The invention relates to the technical field of preparation of
rare earth functional materials, and particularly discloses a preparation method and device of a trinity
coupling reinforced
rare earth oxide. The preparation device comprises an ultrasonic-
microwave composite
resonant cavity, a micro-channel reaction unit, an ultrasonic unit, a
microwave heating unit, a pulse synchronous triggering module and a multi-parameter linkage closed-
loop control module, and in-situ synchronous
coupling of a micro-channel, ultrasonic and
microwave in the cavity can be achieved. The preparation method is implemented based on the device, sequentially comprises five steps of
raw material preparation, parameter presetting,
coupling reaction, closed-loop regulation and control and product collection, and can realize time-space synchronous propulsion of precursor
nucleation, agglomeration inhibition and in-situ
crystallization. According to the device and the preparation method, the
mass transfer efficiency in the
rare earth oxide preparation process can be effectively improved, product
particle aggregation is inhibited, the stability and the production efficiency of
continuous production are improved, and the large-scale preparation requirements of high-end rare earth oxides are met.