The invention relates to a
sol-
gel preparation method of a
ceramic bonding agent. The preparation method comprises the steps that 1)
zinc acetate and
zirconium acetate are taken and dissolved in an
acetic acid solution to prepare a
mixed solution A, and
sodium nitrate,
lithium nitrate and
aluminum nitrate are taken and dissolved in a
boric acid solution to prepare a
mixed solution B; 2) tetrabutyltitanate is taken and added into absolute
ethanol to prepare a solution, the
mixed solution A is added, and heat reaction is carried out under ultrasonic conditions to prepare
sol A; 3) firstly the mixed solution B is added into acidic silica
sol for mixing uniformly, and then the sol A is added to prepare mixed sol; 4)
ammonia is added into the mixed sol under the ultrasonic conditions, so thatpH of a
system reaches 5 or above, and wet gel is prepared; and 5) the obtained wet gel is dried, sintered and cooled to obtain the
ceramic bonding agent. According to the preparation method, the uniform mixing of components of the
ceramic bonding agent at the
molecular level is promoted through smooth rubber
alloy, the grain size is small, the reactivity is high, refractoriness is greatly reduced, and high-temperature fluidity is significantly improved; and formed pores after
sintering are small and uniform, the structure is uniform without defects, and the
mechanical strength is high.