angle detection mechanism, a single board I defective product separation mechanism, a 90-degree steering mechanism III, a single boardII vertical splicing mechanism, a 90-degree steering assembly mechanism, a single board II horizontal splicing mechanism, a 90-degree steering mechanism IV, a single board II defective product separation mechanism, a single board automatic gluing mechanism, a glue board assembly mechanism, a stacking mechanism, an automatic conveying mechanism and a full-automatic cold pressing mechanism. According to the full-automatic multi-layer board double machine production line, the flow line production from single board finishing to assembly cold pressing is achieved, a traditional production technology process of a multi-layer board is greatly simplified, intermediate links are reduced to achieve the flow production, the product quality of single board production is improved, the problems of cavity, sticking, color difference and the like existing in single board production are solved, meanwhile the needs of assembly speed can be met, the supplement amount of a supplement mechanism is avoided, the intermediate conveying link is greatly reduced, and the working efficiency is improved.
Owner:山东昶兴智能科技有限公司

Method and device for detecting content of carbon tetrafluoride in electrical equipment

The invention discloses a device for detecting the content of carbon tetrafluoride in electrical equipment. The device comprises a first pipeline, a second pipeline, a third pipeline, a first valve, asecond valve, a third valve, a carbon tetrafluoride detector, a gas storage tank and a compressor, wherein the first pipeline is connected with the electrical equipment and used for forming a ventilating gas line; the second pipeline is connected with the first pipeline and used for forming a measuring gas line; the two ends of the third pipeline are connected with the second pipeline separatelyto form a recharge gas line; the first valve is arranged on the first pipeline; the second valve is arranged on the second pipeline; the third valve is arranged on the third pipeline; the carbon tetrafluoride detector is arranged on the second pipeline and used for detecting the content of carbon tetrafluoride in the measuring gas line; the gas storage tank is arranged on the second pipeline and used for storing a gas sample detected by the carbon tetrafluoride detector; the compressor is arranged on the second pipeline, connected with the gas storage tank and used for recharging the gas sample in the gas storage tank into the electrical equipment. The device is used for accurately detecting the content of carbon tetrafluoride in the electrical equipment with environmental friendliness. The invention further discloses a method for detecting the content of carbon tetrafluoride in the electrical equipment.
Owner:STATE GRID CHONGQING ELECTRIC POWER CO ELECTRIC POWER RES INST +2

Medicine loading device and medicine recovery method

The present invention provides a medicine loading device that, on the basis of prescription information, can prevent the wrong medicine from being loaded. This medicine loading device includes a body,a medicine dispensing cassette, and a means for identifying medicines. The medicine dispensing cassette comprises a lid that can be opened / closed, and a lock mechanism for locking the lid. The lock mechanism is released when the type of the medicine, as detected by the means for identifying medicines, matches the type of medicine stored in the medicine dispensing cassette.
Owner:YUYAMA MFG CO LTD

Method for controlling gushing in advancing process of shield tunneling machine

The invention provides a method for controlling gushing in the advancing process of a shield tunneling machine. The method comprises the steps that under the situation that the shield tunneling machine conducts advancing to the position at a first preset distance from a river, and high-molecular polymers are added into a soil bin of the shield tunneling machine; a migration riverway is excavated in the position, at a second preset distance from the river, in the large mileage direction of an advancing route of the shield tunneling machine; a water-intercepting dam is constructed at the upstream position of the river, a water-retaining wall is constructed at the downstream position of the river, and thus a river-closure riverway is determined; river water in the river is diverted to flow tothe migration riverway; riverway hardening construction is conducted on the river-closure riverway; precipitation wells are driven on the two sides of the position, between the shield tunneling machine and the river-closure riverway, of the advancing route; and after the shield tunneling machine passes through the part below the river-closure riverway, the water-intercepting dam and the water-retaining wall are dismantled so as to enable the river water in the riverway to flow back to the river-closure riverway. Through the method, the gushing phenomenon occurs when the shield tunneling machine downwards passes through the river can be effectively prevented, ground surface subsidence caused by gushing is avoided, the construction progress is ensured, and the safety risk is avoided effectively.
Owner:CHINA RAILWAY 12TH BUREAU GRP +1

Sewage circulating filtration system

The invention discloses a sewage circulating filtration system. The system comprises a sewage tank, a clear water tank, a pump assembly and a filtering device, a purification filter element is arranged in the clear water tank, the purification filter element is of a hollow structure, and a cavity is formed in the purification filter element; the pump assembly can form negative pressure in the sewage tank so as to pump sewage in the sewage tank into the cavity of the purification filter element after passing through the filter device; a flocculating agent is contained in the cavity and is used for polymerizing impurities in the sewage into granular aggregates and settling the granular aggregates in the cavity; the pump assembly can form positive pressure in the cavity, so that the polymerized and settled sewage is filtered by the filter element and then is pressed out of the water purification tank for recycling. The sewage circulating filtration system is good in cleaning effect, low in production and manufacturing cost, convenient and flexible to use, favorable for saving water and good in market popularization prospect.
Owner:GUANGDONG YUNHAN INTELLIGENT TECH CO LTD

Energy saving and environment friendly street lamp

The invention discloses an energy-saving and environment-friendly street lamp, which comprises a waterproof base, an electric control box, a light box, etc., the upper end of the waterproof base is provided with an electric control box, and the upper end of the electric control box is provided with a light box. A through hole is opened in the center of the plate body at the connecting part of the control box, the lower end of the lifting rod passes through the through hole to connect with the electric control box, and the energy-saving bulb is installed on the bottom of the lifting rod through the rotating shaft. At the upper end, the rear end of the energy-saving bulb is fixed with a lampshade, the top of the arc-shaped plate is provided with a solar panel, the bottom of the arc-shaped plate is provided with two symmetrical connection protrusions, and the top of the light box is provided with There is a connection block corresponding to the connection protrusion, and the connection protrusion and the connection block are hinged together, so that the arc-shaped plate can rotate at the hinge point as the center of a circle. The energy-saving and environment-friendly street lamp of the present invention has the characteristics of obvious energy-saving effect, convenient use and long service life.
Owner:TIANJIN BANGHENG TECH

Automotive, automatic transmission and hybrid hydraulic control systems

ActiveCN103277505BSmall volumeRealize the function of pre-gear at startGearing controlSlow-startAutomatic transmission
The invention discloses an automobile, an automatic transmission and a hybrid power hydraulic control system. The hybrid power hydraulic control system comprises a first reversing valve, a second reversing valve and a third reversing valve. The first reversing valve is provided with a first valve port, a second valve port, a third valve port, a fourth valve port, a fifth valve port and a sixth valve port. The second reversing valve is provided with a first connector, a second connector, a third connector, a fourth connector and a fifth connector. The second valve port is suitable for being communicated with a cooling lubricant passage of the hydraulic control system, the third valve port is respectively connected with the third connector and the third reversing valve, the fourth valve port is respectively connected with the third connector and the third reversing valve, the fourth connector is suitable for being connected with the cooling lubricant passage, and the fifth port is suitable for being connected with a shift executing component of the automatic transmission. A main oil pump is respectively connected with the first connector, the second connector and the third reversing valve. An auxiliary oil pump is respectively connected with the first valve port and the sixth valve port. An energy accumulator is connected with the fifth valve port, and a driving device is used for driving the auxiliary oil pump to work. The hybrid power hydraulic control system is simple in structure, easy to control, and capable of effectively solving the problem of slow start of the automobile.
Owner:HYCET TRANSMISSION TECH HEBEI CO LTD

Passive underwater navigation communication positioning system and method

The invention relates to a passive underwater navigation communication positioning system and method. The passive underwater navigation communication positioning system comprises a passive probe unitand a data communication label unit. The passive probe unit comprises a sensitive element, an energy storage element and a power amplifier; the data communication label unit comprises a data processorand a storage element. The sensitive element, the data processor and the power amplifier are connected with one another, and the storage element is connected with the data processor; and the energy storage element is used for providing power for the power amplifier, the data processor and the storage element. The distance between the underwater vehicle and each passive underwater navigation communication positioning system and the position information of each system are combined and thus the actual position of the underwater vehicle can be calculated, so that a problem that the absolute coordinates of the underwater vehicle deviate and cannot be corrected in time after long-time navigation due to accumulated errors, ocean current or crustal movement and other factors can be solved.
Owner:HARBIN ENG UNIV

Treatment method of cellulose acetate butyrate production wastewater

The invention belongs to the field of wastewater treatment, and in particular relates to a treatment method for wastewater produced from cellulose acetate butyrate. The technical problem to be solved by the invention is that the existing treatment process is complex, the operation cost is high, and the amount of sludge is large. The solution of the present invention to solve the above-mentioned technical problems is to provide a treatment method for cellulose acetate butyrate production wastewater, comprising the following steps: 1) the cellulose acetate butyrate production wastewater first enters the adjustment tank for treatment for 12-16 hours, and then enters the immobilized photosynthesis Bacteria pool treatment for 46-52 hours; 2) The effluent from the immobilized photosynthetic bacteria pool enters the first settling tank for 2-3 hours; 3) The supernatant after the first settling tank settles flows into the anoxic tank for 20-28 hours; 4) The anoxic tank The treated effluent enters the aerobic tank for 20-28 hours; 5) The effluent treated in the aerobic tank enters the secondary sedimentation tank for 2-3 hours, and then the supernatant enters the discharge port for discharge or recycling. The method of the invention has good treatment effect, low operation cost, and can discharge up to the standard stably.
Owner:SICHUAN NITROCELLULOSE CORP +1

A kind of preparation method of perfluorocyclohexyl fluoride

The invention discloses a preparation method of perfluorocyclohexylformyl fluoride. (a) by volume, 5-6 parts of electrolyte, 15-16 parts of anhydrous hydrofluoric acid and 2-3 parts of solubilizer are put into the Reaction kettle, under the conditions of temperature 10-25°C and pressure 0.05-0.15MPa, react for 1-5 hours to obtain the electrolytic configuration solution, which is ready for use; (b) continuously add the electrolytic configuration solution obtained in step (a) to the circulation tank , and then fed into the electrolytic cell through a circulating pump, and the electrolytic fluorination reaction is carried out at a temperature of 15-35 °C under normal pressure. The gas phase product obtained by electrolysis enters the product condenser through the pipeline, and the liquid phase condensed by the product condenser enters the product separator for stratification. The upper inorganic phase is hydrogen fluoride, which is sent to the circulation tank to participate in the electrolytic fluorination reaction again. The lower inorganic phase After filtration and rectification, the product of perfluorocyclohexylformyl fluoride is obtained. The invention has the advantages of simple process, long operation period, stable product quality, energy saving and environmental protection.
Owner:ZHEJIANG JUSHENG FLUOROCHEM
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