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90results about How to "Increased tensile strength at room temperature" patented technology

Repeated solid solution aging thermal treatment process of titanium alloy

The invention relates to a repeated solid solution aging thermal treatment process of titanium alloy. The process includes the steps that a titanium alloy forge is subjected to heat preservation at the temperature T for t minutes, wherein T is larger than or equal to Tbeta-15 DEG C but smaller than or equal to Tbeta+15 DEG C, t is equal to eta*delta max, delta max is the maximum section thickness of the forge and is shown in millimeters, and eta is the heating coefficient and ranges from 0.2 min/mm to 0.8 min/mm; then the forge is discharged out of a furnace to be air-cooled or wind-cooled or water-cooled to be at the room temperature, then the cooled forge is subjected to heat preservation at the temperature of T for t minutes, wherein T is larger than or equal to Tbeta-25 DEG C but smaller than or equal to Tbeta-50 DEG C, the computational formula of t is as above, namely t=eta*delta max, and the heating coefficient eta ranges from 0.3 min/mm to 1.2 min/mm; then the forge is discharged out of the furnace to be air-cooled or wind-cooled or water-cooled to be at the room temperature, the cooled forge is subjected to heat preservation at the temperature T ranging from 540 DEG C to 600 DEG C, and the heat preservation time t ranges from 0.5 hour to 2 hours; the forge is discharged out of the furnace to be air-cooled to be at the room temperature, the cooled forge is subjected to heat preservation at the temperature T ranging from 400 DEG C to 540 DEG C, and the heat preservation time t ranges from 4 hour to 24 hours; and then the forge is discharged out of the furnace to be air-cooled to be at the room temperature. The repeated solid solution aging thermal treatment process of the titanium alloy is suitable for thermal treatment of near-beta type, metastable beta type and steady beta type ultrahigh-toughness titanium alloy so as to obtain required microscopic structures with high overall performance and multi-scale precipitated phases mixed.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

High-temperature-resisting material as well as preparation method and application thereof

The invention provides a high-temperature-resisting material as well as a preparation method and application thereof. The high-temperature-resisting material is mainly prepared from the following components by mixing and sintering: based on the weight percentage content, 60 percent to 90 percent of refractory aggregate with the granularity of 140 meshes or less, 1 percent to 25 percent of refractory aggregate with the granularity of 200 meshes or more and 2 percent to 25 percent of a binding agent. According to the high-temperature-resisting material provided by the invention, the refractory aggregate with different granularities is combined according to a scientific proportion and then is sintered, so that bridging connection, realized by point contact, between the refractory aggregate (namely aggregate) and the other aggregate can be promoted, and tight connection of bridging is also promoted; a microscopic structure is adopted so that the porosity of the material reaches 30 percent or more and the volume density is less than or equal to 1.5g / cm<3>; cracks are not easily expanded so that the thermal shock performance is good, the pouring temperature is greater than or equal to 1650 DEG C and the room-temperature tensile strength is greater than or equal to 1.0MPa.
Owner:JINAN SHENGQUAN DOUBLE SURPLUS CERAMIC FILTER

Gadolinium-containing die-casting thermostable high-zinc magnesium alloy and method for making same

ActiveCN101177751AImprove strength and plasticityIncrease lattice distortionAluminiumMetal
The invention relates to die-casting and heat-resistant high zinc magnesium alloy with gadolinium content and preparation method thereof and is used in the metal material field. The alloy components and weight percentages thereof are that: Zinc: 6-10 percent, aluminum: 3-7percent, gadolinium: 0.2-2.0 percent, impurity element Fe is less than 0.005 percent, Cu is less than 0.015 percent, Ni is less than 0.002 percent and the rest is magnesium. Pure magnesium, pure zinc, pure aluminum and Mg-25percent Gd are preheated, and then the pure magnesium is put into a melting furnace with the protection of gas to be melted; the pure zinc and the pure aluminum are added immediately after magnesium ingot is thoroughly melted, and scum on the surface is skimmed after the pure zinc and the pure aluminum are thoroughly melted; the temperature rises continuously, Mg-25 percent Gd master alloy is added, and scum on the surface is skimmed after the master alloy is completely melted; melted mixture obtained is stirred, and then refined, stirred and led to be still after the furnace temperature is adjusted; alloy liquid obtained is die-cast after scum on the surface is skimmed and the temperature of the alloy liquid is adjusted down. The invention has low cost and high production efficiency, and improves mechanical properties of the alloy in room temperature and high temperature and creep properties of the alloy.
Owner:SHANGHAI LIGHT ALLOY NET FORMING NAT ENG RES CENT

Preparation method of TiAl-based alloy with fine fully lamellar microstructure

The invention relates to a preparation method of a TiAl-based alloy with a fine fully lamellar microstructure, which belongs to the technical field of preparation of titanium alloys. The preparation method comprises the following steps: placing a powder metallurgic TiAl-based alloy at a temperature which is 5 DEG C-15 DEG C higher than the alpha-phase beta-phase transformation temperature Talpha; and preserving the heat for 15-25 minutes under a protective environment, and cooling to obtain the TiAl-based alloy with the fine fully lamellar microstructure, wherein the powder metallurgic TiAl-based alloy matrix structure is a nearly gamma structure or a gamma structure. According to the preparation method of the TiAl-based alloy with the fine fully lamellar microstructure disclosed by the invention, the fully lamellar microstructure with eutectic cell dimension of 150 microns-320 microns and lamellar spacing of 0.2 micron-0.4 micron can be obtained by a simple thermal treatment method. Moreover, the preparation method is free of hot mechanical treatment, simple in process and low in cost, so that not only can structure optimization be carried out before alloy forming, but also treatment can be directly carried out onto a formed piece. Besides, the preparation method has the advantages of being capable of controlling the microscopic structure of the alloy, simple in production process, regular in used equipment, low in production cost and the like, and is convenient for industrial production.
Owner:CENT SOUTH UNIV

Preparation method of fine grain magnesium alloy

The invention relates to a preparation method of a fine grain magnesium alloy. In the method, the preheating temperature of a mould is 350+/-5 DEG C; a magnesium alloy blank is subjected to at least five passes of extrusion and deformation; the preheating temperature of the magnesium alloy blank is 250+/-5 DEG C-380+/-5 DEG C; the extrusion rate is 2mm/s-15mm/s, and the extrusion direction each time is different; and the preheating temperature of the magnesium alloy blank changes from high to low, and the extrusion rate is varied from large to small. According to the preparation method provided by the invention, a multi-pass multi-direction temperature-variable extrusion technology is adopted, i.e., the temperature and extrusion rate of the magnesium alloy blank are gradually reduced along with the increase of extrusion pass, and forces are applied in the different directions of magnesium alloy so as to carry out extrusion and deformation, thereby improving the deformation nonuniformity of a magnesium alloy structure in the conventional isothermal extrusion deformation and preventing full growth and grain mixing of dynamically recrystallized grains due to high temperature in the extrusion process. Thus, the grains of the magnesium alloy obtained by using the multi-pass multi-direction temperature-variable extrusion deformation are obviously fined, and the size of the grain is uniform.
Owner:NO 59 RES INST OF CHINA ORDNANCE IND

Iron-chromium-aluminum alloy with high plasticity and long service life

The invention relates to an iron-chromium-aluminum alloy with high plasticity and long service life. The iron-chromium-aluminum alloy comprises the following components in percentage by weight: 13.5-14.5 percent of chromium, 3.5-4.5 percent of aluminum, less than or equal to 0.03 percent of carbon, less than 0.24 percent of silicon, 0.3-0.5 percent of titanium, 0.25-0.35 percent of vanadium and the balance of iron. In the invention, the carbon content of the alloy is controlled: carbon plays a harmful role in the inoxidability of the iron-chromium-aluminum alloy, and the formation of harmful carbonates and nitrides can be avoided by lowering the carbon content, so that the plasticity of the alloy is improved. A reasonable aluminum-chromium content ratio is selected: the oxidizing speed of the iron-chromium-aluminum alloy is lowered along with the increase in the aluminum and chromium content, but the plasticity is lowered along with the increase in the aluminum and chromium content. Titanium is doped: the nitriding resistance and corrosion resistance of the alloy are improved. Vanadium is added: tissue product grains of the alloy can be fined, the grain coarsening temperature is raised, the overheat sensitivity of the alloy is lowered, and high hardness and chemical stability with a silicide formed by silicon are realized.
Owner:DANYANG HUALONG SUPERIOR STEEL

Forging method for improving mechanical property of TC4 alloy blade

The invention relates to a forging method for improving the mechanical property of a TC4 alloy blade, which is used for solving the technical problem of poor mechanical strength in a traditional TC4 titanium alloy blade. The invention has the technical scheme that the forging method comprises the following steps of: carrying out solid hydrogen distributing treatment on the TC4 alloy; machining the obtained solid hydrogen distributing titanium alloy blank after treatment into a solid hydrogen distributing titanium alloy prefabricated blank; blowing sand and polishing; spraying a lubricating agent; heating before forging; forging the solid hydrogen distributing titanium alloy blank to obtain a solid hydrogen distributing titanium alloy blade forging piece; removing flash; blowing sand and polishing; and removing hydrogen. The TC4 titanium alloy is subjected to solid hydrogen distributing treatment, so that the tensile strength of the TC4 titanium alloy at room temperature is improved to be 1055-1065MPa from 925-985MPa in the background art; the yield strength of the TC4 titanium alloy at room temperature is improved to be 990-1000MPa from 884-945MPa in the background art; the tensile strength of the TC4 titanium alloy at 400DEG C is improved to be 700-710MPa from 630-675MPa in the background art; and the yield strength of the TC4 titanium alloy at 400DEG C is improved to be 605-615MPa from 593MPa in the background art.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Aluminum alloy and heat treatment method thereof

The invention discloses heat treatment method of an aluminum alloy. The aluminum alloy comprises, by mass, 8%-10% of metal fibers, 5.5%-7.2% of Mg, 1.0%-2.5% of Zn, 0.8%-1.8% of Cu, 0.08%-0.18% of Sc,0.08%-0.18% of Zr, 0.12%-0.22% of Y, 0.02%-0.07% of Si, 0.02%-0.07% of Mn, 0.01%-0.03% of Er, 0.01%-0.03% of Ce, no more than 0.15% of impurities, and the balance Al. The heat treatment method comprises the steps that S1, high-temperature heat treatment is conducted on the aluminum alloy at the temperature of 500-600 DEG C, and after high-temperature heat treatment, quenching is conducted on thealuminum alloy with PAG quenching liquid, so that the aluminum alloy subjected to high-temperature treatment is obtained, wherein the content of PAG polymers in the PAG quenching liquid is 15-60 wt%,the temperature of the PAG quenching liquid is 40-80 DEG C, and the stirring speed of the PAG quenching liquid is 100-200 r/s; S2, cold-deformation treatment is conducted on the aluminum alloy subjected to high-temperature treatment, so that the aluminum alloy subjected to cold deformation is obtained; S3, the aluminum alloy subjected to cold deformation is tempered at the temperature of 300-400 DEG C for 1-2 h; and S4, afterwards, annealing treatment is conducted on the aluminum alloy at the temperature of 100-160 DEG C for 6-8 h, and thus, the strength of the aluminum alloy is improved. Theinvention further provides the aluminum alloy prepared through the heat treatment method.
Owner:益阳仪纬科技有限公司

Method for improving comprehensive performance of carbon nanomaterial reinforced nickel-based superalloy

The invention provides a method for improving the comprehensive performance of a carbon nanomaterial reinforced nickel-based superalloy, and belongs to the field of powder metallurgy and superalloy. Aiming at the problem that the high-temperature oxidation resistance of the carbon nanomaterial reinforced nickel-based superalloy is reduced, the surface of a carbon nanomaterial is coated with a compact Ni layer for the first time, so that the problems of poor mechanical property and high-temperature oxidation resistance caused by easy agglomeration of the carbon nanomaterial, poor bonding with amatrix interface and the like are solved. Through a specific ball milling process, mixed powder with uniformly dispersed carbon nanomaterials is obtained, and further uniform dispersion of the carbonnanomaterials is realized. A carbon nanomaterial reinforced Rene104 nickel-based composite material is prepared through spark plasma sintering (SPS), hot isostatic pressing, hot pressing, hot extrusion or hot forging, or 3D printing and other powder forming methods, so that the prepared material is excellent in mechanical property and excellent in high-temperature oxidation resistance, and the problem that the carbon nanomaterial reinforced metal-based composite material cannot be used as a high-temperature structural material is effectively solved.
Owner:CENT SOUTH UNIV

Flame-retardant graphene titanium-aluminum-based composite material and preparation method

The invention belongs to the technical field of titanium alloy materials, and relates to a flame-retardant graphene titanium-aluminum-based composite material and a preparation method. The composite material is prepared from the following components in percentage by mass: 0.01 to 1 percent of graphene oxide and a titanium and aluminum compound. By adoption of a method of combining temperature-controlled mechanical stirring, vacuumizing treatment, hot isostatic pressing and the like, interface bonding characteristics of graphene oxide and titanium and aluminum compound mixed powder are improved, and the bulk density and the subsequent forming property of the mixed powder are improved; furthermore, the graphene oxide is basically decomposed to form graphene which is uniformly dispersed, so that the excellent mechanical property and the physical and chemical properties of the graphene are fully exerted; the flame retardant property of the obtained composite material is twice that of a common high-temperature titanium alloy or above, and the heat resistance is higher; and a brand-new technical scheme is provided for solving titanium fire of an aero-engine. The flame-retardant graphenetitanium-aluminum-based composite material is a novel material concept; a prepration process is short, can accurately control parameters, and is suitable for batch preparation.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS
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