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120results about How to "High fracture toughness" patented technology

Novel titanium alloy partitioned beta heat treatment process

ActiveCN102851627AGuaranteed uniformityPrecise control of primary alpha phase contentTitaniumTitanium alloy
The invention discloses an accuracy control-based novel titanium alloy partitioned beta heat treatment process. The process includes: first subjecting alpha+beta area forged alpha type and alpha-beta type titanium alloys to preheating at Tbeta-(20DEG C-40DEG C), calculating the heat preservation time according to t(min)=eta*delta max, with the delta max being the largest section thickness of a forged piece and the heating coefficient eta ranging from 0.5 to 0.8; then raising the temperature to (Tbeta-5DEG C)-(Tbeta+5DEG C) along with a furnace, and calculating the heat preservation time t(min) according to the above calculation formula, with the heating coefficient eta ranging from 0.2 to 0.6; and then raising the temperature to (Tbeta+5DEG C)-(Tbeta+30DEG C) along with the furnace again, and calculating the heat preservation time t(min) according to the above calculation formula, with the heating coefficient eta ranging from 0.2 to 0.5; and subjecting the forged piece discharged from the furnace to air cooling or cooling at certain cooling rate. The process is suitable for heat treatment of large, complex, variable section alpha type and alpha-beta type titanium alloy forged pieces, so that required high comprehensive performance lamellar structures with high ductility, high toughness and low fatigue crack propagation ability can be obtained, thus meeting the requirements of airplane and aero-engine manufacturing for large and complex variable section forged pieces or parts with uniform structure performance.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Repeated solid solution aging thermal treatment process of titanium alloy

The invention relates to a repeated solid solution aging thermal treatment process of titanium alloy. The process includes the steps that a titanium alloy forge is subjected to heat preservation at the temperature T for t minutes, wherein T is larger than or equal to Tbeta-15 DEG C but smaller than or equal to Tbeta+15 DEG C, t is equal to eta*delta max, delta max is the maximum section thickness of the forge and is shown in millimeters, and eta is the heating coefficient and ranges from 0.2 min/mm to 0.8 min/mm; then the forge is discharged out of a furnace to be air-cooled or wind-cooled or water-cooled to be at the room temperature, then the cooled forge is subjected to heat preservation at the temperature of T for t minutes, wherein T is larger than or equal to Tbeta-25 DEG C but smaller than or equal to Tbeta-50 DEG C, the computational formula of t is as above, namely t=eta*delta max, and the heating coefficient eta ranges from 0.3 min/mm to 1.2 min/mm; then the forge is discharged out of the furnace to be air-cooled or wind-cooled or water-cooled to be at the room temperature, the cooled forge is subjected to heat preservation at the temperature T ranging from 540 DEG C to 600 DEG C, and the heat preservation time t ranges from 0.5 hour to 2 hours; the forge is discharged out of the furnace to be air-cooled to be at the room temperature, the cooled forge is subjected to heat preservation at the temperature T ranging from 400 DEG C to 540 DEG C, and the heat preservation time t ranges from 4 hour to 24 hours; and then the forge is discharged out of the furnace to be air-cooled to be at the room temperature. The repeated solid solution aging thermal treatment process of the titanium alloy is suitable for thermal treatment of near-beta type, metastable beta type and steady beta type ultrahigh-toughness titanium alloy so as to obtain required microscopic structures with high overall performance and multi-scale precipitated phases mixed.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Graphene composite B4C superhard material preparation method

A graphene composite B4C superhard material preparation method is characterized by comprising the following steps: graphene oxide with the sheet diameter greater than 1mum and the layer number not more than five is mixed with B4C powder with the particle size not more than 3mum, the graphene oxide volume fraction is 0.3% -5%, water with the mass of 20-40 times of the mass of the B4C are added for ultrasonic treatment for 10-30min to obtain a graphene oxide / B4C mixture liquid, the graphene oxide / B4C mixture liquid is stirred for 2h more for more uniform mixing, and finally the graphene oxide / B4C mixture liquid is stirred and dried at a drying temperature below 100 DEG C at atmospheric pressure to obtain mixed powder; the mixed powder is pre-pressed into an initial blank in a molding apparatus; the initial blank is put into a high temperature and high pressure apparatus for high pressure sintering to obtain a graphene composite B4C superhard material, wherein the sintering temperature 1300-1600 DEG C, the sintering pressure is greater than 3GPa, and the sintering time is greater than 10min. The superhard material is harder than 19GPa, the fracture toughness reaches 8.76MPa. m1 / 2, and the fracture toughness of the graphene composite B4C superhard material is improved by more than 1 times compared with that of a pure B4C material.
Owner:INST OF FLUID PHYSICS CHINA ACAD OF ENG PHYSICS

Multi-crystal-nucleus composite transparent glass ceramic and preparation method thereof

The invention discloses multi-crystal-nucleus composite transparent glass ceramic and a preparation method thereof. The preparation method of the multi-crystal-nucleus composite transparent glass ceramic comprises the following steps that: S1, multiple nucleating agents are added during glass melting; S2, plain glass with a certain boundary dimension is obtained after processing; S3, the plain glass obtained in S2 is placed under the condition that the temperature is T1 and heated for 1-6 hours for annealing treatment, after annealing treatment is completed, the plain glass is placed under thecondition that the temperature is T2 and is heated for 1-6 hours and subjected to nucleation treatment, after nucleation treatment is completed, the plain glass is placed under the condition that thetemperature is T3 and heated for 0-3 hours for crystallization treatment, and T1 is smaller than T2. According to the invention, the glass ceramic containing various crystal nucleuses and crystal phases of lithium disilicate and petalite is prepared, the nucleation and crystallization energy required by the crystal precipitation is reduced through the multiple crystal nucleuses, the heat treatment temperature and the heat treatment time can be reduced, the crystal ratio can be adjusted, and the glass ceramic prepared through the preparation method has characteristics of enhanced damage resistance, good fracture toughness and wide application range.
Owner:CHONGQING XINJING SPECIAL GLASS CO LTD

Preparation method of gradient carbon fiber/hydroxyapatite (HA) composite material

The invention relates to a preparation method of a gradient carbon fiber/hydroxyapatite (HA) composite material. The method comprises the following steps: performing compound modification on carbon fibers via low-temperature oxidation and a HA membrane layer pulling and drawing method; dispersing nanometer HA powder, an organic monomer acrylamide, a cross-linking agent N, N-methylene bisacrylamide, a dispersant sodium hexametaphosphate, an initiator ammonium persulfate, a catalyst N,N,N',N'-tetramethylethylenediamine and ammonium hydroxide into deionized water so as to prepare modified carbon fiber-HA duplex ceramic slurry; performing centrifugal molding on the duplex ceramic slurry; then taking out a centrifugal barrel and putting the centrifugal barrel into a water bath kettle so as to realize the curing molding of modified carbon fiber-HA gel; demolding a green body and then drying the green body in a drying box; and sintering the green body under the argon atmosphere in a tubular furnace so as to obtain the gradient carbon fiber-HA composite material. The method has the advantages that the content of carbon fibers at the bottom of the composite material is high, so that the strength and the toughness of the composite material can be improved during the load bearing; the content of HA at the top of the composite material is high, so that the osteoinduction and the biocompatibility of the composite material can be improved when the composite material is implanted into a human body; the centrifugal molding technology is adopted, so that the problem of stress concentration caused by the reason that the carbon fibers are likely to agglomerate during the dry pressing is solved, and thus the mechanical property of the composite material is improved.
Owner:LIAONING UNIVERSITY OF TECHNOLOGY

Method for preparing ceramic biological material with abrasion self-remediation function in in-vivo environment

The invention discloses a method for preparing a ceramic biological material with an abrasion self-remediation function in an in-vivo environment. The ceramic biological material comprises the following raw materials in percentage by mass: 90-99% of zirconia powder (alumina powder) and 1-10% of metal powder. The method comprises the following steps: putting the raw materials into a planet ball mill, uniformly mixing according to a wet method, drying, and performing hot-pressing sintering at 1100-1800 DEG C for 0.5-3 hours in the presence of an inert atmosphere. The metal doping mass ratio in the prepared ceramic biological material is within 1-10%; when the ceramic biological material is used as a friction accessory (such as an artificial joint and an artificial intervertebral disc) in a human body, because of fiction abrasion and corrosion, a layer of protein biological membrane can be formed on a friction interface, along with friction, the protein biological membrane can be converted into a graphite layer, and friction and abrasion of the ceramic biological material can be effectively reduced. Abrasion remediation of the ceramic biological material can be achieved, and the ceramic biological material is good in abrasion self-remediation function in the human body.
Owner:SOUTHWEST JIAOTONG UNIV

Preparation technology of high-comprehensive-performance aluminum-lithium alloy plate

The invention relates to a preparation technology of a high-comprehensive-performance aluminum-lithium alloy plate. The technology comprises the following steps that a cast ingot is subjected to temperature-controlled primary rolling, is rapidly cooled to the room temperature and then is placed into a high-temperature air circulation furnace to be heated, after heat preservation is performed for a period of time, the temperature is reduced to the specific temperature, the cast ingot is discharged from the furnace, secondary hot rolling is performed, and the cast ingot is rapidly cooled to the room temperature after being subjected to hot rolling to the specified size; and then the rolled plate is subjected to solid solution quenching, cold deformation and artificial aging treatment. By means of temperature-controlled hot primary rolling and rapid cooling after rolling, a Widmanstatten structure can be fully broken, appropriate deformation stored energy is reserved, the plate is recrystallized to a certain degree in the subsequent high-temperature heating process, flat and straight grain boundaries among grains in the hot-rolled plate are eliminated, and part of nested morphology is formed; through secondary rolling and rapid cooling at the specific temperature, a recrystallized structure can be transformed into a deformed structure again, and precipitation of large-size Widmanstatten is inhibited, so that the aluminum-lithium alloy treated to be in a final use state has excellent comprehensive performance.
Owner:AVIC BEIJING INST OF AERONAUTICAL MATERIALS

Preparation method of zirconium ball carrier, and application of zirconium ball carrier to manganese-based desulfurizing agent

The invention discloses a preparation method of a zirconium ball carrier, and application of the zirconium ball carrier to a manganese-based desulfurizing agent. During the preparation, zirconia is used as a carrier support body; polyether sulfone is used as a bonding agent; polyvinylpyrrolidone is used as a dispersing agent; through two-way substitution of N-methyl pyrrolidone and water, a sphere is formed by a wet process in water; after high-temperature sintering, a spherical wear-resistant carrier of a porous structure is formed, i.e., the zirconium ball carrier is obtained. A bran-new carrier preparation method is used; the porous wear-resistant spherical carrier is prepared by a phase inversion method; the spherical carrier is suitable for the preparation of all impregnated catalysts; the problems that the air resistance of a conventional powder catalyst is great, so that the spherical carrier can be swept and taken away by airflow during experiment, and the like are solved. When the carrier is used for preparing a high-temperature manganese-based desulfurizing agent, a high-precision renewable desulfurizing agent is obtained; the desulfurizing agent can be used for removing H2S in an IGCC (Integrated Gasification Combined Cycle); the technical support is provided for electric field electricity generation of an SOFC (Solid Oxide Fuel Cell) with high energy utilization efficiency.
Owner:CHINA UNIV OF MINING & TECH

Welding method for reducing site-welding stress deformation of thick-walled steel structure

The invention provides a welding method for reducing the site-welding stress deformation of a thick-walled steel structure, and relates to a welding method. The problems that for an existing steel structure, adjustment of welding residual strain to a welding process is passive, cumbersome and difficult, and the structure of welding joints is poor in stability and anti-fatigue performance are solved. The method comprises the steps that multiple inlaid internal webs are arranged at welding grooves of welding groove at intervals in the length direction of a welding seam, wherein a skeleton systemstructure is jointly formed by welding groove walls of base materials and the inlaid internal webs; welding of the internal webs is conducted, wherein back gouging welding is adopted to ensure complete fusion between the internal webs and the base materials of the welding groove walls of the butt joints; and after the skeleton system structure of the butt joints is welded and formed, filling welding is conducted on a partition space formed by the welding groove walls of the base materials and the multiple inlaid internal webs in an enclosing manner, and cover surface welding is conducted in the longitudinal welding direction of the welding seam. The welding method is used for reducing the site-welding stress deformation of the thick-walled steel structure.
Owner:HARBIN INST OF TECH +6
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