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100results about How to "Low acid concentration" patented technology

Method for preparation of compound amino acid liquid from cottonseed meal

The invention relates to a method for preparation of a compound amino acid liquid from cottonseed meal. The method includes: firstly carrying out mechanical crushing and cooking pretreatment on cottonseed meal, then inoculating Aspergillus niger, Aspergillus oryzae and Saccharomyces cerevisiae, and conducting culture under an aerobic condition for 15-20h to form a first level enzymolysis system, then inoculating Bacillus subtilis and bacillus licheniformis respectively to further conduct aerobic culture for 18-32h so as to form a fermentation broth, then adding edible grade concentrated hydrochloric acid into the fermentation broth to perform acid hydrolysis, and carrying out filtration and acidity adjustment settlement in order at the end of the hydrolysis to obtain the compound amino acid liquid, then refining the compound amino acid liquid by a complexing affinity extraction technology, mixing the extraction residual water phase generated in the refining process with the compound amino acid liquid to prepare light soy sauce, and taking the raffinate oil phase as an extraction agent for cycle use in refining of next batch compound amino acid liquid. The method provided by the invention not only effectively improves the raw material utilization rate, reduces the production cost, avoids generation of toxic by-products, but also increases the additional value of the product.
Owner:WUHAN POLYTECHNIC UNIVERSITY

Dilute nitric acid production process

The invention belongs to the field of chemical industry, and in particular, relates to a dilute nitric acid production process. The process includes the following steps: after ammonia evaporation andheating, adjusting the flow quantity, allowing gas ammonia to enter an ammonia-air mixer and uniformly mixing the gas ammonia with compressed air; allowing the ammonia-air mixture after mixing to enter an oxidation furnace, carrying out catalytic oxidation reaction on a platinum mesh surface, oxidizing ammonia into nitric oxide, recycling waste heat from process gas leaving the catalyst through awaste heat boiler and tail gas respectively, and then condensing by a low-pressure quick cooler, after separation of dilute acid, mixing the process gas with air from a bleaching tower, and then allowing the mixed gas to enter an oxidation nitrogen compressor; further increasing the temperature of gas through the compressed process gas; recycling waste heat of the compressed process gas, cooling,and then allowing the cooled process gas to enter an absorption tower; and carrying out a reaction of oxide of nitrogen in the absorption tower after absorption with water to generate nitric acid. Theprocess has the advantages of high nitrogen oxide absorption rate, low ammonia consumption, high acid concentration and low tail gas emission concentration, and can reach the standard without furthertreatment.
Owner:SICHUAN GOLDEN ELEPHANT SINCERITY CHEM CO LTD

Two-stage curing vanadium extraction method of stone coal vanadium ores

The invention provides a two-stage curing vanadium extraction method of stone coal vanadium ores. The two-stage curing vanadium extraction method comprises the following steps: (1) firstly, breaking and grinding the stone coal vanadium ores, and then adding water and concentrated sulfuric acid to the obtained ore powder and mixing evenly to obtain a mixture, wherein the mass of the concentrated sulfuric acid added accounts for 10%-15% of the mass of the stone coal vanadium ores; (2) curing the mixture, next, leaching the obtained mixture by use of water, and performing liquid-solid separation to obtain a vanadium-containing leaching solution and leaching slag; (3) adding concentrated sulfuric acid to the leaching slag and mixing evenly, next, curing, leaching the obtained mixture by use of water, and performing liquid-solid separation to obtain a vanadium-containing leaching solution and leaching slag, wherein the mass of the concentrated sulfuric acid added accounts for 10%-15% of the mass of the stone coal vanadium ores; and (4) blending the vanadium-containing leaching solution of the step (2) and the vanadium-containing leaching solution of the step (3). The two-stage curing vanadium extraction method of the stone coal vanadium ores has the advantages that side reactions in curing are effectively inhibited and the vanadium leaching rate is greatly increased. A two-stage low-acid curing method is adopted, the acid concentration is relatively low, and the curing process is clean and environment-friendly; and as a result, the two-stage low-acid curing method has a great industrial application prospect.
Owner:肃北蒙古族自治县西矿钒科技有限公司
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