129results about How to "Reduce Methanol Content" patented technology

The invention discloses a process for refining C-4 hydrocarbon fluid. Preparation equipment includes a methanol removing tower, a first hydrogenation reactor, a second hydrogenation reactor, a depropanizing column, a dethanizing column and an adsorption tower, wherein the top of the methanol removing tower is connected with the bottom of the first hydrogenation reactor through a high-efficiency coalescer; the top of the first hydrogenation reactor is connected with the bottom of the second hydrogenation reactor through a pipeline; the top of the second hydrogenation reactor is connected with the depropanizing column through another pipeline; the top of the depropanizing column is connected with the dethanizing column through another pipeline; and the bottom of the dethanizing column is connected with the adsorption tower through another pipeline. The process mainly aims to a purification process of an alkylation raw material, and comprises the following steps: by taking mixed C-4 hydrocarbon as a raw material, extracting with water to remove methanol so as to reduce the content of methanol in C-4 hydrocarbon to be lower than 50ppm, selectively adding hydrogen and isomerizing so as to reduce the content of butadiene in C-4 hydrocarbon to be lower than 50ppm, converting more than 70% of 1-butene into 2-butene, and finally rectifying to remove dimethyl ether and C-3, thereby obtaining refined C-4 as the alkylation raw material, and a byproduct refined C-3 as a propane dehydrogenation propylene raw material.

The invention relates to a production process of a red date ice wine. The process comprises the steps of impurity removing, fruit selecting, washing, crushing, rehydrating, beating, separating, enzymolysis, centrifugal separating, extracting, secondary centrifugal separating, filtering, low-temperature concentrating, yeast activating, controlled-temperature fermenting, fermentation stopping, low-temperature aging, filtering and clarifying, cold treating, sterilizing and filtering, and filling. The process provided by the invention has the advantages that: red date is adopted as a raw material, and a low-temperature rehydration and high-temperature extraction two-stage process is adopted, such that red date juice color, flavor and various rich nutrient contents are ensured, and physiologically active substances in red dates are extracted to a maximal extent; with a two-step method red date ice wine production process that red date juice is produced first and biological fermentation is then carried out, the produced product has a date red color, clarified wine body, rich fragrance, and delicate and mellow mouthfeel. The ice wine has typical characteristics of iced fruit wines, and assists in filling the vacancy in domestic market.

Persimmon wine and a brewing method belong to the technical field of brewing science and engineering. The invention aims to solve the technical problem of providing the persimmon wine keeping the original flavor of persimmons and a brewing method of the persimmon wine. The process is as follows: 1. selecting fruit; 2. breaking and sterilizing; 3. adding yeast and primarily fermenting for 1d; 4. juicing and separating pomace; 5. adding sugar and secondarily fermenting; 6. filtering residue and can sealing; 7. clarifying with pectinase and filtering; and 8.cryotreating and canning. The persimmon wine is characterized in that the persimmon wine is faint yellow, clear and transparent and has pure, fine, refreshing and harmonious aroma. The invention has the following advantages: 1. full persimmons are extracted and the juice is used for fermentation, without adding water; and 2. pectinase is not added in the processes of juice extraction and fruit wine brewing, and astringency removal process is omitted. The invention plays important roles in promoting reasonable processing and utilization of the persimmon resources, forming the post-harvest processing industrial chain and adjusting the fruit processing industrial structure.

The invention discloses a method for brewing white spirit by adopting red dates as a major ingredient. In the invention, the white sprit is prepared by taking fresh or dry red dates as the major ingredient and bran as an auxiliary material and adopting the following steps of: selecting and soaking the red dates, crushing the major ingredient to obtain jujube paste, pre-steaming the auxiliary material, fermenting and distilling the major ingredient and the auxiliary material and the like. In the invention, traditional Chinese medicines are also added to the red dates for crushing during the process of crushing the red dates to obtain the jujube paste, wherein the traditional Chinese medicines contain polyphenol acid as an active component; as the traditional Chinese medicines are added for inhibiting the activity of pectin methyl esterase contained in the major ingredient, the purpose of reducing the generation amount of methanol is achieved. The method is simple to operate, is easy to control, and has a good methanol removing effect, and the quality of the spirit product is greatly improved. The method disclosed by the invention is used for brewing the white spirit with data flavor by adopting the red dates as the major ingredient and the bran as the auxiliary material; the content of methanol can be reduced to lower than 0.06%; all indexes of the white spirit product can meet standards of national level I spirit; and the white spirit product has rich jujube fragrance.

The invention discloses jujube-flavored white spirit and a brewing process thereof. A preparation method of the liquor comprises the following steps: grinding, steaming and spread-cooling jujube, wheat, sorghum, glutinous rice, corn, rice, pea and rice hull according to certain proportions, uniformly mixing with the addition of yeast powder, sealing and fermenting in pit mud for more than 4 months; beginning to distill after 4 months in a mode of distilling twice every month; ultrasonically processing liquor obtained from distillation firstly, and then storing the liquor together with tourmaline, limonite and medicinal stone in a porcelain jar for more than 6 months, thus completing aging. The liquor overcomes shortcomings in the prior art, and is simple and convenient in operation, short in production cycle, high in liquor yield and good in quality. The jujube-flavored white spirit disclosed by the invention is stable in quality, free from restoring and long in aftertaste, people drinking the white spirit are not easy to become drunk and quick to be sobered up, and the white spirit, after drunk, is free from a problem of headache, free from such harmful material components as methanol, and is capable of relieving pressure on liver and kidney after drinking and effectively relieving damage to body.

The invention relates to a brewing method of low-methanol-content Chinese date wine, and belongs to the technical field of brewing. The method includes sorting Chinese dates, cleaning, stoning, soaking with hot water, pulping, adding pectin esterase and cellulase, performing enzymatic hydrolysis, stirring and cooking in an air-lift combined mechanical manner, centrifuging, separating supernatant, adjusting the supernatant with white sugar and citric acid, sterilizing, inoculating, fermenting, clarifying, filtering, adding a clarifying agent, and aging by using an oak barrel. The method degrades cell walls of fruit tissues by using the pectin esterase and the cellulase, degrades polysaccharides to allow effective components inside the Chinese dates to dissolve out, and increases the content of juice nutrients and the juice yield. Through stirring and cooking in the air-lift combined mechanical manner, methanol produced by pectin substance zymolysis through the pectin esterase and methanol produced by other reasons are separated along with stirring, cooking and high-pressure air blowing, thus reducing the methanol content in Chinese date juice pulp.

The invention relates to a fruit wine brewing method, and in particular relates to a low-yield methanol and higher alcohol fruit wine brewing process. The product prepared by the method disclosed by the invention fills blank of specific fruit wine brewing technology research in China, improves product quality of specific fruit wine, and enhances purity and typical aroma characteristic of wine and increases sense quality of the specific fruit wine, so as to make it possible to produce high-quality fruit wine products in many excellent fruit production zones. The technical scheme adopted by the invention comprises the following operation steps: (1) sorting fruit raw materials; (2) crushing, pulping and adding into a tank; (3) adding sulfur dioxide; (4) adding pectinase, and standing at low temperature; (5) naturally increasing temperature, adding a yeast culture liquor to start fermentation; (6) fermenting at controlled temperature, and monitoring fermentation; (7) separating, squeezing and continuing to ferment; (8) transferring to another tank, adding sulfur dioxide and storing; (9) aging in the presence of wine lees; and (10) clarifying, stabilizing, filtering and bottling.

The invention discloses a method for brewing a distilled spirit by using rice as a raw material. According to the method for brewing the distilled spirit, rice is used as the raw material, and white granulated sugar is added for heat preservation before koji and yeast are added into the raw material, thus ensuring that microorganisms in the koji and yeast can be fully activated. In the post-fermentation process, the rice can be fermented fully, the liquor yield can be improved, and the methanol content can be reduced at the same time; the yield can be improved, and the quality of products can be improved at the same time. The liquor obtained by first distillation is subjected to second distillation to finally obtain the product; by virtue of twice distillation, the methanol content in the liquor can be reduced, and the quality of the liquor can be improved.

The invention discloses a process for extracting methanol using water in manufacturing of methyl methacrylate products, wherein the MMA containing a small amount of menthol and water are fed into a static mixer by the proportion of 1:1-5, then into a water extraction pot, the upper layer is the extracted MMA monomer, which enters the next water extraction pot through an overflow port, the lower layer is aqueous solution of menthol, which is pumped onto an upper water extraction pot by a measuring pump, through the extraction by several water extraction pots, the methanol in the MMA can be removed substantially.

The invention discloses fermented red pitaya wine, pitaya brandy and a production method thereof. The method includes: integrally crushing red pitayas, and adding pectinase for enzymolysis; adding yeast, yeast nutrients, vitamin C and chitosan to realize mixed fermentation; after fermentation is in full play, performing low-temperature fermentation through maceration, and carrying out aging, purifying, oak powder treatment, freezing and sterilization aftertreatment to obtain the fermented red pitaya wine; subjecting the prepared original wine to crude distillation and rectification, storing and aging to obtain red pitaya brandy. Whole-fruit fermentation is adopted, technical simplicity and low equipment input cost are realized, and the comprehensive utilization rate of red pitayas is increased; the red pitaya wine is rich in fruity aroma, rich and full in texture, stable in the presence of light, thermal and the like and free of fading, suspensions, precipitates and turbidity after normal-temperature placement over one year; the pitaya brandy is unique in nutrient and aroma, prominent in typicality and superior in quality.

The invention discloses a low-methanol mango-sugarcane wine and a brewing method thereof. The brewing method comprises the following steps: 1) taking mango pulp, beating, and obtaining mango raw pulp;2) mixing raw mango pulp and sugarcane juice evenly, adding fruit wine yeast, and fermenting for 1-3 days at the temperature of 28-32 DEG C, then adding sugar component, carrying out main fermentation under the condition of <28 DEG C until the total soluble sugar content in the fermentation broth is less than or equal to 70g/L, and collecting the fermentation broth; 3) cooling the fermentation broth to 15-18 DEG C and performing fermentation until the total soluble sugar content in the wine reaches the sugar content of the desired brewing type, further reducing the temperature of the obtainedliquor to 4-8 DEG C with heat preservation until a certain amount of gel is generated on the upper layer of the material liquid, filtering and collecting the filtrate; 4) adding a clarifying agent into that filtrate, filtering and sterilizing the obtained material to obtain a liquor; and 5) aging the obtained liquor to obtain the mango-sugarcane wine, wherein the mango-sugarcane wine brewed by the method has low methanol content and good taste.

The invention relates to cherry health wine and a making method thereof. The cherry health wine is made by fermenting, by weight, 80-95% of cherry pulp and 20-5% of mulberry pulp. The two pulps are mixed; pectinase is added to provide a higher juicing rate; low-temperature vacuum concentration helps increase the juice sugar degree and reduce the methanol content; a low-temperature half-fermentation making technique imparts strong fruit fragrance and suitable sourness and sweetness to the cherry health wine. The cherry health wine made herein has the advantages that the mulberry fruit is addedfor coordinated fermentation so that color of the cherry health wine is significantly improved, and the cherry health wine is as functional as cherry to replenish blood by high iron and prevent gout,and as functional as mulberry fruit to improve physical fitness, tonify kidney, darken hair and maintain beauty.

The invention relates to a device and a process for recycling methyl alcohol from gas field alcohol-containing sewage based on a gas stripping process and a vacuum membrane distillation process. A complex process route of performing gas stripping first to obtain a dilute methyl alcohol solution with fewer impurities and then concentrating the dilute methyl alcohol solution through vacuum membrane distillation is adopted. The device and the process have the beneficial effects that related equipment such as a complex rectifying tower, a reboiler and a reflux tank is not needed, so that equipment investment is greatly reduced; the integrated process does not generate methyl alcohol reflux, so that repeated heating of reflux and tower bottoms is avoided, raw materials are sufficiently heated by waste heat of a methyl alcohol product and tower bottom water; waste heat of raw materials heated at a gas-stripping section provides energy for phase change of vacuum membrane distillation, so that methyl alcohol recycling energy consumption is greatly reduced and economic benefits are improved; the problems that content of impurities of alcohol-containing sewage of the raw materials is relatively high and the solution pollutes the hydrophobic microporous membrane are avoided, and the service life of the membrane is prolonged; the gas stripping process and the vacuum membrane distillation composite process are integrated, so that recycling efficiency is improved, and content of methyl alcohol in alcohol-containing sewage is reduced.

The invention discloses a methanol pre-rectifying tower heating process by utilizing a methanol synthetic reaction gas. The methanol pre-rectifying tower heating process mainly comprises the following steps: using the methanol synthetic reaction gas as a heat source for heating a reboiler of a methanol pre-rectifying tower, and then performing feeding heat exchange on the methanol pre-rectifying tower; adopting a negative pressure as the operating pressure at the top of the methanol pre-rectifying tower, wherein the negative pressure is controlled by a water ring vacuum pump; cooling the non-condensable gas pumped by the water ring vacuum pump from the top of the tower, and then feeding the cooled non-condensable gas to a fuel gas pipe network; adding a certain volume of fresh water to the water ring vacuum pump, meanwhile adopting a certain volume of circulating liquid to control the liquid level in a circulating liquid storage tank of a circulating vacuum pump, and feeding the pumped circulating liquid to a reflux tank of the methanol pre-rectifying tower as a reflux liquid of the methanol pre-rectifying tower.

The invention discloses a manufacturing method of dimethyl ether hydrated by carbinol, which comprises the following steps: introducing raw material with carbinol into catalytic distilling tower; hydrating at least partial carbinol to produce dimethyl ether and water; guiding partial steam from the top of catalytic distilling tower into autoclave of second distilling tower; using liquid-phased material in the second distilling tower as reflux liquid to lead into top of catalytic distilling tower; obtaining the mass with dimethyl ether as main component of top of second distilling tower; introducing liquid-phased mass of catalytic distilling tower into the third distilling tower; obtaining the mass with carbinol as main component of third distilling tower to lead into top of catalytic distilling tower or autoclave of second distilling tower; draining water mass as main component from the autoclave of third distilling tower.

The invention relates to a preparation method of kiwi fruit brandy. The preparation method comprises the following steps: preparing kiwi fruit wine; carrying out distilling purification on the kiwi fruit wine to produce brandy; preparing kiwi fruit roots; baking the kiwi fruit roots; and immersing the kiwi fruit roots in the obtained brandy. The kiwi fruit wine is subjected to distilling purification to produce the high-alcohol-content brandy, and the wide kiwi fruit roots are baked and used for storage or immersion instead of the oak barrel or oak sheet used by western brandy, so that the brandy has a unique flavor. The kiwi fruit brandy produced by the technique has the unique flavor, and also has the particular health care and therapeutic functions of the kiwi fruit roots, and the kiwi fruit brandy obtained by immersing the kiwi fruit roots is golden, clear and transparent.

Belonging to the technical field of wine brewing, the invention particularly relates to a preparation method of rosa sterilis honey fruit wine. The method includes the steps of: (1) raw material treatment; (2) juice taking; (3) fermentation liquor adjustment; (4) yeast inoculation; (5) primary fermentation; (6) clarification; (7) ageing; (8) blending; and (9) filtering and bottling: filtering theblended fruit wine by a filtering instrument, and then performing bottling. The rosa sterilis honey fruit wine provided by the invention adopts rosa sterilis and honey as the raw materials, wherein the rosa sterilis is rich in nutrition, contains a lot of vitamin C and polyphenol, has strong fragrance, is coordinated with the mellow and sweet taste of honey, so that the wine body is clear and bright, has harmonious fragrance, delicate and refreshing taste and moderate acerbity, the fruit wine having harmonious fruit fragrance, honey fragrance and wine fragrance is unique in flavor, has low alcoholic strength, more conforms to the development trend of massive health, and is suitable for people of all ages to drink.

The invention provides a catalyst for the catalytic conversion of a synthetic gas as well as a preparation method and application thereof. The catalyst is prepared from the following components in percentage by weight: 9.8% to 78.5% of Co based catalyst, 0.2% to 16.5% of oxide aid and 5% to 90% of Rh based catalyst. The catalyst provided by the invention is a dual-function catalyst, wherein the Cobased catalyst is mainly used for carrying out the generation of olefin; the carrying out of the process can be obviously promoted due to the existence of the oxide aid; the Rh based catalyst is mainly used for the hydroformylation of the olefin; the olefin generated by the Co based catalyst is enabled to further react with the synthetic gas to prepare mixed alcohol with high value added; the catalyst has excellent catalytic performance; low methane and methanol contents and the high alcohol selectivity are presented in product distribution; and the total selectivity of chemical products (alcohol and olefin) with high value added reaches 90% or above.

The invention discloses a method for preparing high-purity refined methanol by three-tower rectification, which is used for preparing high-purity refined methanol by treating a methanol crude product by using a three-tower rectification method. The method comprises the steps of: based on diluted alcohol water or soft water as an extraction agent, distilling in a pre-separating tower to remove low-boiling substances in the methanol crude product and water-insoluble gas so as to obtain pre-separated methanol; sending pre-separated methanol into a pressurizing tower for pressurized rectification treatment, cooling light components at the tower top of the pressurizing tower, returning a part of the light components to the tower top of the pressurizing tower for refluxing, and collecting the rest of the light components as the refined methanol product; sending heavy components at the tower bottom of the pressurizing tower into a main rectifying tower for rectification, cooling light components at the tower top of the main rectifying tower, returning a part of the light components to the tower top of the main rectifying tower for refluxing, and collecting the rest of the light components as the refined methanol product; and discharging the main rectifying tower bottom liquid as waste liquid. By using the 'three-tower rectification' method, the problem that methanol azeotropes cannot be separated in the methanol products is effectively solved, the purity of the obtained refined methanol product reaches more than 99.9%, the mass percent concentration of methanol in the discharged waste liquid is smaller than 1.0%, and the pollution of effluents to the environment is reduced because the methanol content is low.