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51results about How to "Inexpensive and easy to operate" patented technology

Treating method for thallium-containing wastewater

The invention provides a treating method for thallium-containing wastewater. The treating method comprises the following steps: 1) adding an oxidizing agent into the thallium-containing wastewater for oxidizing; 2) performing sedimentation treatment including sodium sulphide sedimentation and flocculant sedimentation on the thallium-containing wastewater subjected to oxidizing treatment; 3) adopting an adsorbent for absorbing the supernatant liquid obtained in the step 2), thereby finishing the treatment for thallium-containing wastewater, wherein styrene-divinyl benzene copolymer is taken as the adsorbent. The treating method for thallium-containing wastewater, provided by the invention, comprises the processes of oxidizing treatment, sedimentation treatment and adsorption treatment; the sedimentation treatment comprises the two steps of sodium sulphide sedimentation and flocculant sedimentation; an oxidation-sedimentation-adsorption combined technique is combined with a physical chemistry method, so that secondary pollution is not caused; according to the treating method provided by the invention, the treating condition is easy to control and thallium in the wastewater can be extremely removed; the raw materials required by the treating method provided by the invention are easily acquired and low in cost; the operation is simple; the running cost is greatly lowered.
Owner:湖南省环境保护科学研究院

Preparation method of 3-selenocoumarin compound

The invention discloses a preparation method of a 3-selenocoumarin compound, which comprises the following steps: in a DCM solvent, synthesizing to obtain the 3-selenocoumarin compound at room temperature by using PIFA as an oxidant and using a coumarin compound and a selenide compound as substrates. According to the method, the reaction raw materials are cheap and easy to obtain, the preparationmethod is simple, PIFA is used as an oxidizing agent, the reaction cost is low, the reaction time is short, the yield is high, the operation is simple, and the method is suitable for synthesizing different types of 3-selenocoumarin compounds. The method disclosed by the invention can be used for synthesizing a series of 3-selenocoumarin compounds, and the synthesized product can be used as an intermediate compound for further constructing a complex active compound; meanwhile, the compound has great drug activity potential.
Owner:WENZHOU MEDICAL UNIV

Method for synthesizing acetanilide derivatives

The invention discloses a method for synthesizing acetanilide derivatives, and belongs to the technical field of organic synthetic intermediates. The method particularly includes steps of adding aniline derivatives, potassium thioacetate, tert-butyl nitrite and acetonitrile into reaction tubes; tightening plugs of the reaction tubes; carrying out magnetic stirring reaction at the temperature of 25DEG C for 4 hours. The aniline derivatives and the potassium thioacetate which is low in cost and easy to operate, is easily available and is stable are used as acetylation reagents, and accordinglya series of acetanilide derivatives can be efficiently synthesized by the aid of the method under the room-temperature conditions. The acetanilide derivatives which are compounds contain arylamine skeletons and can be used for synthesizing and modifying organic synthetic intermediates and medicines, and novel and effective synthesis processes can be provided to screening medicines. The reaction can be accelerated by the tert-butyl nitrite to synthesize the compounds which are the acetanilide derivatives. Compared with existing synthesis methods, the method has the advantages that reaction conditions are simple, raw materials for the acetanilide derivatives are low in cost and easy to operate, are easily available and are stable, and functional groups of substrates are good in tolerance.
Owner:JIYANG COLLEGE OF ZHEJIANG A & F UNIV
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