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39results about How to "Retain heat resistance" patented technology

Preparation method of self-adhesive pure polyimide composite paper

ActiveCN108071042ARetain thermal performanceRetain radiation resistancePaper coatingPaper/cardboardFiberPapermaking
The invention relates to a preparation method of self-adhesive pure polyimide composite paper. The preparation method comprises the following steps: under the protection of nitrogen, adding diamine monomers and dianhydride monomers into an aprotic polar solvent for reacting; then, adding a catalyst to perform a polymerization reaction to obtain a polyimide stock solution; filtering, defoaming, diluting, and injecting into a precipitation solution to obtain a polyimide precipitation fibre suspension; washing, filtering and drying to obtain polyimide precipitation fibres; mixing the polyimide precipitation fibres and polyimide chopped fibres to obtain a homogeneous slurry; papermaking, squeezing and drying to obtain polyimide composite paper; performing solvent spraying after-treatment, coldpressing, and drying to obtain the self-adhesive pure polyimide composite paper. According to the preparation method of the self-adhesive pure polyimide composite paper, the solvent spraying after-treatment is adopted, part precipitation fibres are dissolved, and a film-fibre coexisting state is formed after a solvent is removed so that the obtained composite paper has the strength of the film, also has the characteristics of paper, remains original heat resistance, irradiation resistance, electrical performance and the like of polyimide paper, has higher strength, and can meet the application with higher requirement on the environment.
Owner:DONGHUA UNIV

Crystalline polyaryletherketone nanofiber membrane and preparation method and application thereof

The invention discloses a crystalline polyaryletherketone nanofiber membrane and a preparation method and application thereof and belongs to the technical field of electrostatic spinning. According tothe method, an electrostatic spinning technology is utilized, and a soluble polyaryletherketone-polyaryletherketone-1,3-dioxolame or polyaryletherketone imine solution is adopted for preparing the crystalline polyaryletherketone nanofiber membrane. The method has the advantages that the operation is simple, there is no need to adopt external aids, the cost is low, large-scale production can be achieved, the limit caused by the insolubility of polyaryletherketone in an organic solvent to a processing method is broken through, and the excellent heat resistance, radiation resistance, chemical corrosion resistance, fatigue resistance, impact resistance, creep resistance, wear resistance, flame retardance and mechanical property of crystalline polyaryletherketone are retained. The crystallinepolyaryletherketone nanofiber membrane prepared by means of the method is controllable in fiber diameter and thickness, does not require the external aids and high-temperature treatment, can be normally used under severe conditions and can be applied into fuel cells, super capacitors and lithium ion batteries.
Owner:JILIN UNIV

Double-crosslinking-point monomer based carboxylic acid type ACM (acrylate rubber) and preparation method thereof

The invention discloses double-crosslinking-point monomer based carboxylic acid type ACM (acrylate rubber) and a preparation method thereof. The carboxylic acid type ACM is prepared from the followingmonomers in percentage by mass through polymerization: 65%-85% of alkyl acrylate monomers, 10%-30% of oil-resistant and low-temperature-resistant monomers and 3%-8% of vulcanization point monomers, wherein the vulcanization point monomers comprise butene diacid diester monomers and olefinic bond type unsaturated monomers containing carboxyl groups, and a mass ratio of the butene diacid diester monomers to the olefinic bond type unsaturated monomers containing carboxyl groups is 1:2-2:3; ester groups in the olefinic bond type unsaturated monomers are ether alcohol with the carbon atom number being 6-10. According to the prepared rubber, on the basis of reservation of low permanent compression set value, oil resistance and heat resistance of carboxylic acid type acrylate rubber, processability is further improved, smoothness of the rubber surface is improved, and obtained acrylate vulcanized rubber composition can be used for preparing parts such as a hydraulic oil delivery pipe, a cylinder gasket, a sealing gasket and the like of an automobile and a locomotive.
Owner:GUANGZHOU SHINE POLYMER TECH

Cold-construction non-curable rubber modified asphalt coating for waterproofing and preparation method thereof

The invention relates to a cold-construction non-curable rubber modified asphalt coating for waterproofing and a preparation method thereof, and belongs to the technical field of chemical engineering.The coating composition is prepared from the following raw materials in parts by mass: 20-40 parts of asphalt, 10-15 parts of thermoplastic rubber, 15-30 parts of a solvent, 8-12 parts of softening oil, 1-2.5 parts of a viscosity regulator, 8-10 parts of phosphated nano silicon oxide, 3-6 parts of 2,2,4-trimethyl-1,3-pentanediol monoisobutyrate, 15-30 parts of calcium carbonate powder and 1-3 parts of mineral fibers. According to the invention, the softening oil, the phosphated nano silicon oxide and the 2,2,4-trimethyl-1,3-pentanediol monoisobutyrate are added into the waterproof coating tomodify the waterproof coating, so that viscosity of the coating is reduced, the flowing property of the coating is improved, the coating can be sprayed under a relatively low-temperature condition of60 DEG C or below, and high energy consumption and high pollution caused by high-temperature spraying are avoided. The coating can be widely applied to waterproofing, dampproofing and seepage proofingof important projects such as high-speed rails, subways, high ways, airports, underground pipe galleries, bridges, tunnels and the like.
Owner:山东省金帅防水材料有限公司

A kind of synthetic method of epoxy-terminated polythioether liquid rubber

The invention discloses a synthetic method for epoxy end group polythioether liquid rubber. The method comprises the following steps: synthesizing sulphydryl end group polythioether liquid rubber by using thiodiglycol, hydroxyethyl-2-hydroxypropyl thioether and the like as main monomers; then using polyethylene glycol diglycidyl ether resin as a transforming agent so as to transform a sulphydryl end group into an epoxy end group so as to finally generate the end group polythioether liquid rubber. The technology has the advantages that the polyethylene glycol diglycidyl ether resin is adopted as the transforming agent of the end group, the defects that the viscosity of a sulphydryl in traditional epoxy modification technology is high, solvents of toluene, butanone and the like are needed to perform dilution, the reaction exotherm is violent, and a side effect is easy to generate are overcome; reactions are smooth, the product quality is easy to control, the viscosity of the generated epoxy end group polythioether liquid rubber is moderate, and the stability is good; the strength of epoxy resin and the toughness and the heat resistance of polythioether rubber are reserved after the end group is transformed, so that the brittleness of the epoxy resin is improved, and the adhesive property of materials is improved.
Owner:锦西化工研究院有限公司

A kind of double crosslinking point monomer carboxylic acid type acrylate rubber and its preparation method

The invention discloses a double crosslinking point monomer carboxylic acid type acrylate rubber and a preparation method thereof. The carboxylic acid type acrylate rubber is obtained by polymerizing the following monomers calculated by mass percentage: 65%-85% of alkyl acrylate monomers; 10%-30% of oil-resistant and low-temperature resistant monomers; 3%-30% of vulcanization point monomers 8%; wherein, the vulcanization point monomers include butenedioic acid diester monomers and ethylenically unsaturated monomers containing carboxyl groups, and the butenedioic acid diester monomers and carboxyl group-containing The mass ratio of the ethylenically unsaturated monomers in the group is 1:2 to 2:3; the ester group in the butenedioic acid diester monomer is an ether alcohol with 6 to 10 carbon atoms. The rubber prepared by the present invention further improves the processing performance and improves the smoothness of the rubber surface on the basis of retaining the low compression set rate, oil resistance and heat resistance of the carboxylic acid type acrylate rubber, and the obtained acrylate vulcanizate composition can be used for Preparation of hydraulic oil pipes, cylinder gaskets, gaskets and other components for automobiles and locomotives.
Owner:GUANGZHOU SHINE POLYMER TECH
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