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43results about How to "Facilitate redispersion" patented technology

Preparation method of highly-dispersed copper-zinc catalyst for carbon dioxide reduction and use method thereof

The invention provides a preparation method of a highly-dispersed copper-zinc catalyst for carbon dioxide reduction and a use method thereof. The preparation method comprises the steps of firstly, synthesizing a copper oxide nano-particle precursor with uniform particle sizes; then preparing a ZIF (Zeolitic Imidazolate Framework)-8 MOFs (Metal Organic Frameworks)-coated copper oxide composite nanomaterial through liquid phase synthesis; and calcining the nano material through temperature programming to obtain the nitrogen-doped carbon framework-coated highly-dispersed copper-zinc catalyst. The preparation method is characterized in that the copper oxide nano-particles are added in the process of preparing the ZIF-8 of the MOFs material, so that the copper oxide nano-particles are uniformly loaded in the MOFs in situ, the copper reduction and redispersion are implemented while the carbon framework-coated highly-dispersed zinc is obtained after high temperature calcination; a large amount of pyridine nitrogen is also present in the carbon framework; a novel preparation technology of a pyridine nitrogen-doped and carbon framework-supported highly-dispersed copper-zinc catalyst is developed; the catalyst is applied to the carbon monoxide hydrogenation reduction reaction to produce carbon monoxide, and has excellent catalytic activity; the highly-dispersed copper-zinc active sitesand the presence of a large amount of pyridine nitrogen have great promotion actions on improvement of the catalytic activity.
Owner:NANKAI UNIV

Insulin nano transdermal patch and preparation method thereof

The invention relates to an insulin nano transdermal delivery preparation and a preparation method thereof. The insulin nano transdermal delivery preparation takes recombinant human insulin as an active pharmaceutical ingredient and is a filled closed type transdermal preparation consisting of an anti-sticking layer, a drug-loaded layer and a back lining layer. The drug-loaded layer consists of nano recombinant human insulin, a carrier, a penetration enhancer and a plasticizer. The nano recombinant human insulin is obtained by dissolving insulin in a solvent, adding water-soluble auxiliary agents including liposome, chitosan, HPMC (hydroxy propyl methyl cellulose) and the like and an aqueous solution of a freeze-drying protective additive, performing low-temperature high-speed stirring and then performing freeze-drying. The patch disclosed by the invention realizes transdermal noninvasive administration through nano-scale combination of insulin and the carrier to ensure that the bioavailability of the insulin is greatly improved; the patch has the advantages of high transdermal absorption rate, fast response, good treatment effect and good product stability, does not have anaphylactic and toxic reactions to skins, and has the characteristics of good safety, small side effect and convenience in use. The preparation method of the insulin nano transdermal patch disclosed by the invention is simple, low in production cost, and easy to magnify.
Owner:HUBEI UNIVERSITY OF MEDICINE

A preparation method and application method of a highly dispersed copper-zinc catalyst for carbon dioxide reduction

The invention proposes a method for preparing and using a highly dispersed copper-zinc catalyst for carbon dioxide reduction. The method first synthesizes copper oxide nanoparticle precursors with uniform particle size, and then prepares copper oxide composite nanomaterials coated with ZIF-8 MOFs through liquid phase synthesis, and obtains nitrogen-doped carbon skeleton-coated composite nanomaterials after temperature-programmed calcination. Highly dispersed copper zinc catalyst. The feature of the present invention is that the method adds copper oxide nanoparticles in the process of preparing MOFs material ZIF-8, so that the copper oxide nanoparticles are evenly loaded in MOFs in situ, and the highly dispersed carbon skeleton coating is obtained after high-temperature calcination. At the same time as zinc, the reduction and redispersion of copper are also realized, and there are also a large amount of pyridine nitrogen in the carbon skeleton. A new preparation technology for highly dispersed copper-zinc catalysts supported by pyridine nitrogen doped carbon skeletons has been developed, and the The catalyst is used in the hydrogenation reduction reaction of carbon dioxide to prepare carbon monoxide, and has excellent catalytic activity. The highly dispersed copper-zinc active sites and the presence of a large amount of pyridinic nitrogen can greatly promote the improvement of catalytic activity.
Owner:NANKAI UNIV
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