The invention provides an
analysis method for polyether
polyol hydroxyl value, which comprises the following steps: A, weighing a polyether
polyol test sample m into a conical flask, and taking another empty conical flask; B, transferring a
phthalic anhydride pyridine solution into the
test sample accommodated conical flask and the empty conical flask respectively, placing the two conical flasks in an oscillation
oil bath pan, and connecting the two conical flasks with an air condensation
pipe for reaction; C, after reaction, taking the two conical flasks out of the
oil bath pan for cooling; D, flushing the two conical flasks with deionized water and
acetone in sequence, and oscillating the two conical flasks to mix the solutions completely; E, adding a
sodium hydroxide aqueous solution into the two conical flasks respectively, and adding a few drops of
phenolphthalein indicator; F, titrating the solutions in the two conical flasks with
potassium hydroxide standard solution until the solutions in the two conical flasks changes into pink; and G, calculating out the polyether
polyol hydroxyl value as per a formula. The method is simple in analysis procedure, has high precision and accuracy, can efficiently shorten detection period, lower experimental cost, and bring certain economical benefits to an enterprise.