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38results about How to "Fill pores" patented technology

Method for preparing silicon carbide coating on graphite surface

ActiveCN102850087AAvoid thermal mismatchHigh bonding strengthChemical vaporsCoating
The invention discloses a method for preparing a silicon carbide coating on a graphite surface. The method includes, firstly, placing a graphite crucible containing solid silicone materials in a high temperature graphitizing furnace and placing a graphite base body on a graphite support in the graphite crucible to generate a silicon carbide coating by means of direct reaction of silicon steam and carbon on the surface of the graphite base body; and secondly, placing the graphite base body which generates the silicon carbide coating on the surface in a chemical vapor deposition (CVD) furnace to be pyrolyzed on the surface of the silicon carbide coating which is located on the surface of the graphite base body to generate a CVD silicon carbide coating. According to the method for preparing the silicon carbide coating on the graphite surface, by means of the direct reaction of the silicon steam formed by heating the solid silicone materials and the carbon on the surface of the graphite base body, an in-situ formed chemical vapor reaction (CVR) silicon carbide coating is firmly combined on the graphite base body so that combination intensity is improved; and then a CVD process is used for pyrolyzing the CVR silicon carbide coating at high temperatures on the CVD silicon carbide coating so that pore space of the CVR silicon carbide coating is effectively filled, and combination strength is improved.
Owner:XIAN CHAOMA SCI TECH

High-reflective acrylic polyurethane coating composition

The invention relates to a high-reflective acrylic polyurethane coating composition which comprises a component A and a component B in a mass part ratio of 20;3. The component A in 100 parts by mass comprises the following materials in part by mass: 30-50 parts of modified hydroxyl acrylic resin, 2-6 parts of auxiliaries, 35-45 parts of heat reflective pigments, 4-8 parts of aerogel and 10-15 parts of organic solvent. The component B in 100 parts by mass comprises the following materials in part by mass: 75-90 parts of polyisocyanate and 10-25 parts of organic solvent. The modified hydroxyl acrylic resin is obtained by cold-blending modified resin and hydroxyl acrylic resin in a mass part ratio of 1-3: 1; the solid content of the modified hydroxyl acrylic resin is greater than or equals to 75wt%; the particle size of heat reflective pigments ranges from 0.55 micron to 1.2 microns; the particle size of the aerogel ranges from 1 micron to 80 microns; the pore size of the aerogel ranges from 10 nanometers to 20 nanometers; and the heat conductivity coefficient of the aerogel is less than or equals to 0.015W/(m k). The polyisocyanate is one or more of HDI (hexamethylene diisocyanate) biuret, HDI trimer and IPDI (isophorone diisocyanate) trimer curing agents. The high-reflective acrylic polyurethane coating composition is high in reflective insulation quality; and the quantity of VOC (volatile organic compounds) of the high-reflective acrylic polyurethane coating component is low.
Owner:CNOOC CHANGZHOU PAINT & COATINGS IND RES INST +2

Vacuum heat insulating plate and preparation and application thereof

The invention provides a vacuum heat insulating plate and preparation and application of the vacuum heat insulating plate. The vacuum heat insulating plate comprises a heat insulating core material and a film material coating the heat insulating core material. The heat insulating core material comprises nanoscale silicon dioxide and is formed by mixing the nanoscale silicon dioxide with multi-scale expanded perlites and chopped fibers in the weight ratio of 10:5-30:1. The specific surface area of the nanoscale silicon dioxide is 100-400m<2>/g. The incompact stacking density of the multi-size expanded perlites is lower than 350kg/m<3>. The length of the chopped fibers is less than 10mm, and the diameter is less than 20mum. The vacuum heat insulating plate is obtained by uniformly mixing the raw materials, putting the uniformly mixed raw materials into a mold for pressing and molding, taking out the molded core materials, drying the molded core materials to constant weight, putting the core materials into a bag which is prepared from the film material in advance, vacuumizing till the vacuum degree is less than 0.1Pa, and then performing hot sealing. The vacuum heat insulating plate is high in strength and good in heat insulating effect. In this way, the vacuum heat insulating plate is applied to the heat insulation of building walls.
Owner:SOUTHEAST UNIV

Tertiary air duct curve prefabricated component for cement kiln

The present invention provides a with tertiary air duct curve prefabricated component for a cement kiln, and aims to resolve the problem of poor anti-erosion performance of the tertiary air duct curve of the prior art. The tertiary air duct curve prefabricated component for the cement kiln comprises the following components by weight parts of: 15-25 parts of 5-8mm black corundum, 15-20 parts of 3-5mm black corundum, 10-15 parts of 1-3mm black corundum, 10-15 parts of 0-1mm black corundum, 10-20 parts by 0-1mm of silicon carbide, 6-10 parts of silicon carbide powder not larger than 200 mesh, 5-10 parts of brown alumina powder not larger than 200 mesh, 4-7 parts of calcium aluminate cement, 3-5 parts of alumina powder, 4-6 parts of silica powder, 0.10-0.15 part of a water reducing agent, 0.01-0.02 part of explosion-proof fiber and 0.5-1 part of heat-resistant steel fiber. The invention uses black corundum and silicon carbide as the main materials for the tertiary air duct curve prefabricated component, and the black corundum can make the matrix and aggregate fully connect and cement at high temperature, effectively fill the pores of aggregate and significantly improve the high temperature properties of the material, thereby increasing the abrasion resistance and alkali erosion resistance of the tertiary air duct curve inner liner.
Owner:ZHEJIANG KINGCRED NEW MATERIAL CO LTD

Calcium sulfate-doped high-performance fiber cement-based composite material and preparation method thereof

The invention discloses a calcium sulfate-doped high-performance fiber cement-based composite material and a preparation method thereof, and belongs to the technical field of cement materials. The calcium sulfate-doped high-performance fiber cement-based composite material consists of cement, fly ash, silica fume, quartz sand, calcium sulfate, water, a water reducing agent, a thickening agent andPVA fibers. The preparation method comprises the following steps of: mixing and pouring the cement, the fly ash, the silica fume, the quartz sand, the calcium sulfate and the thickening agent into a stirrer for dry stirring for two minutes; pouring the water reducing agent into the water, and pouring the mixture of the water reducing agent and the water into the stirrer for stirring for four minutes after being fully and uniformly mixed; and then adding the PVA fibers into a stirring pot for stirring for three minutes at the speed of 90-100 revolutions per minute and for one minute at the speed of 180-190 revolutions per minute. According to the composite material and the preparation method thereof, the raw materials are convenient to obtain, the preparation process is simple, and the strength of a test piece is improved while the good tensile mechanical property of the test piece is maintained by adding the calcium sulfate. Meanwhile, the fly ash is adopted to replace the cement in the cementing material, so that an industrial waste residue is consumed, and the carbon emission is reduced.
Owner:BEIJING UNIV OF TECH

Vacuum heat insulating plate and preparation and application thereof

The invention provides a vacuum heat insulating plate and preparation and application of the vacuum heat insulating plate. The vacuum heat insulating plate comprises a heat insulating core material and a film material coating the heat insulating core material. The heat insulating core material comprises nanoscale silicon dioxide and is formed by mixing the nanoscale silicon dioxide with multi-scale expanded perlites and chopped fibers in the weight ratio of 10:5-30:1. The specific surface area of the nanoscale silicon dioxide is 100-400m<2> / g. The incompact stacking density of the multi-size expanded perlites is lower than 350kg / m<3>. The length of the chopped fibers is less than 10mm, and the diameter is less than 20mum. The vacuum heat insulating plate is obtained by uniformly mixing the raw materials, putting the uniformly mixed raw materials into a mold for pressing and molding, taking out the molded core materials, drying the molded core materials to constant weight, putting the core materials into a bag which is prepared from the film material in advance, vacuumizing till the vacuum degree is less than 0.1Pa, and then performing hot sealing. The vacuum heat insulating plate is high in strength and good in heat insulating effect. In this way, the vacuum heat insulating plate is applied to the heat insulation of building walls.
Owner:SOUTHEAST UNIV

Preparation method of zirconium tungstate-containing aluminum-based composite material with high comprehensive performance

The invention discloses a preparation method of a zirconium tungstate-containing aluminum-based composite material with high comprehensive performance, and relates to a preparation method of a ZrW2O8 aluminum-based composite material. The problems that an existing ZrW2O8 / Al composite material is low in strength, and the thermal expansion coefficient of the composite material is large due to the fact that the content of gamma-ZrW2O8 is too high are solved. The method comprises the following steps: weighing ZrW2O8 powder, high-strength ceramic powder and an aluminum matrix as raw materials; the preparation method comprises the following steps: mixing high-strength ceramic powder and ZrW2O8 powder, carrying out ball milling, pre-pressing to obtain a reinforcement preform, preheating, preparing a molten metal matrix, carrying out liquid aluminum infiltration, and carrying out annealing treatment on the composite material. The volume fraction of a reinforcement is increased by adopting a mixing ratio of various particle sizes, internal stress is reduced through stress relief annealing treatment, so that the thermal expansion coefficient of the composite material is reduced, and the comprehensive performance of the composite material is improved.
Owner:HARBIN INST OF TECH

Compound amorphous seed added electrical porcelain and preparation method thereof

InactiveCN104803668AIncreased elastic strain energyEasy to prepare ingredientsBreaking strengthMullite
The invention discloses compound amorphous seed added electrical porcelain and a preparation method thereof. The compound amorphous seed added electrical porcelain is prepared from the following raw materials in weight percent: 10-20% of SiO2, 10-25% of Al2O3, 10-20% of Fe2O3, 1-5% of TiO2, 2-10% of CaO, 0-3% of MgO, 5-15% of K2O, 3-8% of Na2O, and 5-20% of compound amorphous seeds. According to the compound amorphous seed added electrical porcelain and the preparation method thereof disclosed by the invention, the compound amorphous seeds (CaB2O4 amorphous seed and CaB4O7 amorphous seed) are added, so that the softening characteristic of the amorphous seeds can be exerted, and the sintering process of the electrical porcelain can be promoted; in the temperature raising process, the compound amorphous seeds can be converted into compound seed crystals (CaB2O4 seed crystal and CaB4O7 seed crystal), and the seed crystals are molten to form a liquid phase, so that the sintering process of the electrical porcelain can be further promoted, the density of the electric porcelain can be improved, and the breaking strength of the electrical porcelain is obviously enhanced; in addition, the addition of the compound amorphous seeds can effectively facilitate crystallization of mullite phase, and furthermore the mechanical strength of the electrical porcelain is obviously improved. The preparation method disclosed by the invention is simple and accessible in raw materials, stable and mature in process, and capable of meeting the requirements of practicability and industrialization.
Owner:FUZHOU UNIV

Zirconia ceramic slurry, preparation method thereof, false tooth and false tooth preparation method

PendingCN114621006ASolve the defect that it is easy to settle for a long timeSolve the defect of easy settlementImpression capsAdditive manufacturing apparatusUv absorbanceTooth Preparations
The invention discloses zirconia ceramic slurry, a preparation method thereof, a false tooth and a false tooth preparation method. The zirconia ceramic slurry is prepared from the following raw materials: yttria-stabilized zirconia, a dispersing agent, an ultraviolet absorbent, a photoinitiator, photosensitive resin, a toughening agent, a bonding aid, a defoaming agent and a silane coupling agent, the invention relates to a light-sensitive ceramic material, which is prepared from the following components in parts by weight: 60 to 75 parts of yttria-stabilized zirconia, 2 to 4 parts of dispersing agent, 1 to 3 parts of ultraviolet absorbent, 3 to 5.2 parts of photoinitiator, 18 to 26 parts of photosensitive resin, 3 to 6 parts of toughening agent, 5 to 11.4 parts of bonding aid and 2 to 2.6 parts of defoaming agent, wherein the yttria-stabilized zirconia is prepared from the following components in parts by weight: 60 to 75 parts of yttria-stabilized zirconia, 2 to 4 parts of dispersing agent, 1 to 3 parts of ultraviolet absorbent, 3 to 5.2 parts of photoinitiator, 18 to 26 parts of photosensitive resin, 3 to 6 parts of toughening agent, 5 to 11.4 parts of bonding aid and 2 to 2.6 parts of defoaming agent; the weight part of the silane coupling agent is 1-3 parts; and the particle size of the yttrium oxide-stabilized zirconium oxide is 50-100 nm. The slurry can effectively overcome the defect that traditional zirconium oxide slurry is easy to settle after being placed for a long time.
Owner:西安优梨数字科技有限公司

A kind of thin flame-retardant medium density fiberboard and its preparation method

ActiveCN105751346BThermoplasticEffectively fills poresDomestic articlesFlat articlesFiberSingle type
The invention discloses a thin flame-retardant medium-density fiberboard which comprises the following raw materials: a fiber raw material, urea resin accounting for 8-16 weight percent of the fiber raw material, a flame retardant accounting for 8-20 weight percent of the fiber raw material, ammonia chloride accounting for 0.12-0.24 weight percent of the fiber raw material and emulsion paraffin accounting for 0.6-1.2 weight percent of the fiber raw material, wherein the flame retardant comprises a solid flame retardant and a liquid flame retardant. The thin flame-retardant medium-density fiberboard disclosed by the invention adopts the two types of flame retardants, namely the solid flame retardant and the liquid flame retardant, and can solve the problem that the structure is simple due to the addition of the single type of flame retardant, so that the mechanical property is reduced; by the collaborative use of the solid flame retardant and the liquid flame retardant, pores inside the fiberboard can be effectively filled; the liquid flame retardant can form a good connecting link between two solid matters; meanwhile, the liquid flame retardant has a certain thermal plasticity, so that the adverse effect of the flame-retardant on the mechanical properties of the board can be reduced to a certain extent.
Owner:文安县和民木业有限公司

A kind of electric porcelain with added composite seed amorphous and its preparation method

The invention discloses compound amorphous seed added electrical porcelain and a preparation method thereof. The compound amorphous seed added electrical porcelain is prepared from the following raw materials in weight percent: 10-20% of SiO2, 10-25% of Al2O3, 10-20% of Fe2O3, 1-5% of TiO2, 2-10% of CaO, 0-3% of MgO, 5-15% of K2O, 3-8% of Na2O, and 5-20% of compound amorphous seeds. According to the compound amorphous seed added electrical porcelain and the preparation method thereof disclosed by the invention, the compound amorphous seeds (CaB2O4 amorphous seed and CaB4O7 amorphous seed) are added, so that the softening characteristic of the amorphous seeds can be exerted, and the sintering process of the electrical porcelain can be promoted; in the temperature raising process, the compound amorphous seeds can be converted into compound seed crystals (CaB2O4 seed crystal and CaB4O7 seed crystal), and the seed crystals are molten to form a liquid phase, so that the sintering process of the electrical porcelain can be further promoted, the density of the electric porcelain can be improved, and the breaking strength of the electrical porcelain is obviously enhanced; in addition, the addition of the compound amorphous seeds can effectively facilitate crystallization of mullite phase, and furthermore the mechanical strength of the electrical porcelain is obviously improved. The preparation method disclosed by the invention is simple and accessible in raw materials, stable and mature in process, and capable of meeting the requirements of practicability and industrialization.
Owner:FUZHOU UNIV

Aerogel heat insulation sleeve for battery and preparation method of aerogel heat insulation sleeve

The invention discloses an aerogel heat insulation sleeve for a battery. The aerogel heat insulation sleeve for the battery comprises a cylindrical sleeve body with one end sealed, wherein grooves are formed in the sleeve body in an axis direction, and the number of the grooves is 1-4, and the grooves are evenly distributed in the circumferential direction. The preparation method comprises the following steps: (1) continuously pumping uniform superfine fiber slurry into a hollow special-shaped mold, allowing fibers to be stacked in the mold and to be automatically woven and formed, and then carrying out drying and demolding to obtain a superfine fiber sleeve; (2) preparing a silicon dioxide micelle particle solution; (3) adding the silicon dioxide micellar particle solution into the superfine fiber sleeve, and then conducting treatment by using a mechanical wave dispersion method to obtain a heat insulation sleeve gel preform; (4) putting the heat insulation sleeve gel preform into an alcoholic solution of a water repellent for modification; and (5) prefabricating the modified heat insulation sleeve gel, and conducting drying and demolding to obtain the aerogel heat insulation sleeve for the battery. The sleeve is uniformly formed, and the defects of non-uniform gum dipping, bending, cavities and the like are effectively avoided.
Owner:GUIZHOU AEROSPACE WUJIANG MACHINERY & ELECTRICITYEQUIP

A kind of high reflectance acrylic polyurethane coating composition

The invention relates to a high-reflective acrylic polyurethane coating composition which comprises a component A and a component B in a mass part ratio of 20;3. The component A in 100 parts by mass comprises the following materials in part by mass: 30-50 parts of modified hydroxyl acrylic resin, 2-6 parts of auxiliaries, 35-45 parts of heat reflective pigments, 4-8 parts of aerogel and 10-15 parts of organic solvent. The component B in 100 parts by mass comprises the following materials in part by mass: 75-90 parts of polyisocyanate and 10-25 parts of organic solvent. The modified hydroxyl acrylic resin is obtained by cold-blending modified resin and hydroxyl acrylic resin in a mass part ratio of 1-3: 1; the solid content of the modified hydroxyl acrylic resin is greater than or equals to 75wt%; the particle size of heat reflective pigments ranges from 0.55 micron to 1.2 microns; the particle size of the aerogel ranges from 1 micron to 80 microns; the pore size of the aerogel ranges from 10 nanometers to 20 nanometers; and the heat conductivity coefficient of the aerogel is less than or equals to 0.015W / (m k). The polyisocyanate is one or more of HDI (hexamethylene diisocyanate) biuret, HDI trimer and IPDI (isophorone diisocyanate) trimer curing agents. The high-reflective acrylic polyurethane coating composition is high in reflective insulation quality; and the quantity of VOC (volatile organic compounds) of the high-reflective acrylic polyurethane coating component is low.
Owner:CNOOC CHANGZHOU PAINT & COATINGS IND RES INST +2

A method for preparing silicon carbide coating on graphite surface

ActiveCN102850087BFill poresAvoid thermal mismatchChemical vapor depositionSilicon
The invention discloses a method for preparing a silicon carbide coating on a graphite surface. The method includes, firstly, placing a graphite crucible containing solid silicone materials in a high temperature graphitizing furnace and placing a graphite base body on a graphite support in the graphite crucible to generate a silicon carbide coating by means of direct reaction of silicon steam and carbon on the surface of the graphite base body; and secondly, placing the graphite base body which generates the silicon carbide coating on the surface in a chemical vapor deposition (CVD) furnace to be pyrolyzed on the surface of the silicon carbide coating which is located on the surface of the graphite base body to generate a CVD silicon carbide coating. According to the method for preparing the silicon carbide coating on the graphite surface, by means of the direct reaction of the silicon steam formed by heating the solid silicone materials and the carbon on the surface of the graphite base body, an in-situ formed chemical vapor reaction (CVR) silicon carbide coating is firmly combined on the graphite base body so that combination intensity is improved; and then a CVD process is used for pyrolyzing the CVR silicon carbide coating at high temperatures on the CVD silicon carbide coating so that pore space of the CVR silicon carbide coating is effectively filled, and combination strength is improved.
Owner:XIAN CHAOMA SCI TECH
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