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51 results about "Petroleum processor" patented technology

The crude oil distillation unit (CDU) is the first processing unit in virtually all petroleum refineries. The CDU distills the incoming crude oil into various fractions of different boiling ranges, each of which are then processed further in the other refinery processing units.

Deep desulfurization method for diesel by coupling of oxidation and extraction

The invention relates to a deep desulfurization method for diesel by coupling of oxidation and extraction, that is a catalyzed oxidation desulfurization method for diesel in petroleum refining technologies. The method comprises the following steps of crushing and fine grinding a zirconium hydroxide carrier, dipping into impregnation liquid formed by aqueous ammonium meta-tungstate solution, placing the impregnation liquid in an ultrasonic generator to carry out ultrasonic facilitating impregnation, boiling off water after the impregnation is finished, drying and baking at high temperature to obtain a WO3/ZrO2 super solid acidic catalyst; adding aqueous hydrogen peroxide solution, extraction solvent and the WO3/ZrO2 super solid acidic catalyst in diesel containing sulfur, carrying out catalyzed oxidation desulfurization reaction under the action of power ultrasonics, cooling to the room temperature after the reaction is finished, separating and recycling the solid catalyst, standing and layering, wherein the upper layer is desulfurized diesel and the lower layer can be reused after regeneration. The invention has simple process, mild condition, high desulfurization degree and gasoline recovery, low cost and no pollution to environment and can obtain ultra-low sulfur clean diesel products.
Owner:YANGZHOU UNIV

Complex sulfurization and denitrification method for distillate

The invention discloses a complex sulfurization and denitrification method for distillate in petrochemical industry and petroleum refining technology. Through the method, sulfides and nitrides are removed from gasoline, diesel oil and other light oil distillate and the oil quality is improved. The technical scheme comprises the following steps of: filling a complexing agent anhydrous AlCl3 and the distillate in a reactor according to a mass ratio of sulfur and nitrogen elements in the distillate to AlCl3 of 0.012-0.120; adding water serving as a complexing aid, wherein the mass ratio of the water to the AlCl3 is 0.08-0.12; carrying out complex reaction at the temperature of between 50 and 80 DEG C for 50 to 70 minutes; after the reaction is finished, making the distillate stand to split phase, wherein the standing time is 10 to 20 minutes; and finally, taking an upper oil phase out, and adding 0.5 to 2.0 volume percent of water to clean residual complex in the oil so as to prepare the refined distillate. The method has the advantages of mild reaction condition, low operating cost, simple technical flow, low equipment investment, good sulfurization and denitrification effects, and use for removing sulfides and nitrides from the distillate in the petroleum refining technology.
Owner:SOUTHWEST PETROLEUM UNIV

Method and device of heavy oil two stage catalytic cracking reforming and gasoline upgrade coupling

The invention is a two-stage heavy oil catalytic cracking conversion method and device, belonging to petroleum refining process and device technical field, separating heavy oil reaction course into top and bottom reacting regions, making raw oil and regenerated catalyst firstly contact and react with each other in the bottom reacting region and successively separating the carbon deposit deactivated catalyst from reacting oil; making the oil gas go up into the second reacting region to mix with the catalyst used in gasoline reaction and continue reaction; a heavy oil reactor is connected in parallel with gasoline reacting part; the gasoline and catalyst complete reaction in the gasoline reactor and then make gas-solid separation in gasoline settler, where the oil gas is discharged through pipeline and the extracted catalyst is fed into pre-rising stages below the first and second heavy oil reacting regions to continue taking part in heavy reaction; a catalyst return pipe is arranged between the pre-rising stages of the gasoline settler and gasoline reactor to make a part of catalyst used in gasoline reaction return to the bottom of the gasoline reactor, so as to take part in gasoline reaction. And it can obviously raise efficiency of heavy oil reactor, improve product quality and need not consume energy because of catalyst change.
Owner:石宝珍

High-temperature corrosion inhibitor for oilfield exploitation and petroleum refining process and preparation method of high-temperature corrosion inhibitor

ActiveCN106433781ASafe and Reliable ProductivitySafe and reliable operabilityDrilling compositionBorehole/well accessoriesPetrochemicalStearic acid
The invention belongs to the technical field of petrochemical equipment and particularly provides a high-temperature corrosion inhibitor for oilfield exploitation and a petroleum refining process. The high-temperature corrosion inhibitor is prepared from raw materials in parts by weight as follows: a raw material group A: 6-8 parts of ricinolic acid and 2-4 parts of stearic acid; a raw material group B: N-methyldiethanolamine, triethanolamine and industrial white oil, wherein the weight of N-methyldiethanolamine is 0.18-0.2 times that of the raw material group A, the weight of triethanolamine is 0.06-0.08 times that of the raw material group A, and the weight of the industrial white oil is 0.35-0.4 times that of the raw material group A. The high-temperature corrosion inhibitor has the corrosion inhibition rate of about 97% and has the advantages of being good in corrosion inhibiting effect, non-irritant, safe, reliable, safe and stable in the production use operation process, environment-friendly and the like. According to the preparation method, performance of the raw materials is comprehensively considered, and the high-temperature corrosion inhibitor with more stable performance and more excellent corrosion inhibition effects can be obtained.
Owner:徐文忠 +1

System for solving ultrahigh gas temperature of dynamic wave furnace of waste acid recycling device

The invention relates to the field of alkylation assorted waste acid recycling devices in the petroleum refining process and in particular relates to a system for solving ultrahigh gas temperature of a dynamic wave furnace of a waste acid recycling device. The system comprises a dynamic wave gas-liquid separator, a filler washing tower and an electric defogger which are connected through a pipeline; the system is characterized in that furnace gas firstly enter a dynamic wave exchange column; the dynamic wave exchange column is connected with one or more reversed injection pipes; a nozzle control valve is arranged on each reversed injection pipe and used for controlling the pressure of the reversed injection pipe; the reversed injection pipes are connected with the dynamic wave gas-liquid separator through a dynamic wave dilute acid pump; the furnace gas enters the dynamic wave gas-liquid separator and carries out gas-liquid separation, then the furnace gas enters the filler washing tower to be washed and cooled, finally the furnace gas enters the electric defogger and removes the residual acid fog. The system is capable of reducing the temperature of a furnace gas outlet of a dynamic wave scrubber, facilitating long-period and safe operation of the device, improving the treatment capacity of the device, reducing the dilute acid treatment capacity and reducing sewage treatment load and cost.
Owner:SHANDONG JINCHENG HEAVY OIL RES INST OFCHEM TECH

Quick-dry fog sealing layer material, and preparation method and application thereof

ActiveCN105542487AClosed maintenance time is shortenedIn situ pavingsOil processingOrganic solvent
The invention relates to a quick-dry fog sealing layer material, which is formed by the following components: 20wt percent to 40wt percent of asphalt-recycling agent, and 5wt percent to 25wt percent of complex solubilizer, wherein the asphalt-recycling agent is formed by deasphalted oil, heavy aromatic oil and additives; the additives are selected from at least one of the following compounds: dibutyl phthalate, epoxidized soybean oil, chlorinated methoxy fatty acid ester and parabens; the mass ratio of the deasphalted oil to the heavy aromatic oil to the additives is 1:0.1 to 1:0.05 to 0.5. The invention also relates to a preparation method and application of the quick-dry fog sealing layer material. According to the quick-dry fog sealing layer material, the heavy aromatic oil and the like during the petroleum refining process are utilized to form the asphalt-recycling agent so as to obtain the fog sealing layer material with high additional value, so that the quick-dry fog sealing layer material can play a role in preventing aging and regenerating on aged asphalt pavements. In addition, according to the quick-dry fog sealing layer material provided by the invention, the maintenance time at low temperature is only 2 to 4h, which is shortened by over half the time for sealing and maintaining of the existing fog sealing layer material.
Owner:EAST CHINA UNIV OF SCI & TECH

Vapor phase heat transfer oil and its preparation process

The invention discloses a gas-phase heat-conducting oil and a preparation process thereof. The gas-phase heat-conducting oil contains alkyl diphenyl and its isomer compounds. The preparation process of gas-phase heat transfer oil includes the following steps: 1. Raw material selection. The raw material selected in this step is the tower bottom material after the catalytic reforming unit in the petroleum refining process or the polyester production raw material p-xylene plant tower bottom material or pyrolysis production Hydrogenation feedstock for ethylene by-products. 2. Extraction of aromatics. In this step, chemical products such as benzene and xylene are obtained, and the remaining products are the primary raw materials for gas-phase heat transfer oil. 3. Precision rectification and purification. In this step, the preliminary raw materials obtained in step 2 are purified, and the fraction at 240°C-270°C is selected, and then the above fraction is sent to a high-efficiency precision rectification tower for further rectification, and the fraction at 252°C-258°C is cut. Narrow cut, ie the final vapor phase heat transfer oil product. This vapor phase heat transfer oil product can completely replace the existing but biphenyl-diphenyl ether products (for example: vp-1, DowthermA, ThermS, ThermS-300 and other foreign vapor phase heat transfer oils).
Owner:北京燕通石油化工有限公司

Method and device of heavy oil two stage catalytic cracking reforming and gasoline upgrade coupling

The invention is a two-stage heavy oil catalytic cracking conversion method and device, belonging to petroleum refining process and device technical field, separating heavy oil reaction course into top and bottom reacting regions, making raw oil and regenerated catalyst firstly contact and react with each other in the bottom reacting region and successively separating the carbon deposit deactivated catalyst from reacting oil; making the oil gas go up into the second reacting region to mix with the catalyst used in gasoline reaction and continue reaction; a heavy oil reactor is connected in parallel with gasoline reacting part; the gasoline and catalyst complete reaction in the gasoline reactor and then make gas-solid separation in gasoline settler, where the oil gas is discharged through pipeline and the extracted catalyst is fed into pre-rising stages below the first and second heavy oil reacting regions to continue taking part in heavy reaction; a catalyst return pipe is arranged between the pre-rising stages of the gasoline settler and gasoline reactor to make a part of catalyst used in gasoline reaction return to the bottom of the gasoline reactor, so as to take part in gasoline reaction. And it can obviously raise efficiency of heavy oil reactor, improve product quality and need not consume energy because of catalyst change.
Owner:石宝珍

High-temperature corrosion inhibitor used in oil field exploitation and petroleum refining process and preparation method thereof

The invention belongs to the technical field of petrochemical equipment and particularly provides a high-temperature corrosion inhibitor for oilfield exploitation and a petroleum refining process. The high-temperature corrosion inhibitor is prepared from raw materials in parts by weight as follows: a raw material group A: 6-8 parts of ricinolic acid and 2-4 parts of stearic acid; a raw material group B: N-methyldiethanolamine, triethanolamine and industrial white oil, wherein the weight of N-methyldiethanolamine is 0.18-0.2 times that of the raw material group A, the weight of triethanolamine is 0.06-0.08 times that of the raw material group A, and the weight of the industrial white oil is 0.35-0.4 times that of the raw material group A. The high-temperature corrosion inhibitor has the corrosion inhibition rate of about 97% and has the advantages of being good in corrosion inhibiting effect, non-irritant, safe, reliable, safe and stable in the production use operation process, environment-friendly and the like. According to the preparation method, performance of the raw materials is comprehensively considered, and the high-temperature corrosion inhibitor with more stable performance and more excellent corrosion inhibition effects can be obtained.
Owner:徐文忠 +1

A method for self-adaptive control of fractionation tower liquid level in petroleum refining process

The invention discloses an adaptive control method for the liquid level of a fractionation tower in the petroleum refining process. In this method, the reverse error neural network and extreme value optimization method are used as adaptive tools, and the predictive PI control strategy is designed in combination with the input and output of the actual operation process. The present invention first uses the data acquisition device to collect the past input and output of the system, and then designs an extreme value optimization algorithm as a solver to adjust the weight of the neural network online, thereby efficiently and accurately training the neural network; after satisfying the set error constraints, The trained neural network weight is used as the identification parameter of the system, and a system model close to the actual situation is established. Finally, the predictive PI control is designed to control the liquid level of the fractionation tower in the process of petroleum refining. By adopting the method of the invention, the interference of model mismatch to the system can be effectively relieved, the control performance is improved, and the application of advanced control in industrial process control is also promoted.
Owner:DONGHUA UNIV

A kind of quick-drying mist sealing layer material and its preparation method and application

ActiveCN105542487BClosed maintenance time is shortenedIn situ pavingsOil processingOrganic solvent
The invention relates to a quick-dry fog sealing layer material, which is formed by the following components: 20wt percent to 40wt percent of asphalt-recycling agent, and 5wt percent to 25wt percent of complex solubilizer, wherein the asphalt-recycling agent is formed by deasphalted oil, heavy aromatic oil and additives; the additives are selected from at least one of the following compounds: dibutyl phthalate, epoxidized soybean oil, chlorinated methoxy fatty acid ester and parabens; the mass ratio of the deasphalted oil to the heavy aromatic oil to the additives is 1:0.1 to 1:0.05 to 0.5. The invention also relates to a preparation method and application of the quick-dry fog sealing layer material. According to the quick-dry fog sealing layer material, the heavy aromatic oil and the like during the petroleum refining process are utilized to form the asphalt-recycling agent so as to obtain the fog sealing layer material with high additional value, so that the quick-dry fog sealing layer material can play a role in preventing aging and regenerating on aged asphalt pavements. In addition, according to the quick-dry fog sealing layer material provided by the invention, the maintenance time at low temperature is only 2 to 4h, which is shortened by over half the time for sealing and maintaining of the existing fog sealing layer material.
Owner:EAST CHINA UNIV OF SCI & TECH
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