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33results about How to "Improve discoloration efficiency" patented technology

Reflection layer material for electrochromic lens and device thereof

The invention discloses a material of a reflecting layer of an electrochromic mirror. The material is characterized in that a used reflecting film is a silver alloy reflecting film, and the work function of the silver alloy is not greater than 4.2eV; a related electrochromic device is manufactured by a negative electrode of an LCD or an LED device or an OLED device, a positive electrode which is glass plated with ITO or transparent conductive film, a frame gel which is epoxy resin, an electrochromic material which is filled in a cavity and UV gel which is dispensed for sealing. The material of the conductive reflecting layer has good performance, higher reflectivity and stability, meanwhile, the material reduces contact potential barrier between the electrode and the electrochromic material, reduces the drive voltage, improves electrochromism efficiency and prolongs the service life of the devices; furthermore, the silver alloy with good performance is taken as the conductive reflecting film to provide the electrochromic device with stable performance.
Owner:宁波视控汽车电子有限公司

Electro-chromic material

The invention provides an electro-chromic material. The electro-chromic material comprises an upper glass substrate, a conducting reflective layer, an electro-chromic material, a transparent conducting layer and a lower glass substrate which are stacked in sequence. The material performance of the conducting reflective layer of the electro-chromic material is excellent, the electro-chromic material has high reflectivity and stability, a contact-potential barrier between an electrode and the electro-chromic material is reduced, drive voltage is reduced, the electro-chromic efficiency is improved, and the service life of a device is prolonged. In addition, silver alloy having excellent performance serves as a conducting reflective film, and an electro-chromic device is stable in performance.
Owner:HUADE PLASTIC PROD CO LTD

Method for increasing gas-chromism thin film gas-chromism speed

InactiveCN101186448AReduced aerochromic response timeEfficient use ofHigh energyUltraviolet
The invention pertains to the technical field of gasochromic film, in particular to a method for improving gasochromism speed of the gasochromic film. The invention adopts sol-gel method for preparing the stable solution containing various metal oxides and the compound solution thereof; and various methods are employed for coating transparent and even gasochromic film on common glass or polished silicon wafer, and ultraviolet or high energy ray and high energy-particle mixing with catalyst are employed in the gasochromic film method so as to change the structure of film and enhance the coloring response speed of the gasochromism of the sol-gel technique, shorten coloring saturation time. Compared with the non treatment film, the gasochromism efficiency are greatly improved; and the performance is the same as the gasochromism produced by magnetron sputtering method, while, cost is greatly reduced; and the produced film by the invention also has the same advantages as the electrochromic film. The invention makes up the shortages of gasochromism smart window made by sol-gel preparation method, thus the smart window technique can be more mature.
Owner:TONGJI UNIV

Preparation method for electrochromism film with molybdenum-doped tungsten oxide nanometer structure for screen printing

The invention discloses a preparation method for an electrochromism film with a molybdenum-doped tungsten oxide nanometer structure for screen printing. According to the technical scheme, the method comprises the following steps: dissolving tungstic acid in hydrogen peroxide; heating in oil bath and stirring for acquiring a clear solution; adding molybdenum oxide, ethylene glycol and deionized water into the clear solution; heating an oil bath pan; condensing and refluxing, thereby acquiring a molybdenum-doped tungsten oxide nanometer sol; centrifuging, and washing for later use; dissolving ethyl cellulose in alcohol under room temperature and stirring, thereby acquiring a clear transparent sol; adding terpilenol and the molybdenum-doped tungsten oxide nanometer sol prepared in the previous step into the sol; performing rotary evaporation on the organic solvent, thereby acquiring molybdenum-doped tungsten oxide nanometer slurry; with a screen printing or scraping method, uniformly attaching the molybdenum-doped tungsten oxide nanometer slurry to an ITO or FTO conductive glass substrate, then calcining in a muffle furnace and naturally cooling, thereby acquiring the electrochromism film with the molybdenum-doped tungsten oxide nanometer structure.
Owner:JIEYANG HONGGUANG COATED GLASS +1

Photochromic material and application thereof

The invention belongs to the field of materials, and particularly relates to a photochromic material and application thereof. The photochromic material is prepared through a method which includes thesteps that (a) tungsten and / or molybdenum source compounds, a surfactant and a solvent are mixed to obtain a first solution, and the surfactant and acid liquor are mixed to obtain a second solution, wherein the surfactant is one or more of lignosulfonate, heavy alkylbenzene sulfonate, alkyl sulfonate, cetyl trimethyl ammonium bromide, sodium dodecyl benzene sulfonate, polyvinylpyrrolidone, polyvinyl alcohol, disodium ethylene diamine tetraacetic acid, lauroyl glutamic acid, sodium octadecyl sulfate and fatty alcohol-polyoxyethylene ether sodium sulfate; and (b) the second solution is dropwiseadded into the first solution to obtain the photochromic material. The photochromic material has high color changing efficiency, secondary pollution such as waste water cannot be generated in the preparation process of the photochromic material, and the photochromic material is quite suitable for being applied to the fields of decoration materials, information storing materials, laminated glass and the like.
Owner:UNIV OF SCI & TECH OF CHINA

Reflecting film structure of transition layer

The invention provides a reflecting film structure of a transition layer. The reflecting film structure comprises a glass substrate, a reflecting layer laminated on the glass substrate and a transition layer arranged between the reflecting layer and the glass substrate. The transition layer is made of Cr or stainless steel or Al or Ti or Ni or ITO or Xn3In2O6 or fluorine-mixed ITO or ZnO. The thickness of the transition layer is 5-200 nanometers. The reflecting film structure of the transition layer is made of the material similar to the reflecting layer, so that firmness in connection between the reflecting layer and the glass substrate is ensured, and color changing efficiency of a transmission layer can be improved.
Owner:HUADE PLASTIC PROD CO LTD

ITO/WO3 composite electrochromic film having nano mosaic structure and preparation method thereof

ActiveCN107512854AIncreased amplitude of electrochromic light modulationEnhanced electrochromic reaction interfaceCoatingsOrganic solventSpray coating
The invention discloses a preparation method of an ITO / WO3 nano composite electrochromic film having a nano mosaic structure. The preparation method comprises the following steps: (1) dissolving prepared ITO nanocrystals in a nonpolar organic solvent to obtain a nanocrystal solution; (2) adding a polar solvent DMF and a ligand exchanger nitronium tetrafluoroborate into the nanocrystal solution, and performing standing or low-speed centrifugal treatment, so that the ITO nanocrystals are transferred into the polar solvent DMF to form an ITO nanocrystal DMF solution; (3) adding a tungsten source precursor into the ITO nanocrystal DMF solution to form a composite solution; (4) adding ethanol into the composite solution to regulate the viscosity and surface tension; (5) coating the solution obtained in the step (4) on a substrate through a spin coating method, a pulling method or a spray coating method to form a wet film; and (6) annealing the wet film in air to obtain the WO3 film. The invention also discloses the ITO / WO3 nano composite electrochromic film prepared through the above method. The preparation method disclosed by the invention is simple and low in cost, thereby being suitable for industrial production.
Owner:ZHEJIANG UNIV

Household gauze, anti-mosquito and anti-insect gauze, multifunctional window and application

The invention belongs to the technical field of smart homes and discloses household gauze, anti-mosquito and anti-insect gauze, a multifunctional window and application. The household gauze is woven from FDY, the anti-mosquito and anti-insect gauze is woven from FDY to which an anti-mosquito and anti-insect agent is added, and the outer layer of the multifunctional window is shielded by a gauze sash in a sliding mode. The anti-mosquito and anti-insect gauze is embedded into the gauze sash. A temperature and humidity inductor is embedded into a frame body and connected with a rainwater shielding device through a wire. An electronic control photochromic glass unit is embedded into the frame body, and the electronic control photochromic glass unit and the rainwater shielding device are both wirelessly connected with a remote control end. The abrasion resistance, oxidation resistance and strength of the FDY are greatly improved; in the aspect of the monofilament elongation-at-break Cv value, it is guaranteed that adhesive force is good after the anti-mosquito and anti-insect agent is added; the colors of the electronic control photochromic glass unit change according to different illumination environments, and the optimal practical effect is achieved.
Owner:高新航

Microdefect-induced electrochromic intelligent glass composite membrane group and preparation method thereof

The invention relates to a microdefect-induced electrochromic intelligent glass composite film group and a preparation method thereof. The microdefect-induced electrochromic intelligent glass composite film group is characterized in that a WO3 layer, an electrolyte layer, a NiO layer and an electrode layer are sequentially arranged on an FTO or ITO surface of an FTO or ITO conductive glass substrate, wherein SiO2 nano microspheres are embedded in the WO3 layer and the NiO layer, the electrolyte layer is a Li < x > Ga < y > O or Li < x > Nb < y > O layer, and the electrode layer is an ITO layer. The beneficial effects of the invention are that: SiO2 nano particles are embedded in the color-changing layer to serve as micro defects; the micro-defect nanospheres and the color-changing layer can form interface defects to promote induced aggregation of ions at a micro-defect interface in the electrochromism process, so that the purpose of improving the color-changing efficiency of the film is achieved, including accelerating the coloring time, increasing the light modulation amplitude, improving the color-changing uniformity and the like. According to the method for preparing the ITO electrode layer through normal-temperature sputtering, the ITO thin film is prepared through normal-temperature sputtering, the performance of the thin film is guaranteed, and meanwhile possible influences of heating on a film system color changing layer and an electrolyte layer are avoided.
Owner:(CNBM) BENGBU DESIGN & RES INST FOR GLASS IND CO LTD

Flexible electrochromic device and preparing method thereof

The present invention relates to a flexible electrochromic device and a preparing method thereof. The preparing method mainly comprises: preparing a flexible extensible PDMS substrate, preparing a PDMS coated with a Dielectric-Metal-Dielectric structure, preparing a TCO-coated PDMS counter electrode, preparing a solid / gel electrolyte; and finally, using a silk screen printing method to print the solid / gel electrolyte onto the PDMS coated with the Dielectric-Metal-Dielectric structure, after the solid / gel electrolyte is cured and formed, placing the TCO-coated PDMS counter electrode onto the solid / gel electrolyte, and performing sealing processing around by using PVB rubber, to form ECDs of a pattern array structure. The flexible electrochromic device provided in the present invention is divided into a flexible substrate, a solid / gel electrolyte layer, an electrochromic layer of a DMD structure, and a transparent conductive layer, so that a plurality of times of circular electrochromismcan be performed, circular electrochromism is more stable, electrochromism efficiency is higher, and the device is flexible. The preparing method is simple, efficient, and low in costs, and can fastimplement industrial production. The flexible electrochromic device and the preparing method thereof are applied to an aspect of car and building intelligence systems, and can reduce energy consumed by cities and achieve an objective of energy conservation.
Owner:SHANTOU UNIV

Novel antibiosis exterior wall high solid emulsion paint

The invention discloses a novel antibiosis exterior wall high solid emulsion paint, which comprises the following ingredients: 10-20 parts of glycol, 1-3 parts of phosphatidylcholine bilayer, 10-20 parts of stearamide, 2-6 parts of dimethicone, 1-3 parts of sodium benzoate, 200-300 parts of ultrafine TiO2, 100-200 parts of ultrafine SiO2, 100-200 parts of light calcium, 50-60 parts of barium sulfate, 400-500 parts of pure propanal emulsion, 10-20 parts of ester alcohol-12, 2-6 parts of ethoxylated alky-sodium sulfide, 3-5 parts of ammoniacal liquor, 2-5 parts of naphthopyrans and 100-200 parts of water. The invention also discloses a preparation method of the novel antibiosis exterior wall high solid emulsion paint. The novel antibiosis exterior wall high solid emulsion paint has the advantages of strong antibiosis capability, high color change efficiency and simple preparation technology.
Owner:ZHEJIANG JINGHU CONSTR GRP

Intelligent temperature control adhesive tape and production process thereof

The invention discloses an intelligent temperature control adhesive tape which comprises an adhesive tape base body, and the adhesive tape base body is coated with an adhesive layer. The adhesive layer is prepared from the following raw materials in parts by weight: 40 to 50 parts of epoxy resin, 10 to 20 parts of crosslinking modified liquid, 5 to 10 parts of modified heat-sensitive material, 3 to 6 parts of polyester polyol, 1 to 5 parts of polyethylene glycol and 1 to 2 parts of rare earth liquid. According to the intelligent temperature control adhesive tape, epoxy resin is adopted as a matrix and matched with raw materials such as cross-linking modified liquid and a modified heat-sensitive material to prepare the adhesive layer, the rare earth liquid is added, the raw material activating effect is achieved, the reaction force between the raw materials is enhanced, plasma treatment is conducted on the adhesive tape matrix, and therefore the microstructure activity is changed, and the temperature control effect is improved. The bonding strength of the adhesive layer and the adhesive tape base body is improved.
Owner:HUNAN WANQI TECH CO LTD

Preparation method of WO3/MoO3 composite electrochromic film

The invention discloses a preparation method of a WO3 / MoO3 composite electrochromic film. A WO3 reaction solution is prepared and a WO3 nanorod array film is prepared by using a hydrothermal method; MoO3 electro-deposition liquid is prepared; MoO3 is electrodeposited on a WO3 nanorod array by using an electrodeposition method; and then a WO3 / MoO3 composite electrochromic film is prepared. According to the invention, the obtained WO3 / MoO3 composite electrochromic film has the better electrochromic performance by being compared with the single WO3 electrochromic film. The preparation method is simple and is easy to operate; and the prepared WO3 / MoO3 composite electrochromic film has advantages of low cost and pollution prevention.
Owner:TIANJIN CHENGJIAN UNIV

Preparation method of tungsten oxide/ammonium molybdate composite film for electrochromism

The invention discloses a preparation method of a tungsten oxide / ammonium molybdate composite film for electrochromism. The method comprises the following steps: firstly, preparing a tungsten oxide film by adopting an optimized hydrothermal method; then depositing ammonium molybdate nanoparticles on the tungsten oxide thin film by adopting an electro-deposition method; and finally obtaining the tungsten oxide / ammonium molybdate composite film material. According to the prepared composite film, the electrochromism performance of tungsten oxide is improved, and the electrochromism efficiency is improved; the preparation method is simple and easy to operate and low in overall cost.
Owner:TIANJIN CHENGJIAN UNIV

Manufacturing method of externally-convex transparent conductive film

The invention relates to the micro nano printing technology field and especially relates to a manufacturing method of an externally-convex transparent conductive film. The method comprises the following steps of manufacturing a base material; directly filling a conductive material in a uv structure groove through a micro-nano printing mode; transferring the conductive material in the groove to a surface of a transparent base material to form a transparent conductive film through static electricity and viscosity of a uv glue in an uv transfer printing mode; coating a uv resin, preparing a pet optical bare material or other optical base materials after one embedded transparent conductive film is manufactured; coating the uv resin on the pet optical bare material or the other optical base materials or the embedded conductive film; and laminating the two materials in a same-size ratio manner, and then carrying out roller impressing. In the invention, advantages of a small resistance and strong conductivity are achieved, a conductive layer is directly based on an optical material without interference of other media, simultaneously a phenomenon that a waste liquid in yellow photoetchingpollutes an environment is avoided, pollution to the environment is prevented, production cost is reduced, and losses of a source material are reduced.
Owner:WUJIANG YOUXIN NEW MATERIAL TECH

Intelligent temperature control tape and its production process

The invention discloses an intelligent temperature-control adhesive tape, comprising an adhesive tape base body, and an adhesive layer is coated on the adhesive tape base; the adhesive layer comprises the following raw materials in parts by weight: 40-50 parts of epoxy resin, 10-20 parts of cross-linking modification liquid parts, 5-10 parts of modified heat-sensitive material, 3-6 parts of polyester polyol, 1-5 parts of polyethylene glycol, and 1-2 parts of rare earth liquid. The intelligent temperature control tape of the invention adopts epoxy resin as the matrix, and prepares an adhesive layer by cooperating with raw materials such as cross-linking modification liquid and modified heat-sensitive material. The addition of rare earth liquid has the effect of activating raw materials and enhancing the reaction force between raw materials. , and then plasma treatment is performed on the tape substrate, so that the microstructure activity changes, and the bonding strength between the adhesive layer and the tape substrate is improved.
Owner:HUNAN WANQI TECH CO LTD

ito/wo with nano damascene structure 3 Composite electrochromic thin film and preparation method thereof

ActiveCN107512854BIncreased amplitude of electrochromic light modulationEnhanced electrochromic reaction interfaceCoatingsSpray coatingOrganosolv
The invention discloses a preparation method of an ITO / WO3 nano composite electrochromic film having a nano mosaic structure. The preparation method comprises the following steps: (1) dissolving prepared ITO nanocrystals in a nonpolar organic solvent to obtain a nanocrystal solution; (2) adding a polar solvent DMF and a ligand exchanger nitronium tetrafluoroborate into the nanocrystal solution, and performing standing or low-speed centrifugal treatment, so that the ITO nanocrystals are transferred into the polar solvent DMF to form an ITO nanocrystal DMF solution; (3) adding a tungsten source precursor into the ITO nanocrystal DMF solution to form a composite solution; (4) adding ethanol into the composite solution to regulate the viscosity and surface tension; (5) coating the solution obtained in the step (4) on a substrate through a spin coating method, a pulling method or a spray coating method to form a wet film; and (6) annealing the wet film in air to obtain the WO3 film. The invention also discloses the ITO / WO3 nano composite electrochromic film prepared through the above method. The preparation method disclosed by the invention is simple and low in cost, thereby being suitable for industrial production.
Owner:ZHEJIANG UNIV

A w with electrochromic properties 18 o 49 /wo 3 Composite film and preparation method thereof

ActiveCN109455946BImprove discoloration efficiencyGreatly improve the color changing efficiencyCoatingsNano structuringComposite film
The invention discloses a W18O49 / WO3 composite film with electrochromic property; a WO3 layer and a W18O49 layer are sequentially deposited on transparent conductive glass from bottom to top. The invention discloses a preparation method of the composite film. The method comprises the following steps: (1) depositing tungsten oxide on the surface of clean transparent conductive glass by using directcurrent (DC) reactive sputtering method, and annealing to obtain the WO3 layer; (2) placing a precursor solution in a reaction kettle, and placing the transparent conductive glass, deposited with theWO3 layer, in the reaction kettle, wherein the WO3 layer of the transparent conductive glass is 0-3mm higher than the liquid level; (3) after the reaction kettle reacts at a preset temperature for apredetermined time, taking out the reaction kettle to obtain the transparent conductive glass having the W18O49 / WO3 composite film. The dense WO3 makes a great contribution to the service cycle stability of the composite film and provides a transition for realization of the WO3 nanostructure morphology with a larger specific surface area, so that the composite film with a higher color changing efficiency is formed.
Owner:NINGBO GEOSTAR PHOTOELECTRIC TECH

Electrochromic device with single substrate structure

ActiveCN102183862BFacilitate the realization of practical applicationSimple production processTenebresent compositionsNon-linear opticsDisplay deviceEngineering
The invention discloses an electrochromic device. The device comprises a conductive substrate (1), and an electrochromic layer (2), an ionic conducting layer (3), an insulating reflection layer (4) and a counter electrode layer (5) which are deposited on the substrate in turn from bottom to top. Due to various tests, bias voltage which is needed to be applied to the electrochromic device with a single substrate structure is low, so that energy is saved, and the device is high in electrochromic property, bright in color, high in response speed and long in service life. The electrochromic device with the structure is simple in production process and low in cost, can be applied to monochromatic display devices such as subtitle billboards, traffic lights and the like, can obtain different color changes through different electrochromic materials, and is expected to be applied to high-contrast unbiased-view displays. The structure and the preparation technology have great development potential and good application prospects.
Owner:HUAZHONG UNIV OF SCI & TECH

Quick-changing blue-light-resistant photochromic lens

InactiveCN112327515AAvoid the hassle of slow discolorationImprove the color change effectOptical partsPhotochromic lensColor changes
The invention discloses a quick-changing blue-light-resistant photochromic lens, which comprises a substrate body; the substrate body comprises a main substrate, a front photochromic substrate and a rear photochromic substrate, the front photochromic substrate is adhered to the center of the front side of the main substrate through shadowless glue, the front side surface and the rear side surfaceof the main substrate are the same and have a first curvature, and the front side surface of the front photochromic substrate has a second curvature, the first curvature being lower than the second curvature; the rear color-changing substrate is adhered to the rear side of the main substrate through shadowless glue, the surface of the rear side of the rear color-changing substrate has a third curvature, and the third curvature is smaller than the first curvature. According to the invention, the front color-changing substrate and the rear color-changing substrate are matched with each other, are respectively adhered to the front side and the rear side of the main substrate, and contain photochromic particles, so that the color-changing effect is enhanced under the action of the substrates,the color-changing efficiency is improved, and the trouble of slow color changing of the conventional lens is avoided.
Owner:SEE WORLD OPTICAL CO LTD

LED optical fiber color-changing vehicle glass

The invention relates to LED optical fiber color-changing vehicle glass, which comprises outer-layer glass, an organic film and inner-layer glass, wherein the organic film is attached to the outer surface of the inner-layer glass, an LED optical fiber color-changing film is clamped between the outer-layer glass and the organic film, and a graphene coating is arranged on the inner surface of the outer-layer glass. According to the invention, the color of the glass is automatically adjusted along with the intensity of external light, so that the harm of strong sunlight to a driver is reduced, and the good sight and the environment in an automobile are kept; and the glass is endowed with good demisting function through the graphene coating with excellent light transmission and capable of being heated.
Owner:李海斌

Nickel oxide nano hierarchical structure electrochromic capacitance material and preparation method thereof

The invention discloses a nickel oxide nano hierarchical structure electrochromic capacitance material and a preparation method thereof, the electrochromic material has a porous ultrathin nanosheet nanowire hierarchical structure, the average thickness of nanosheets is 10-20 nm, and the average diameter of nanowires is 5-7 nm. According to the invention, a one-step hydrothermal method is utilized to directly grow a porous ultrathin nanosheet nanowire hierarchical array on the surface of FTO conductive glass, so that the electrochromic capacitance material is prepared. According to the invention, the nickel oxide nanosheets are uniformly grown and distributed, the superfine nanowires are rooted on the surface of the nanosheet array, and the material has excellent visible light / infrared dual-band electrochromic performance, can realize rapid reversible conversion between transparency and black brown under different voltages, has excellent capacitive performance and shows a dual-function characteristic. The nickel oxide film with the nanoscale hierarchical structure can be used for novel intelligent display materials and intelligent color-changing energy storage materials such as electrochromic intelligent windows and mobile phone back shells.
Owner:HEFEI UNIV OF TECH

Polytungstate-hydrotalcite composite photochromic ultrathin film and preparation method thereof

The invention discloses polytungstate-hydrotalcite composite photochromic ultrathin film and a preparation method thereof and belongs to the technical field of inorganic composite photochromic materials. The preparation method includes the steps of preparing hydrotalcite stripped with formamide solvent; preparing polytungstate-superpolymer complex solution; and alternately assembling processed substrates with positive charge in the two solutions to obtain the polytungstate-hydrotalcite composite photochromic ultrathin film. The polytungstate-hydrotalcite composite photochromic ultrathin film is fine in photochromism, short in response time, fine in reversibility and high in chromic amplitude, and both chromic strength and thickness of the film can be precisely controlled by changing assembly times.
Owner:BEIJING TECHNOLOGY AND BUSINESS UNIVERSITY

A preparation method of screen-printed molybdenum-doped tungsten oxide nanostructure electrochromic film

The invention discloses a preparation method of an efficient color-changing silk-screen printing molybdenum-doped tungsten oxide nano-structure electrochromic film. According to the technical scheme,the method is characterized by comprising the following steps: dissolving tungstic acid in hydrogen peroxide, carrying out oil bath heating and stirring until a clear solution is obtained, adding molybdenum oxide, ethylene glycol and deionized water into the clear solution; then heating an oil bath pot, performing reflux condensation to obtain molybdenum-doped tungsten oxide nano sol, and outperforming centrifugation and washing the sol for later use; dissolving ethyl cellulose in ethanol at room temperature, stirring the mixture to obtain clear and transparent sol, adding terpilenol and the molybdenum-doped tungsten oxide nano sol prepared in the previous step into the sol, and carrying out rotary evaporation on an organic solvent to obtain molybdenum-doped tungsten oxide nano slurry; uniformly coating the molybdenum-doped tungsten oxide nano slurry on an ITO or FTO conductive glass substrate by adopting a silk-screen printing or blade coating method, then calcining the substrate byusing a muffle furnace and naturally cooling the substrate to obtain the molybdenum-doped tungsten oxide nano-structure electrochromic film.
Owner:JIEYANG HONGGUANG COATED GLASS +1

al with mosaic structure 2 o 3 /wo 3 Nanocomposite electrochromic film and preparation method thereof

The invention discloses a preparation method of an Al2O3 / WO3 nano composite electrochromic film having a mosaic structure. The preparation method comprises the following steps: 1) dissolving Al2O3 nanoparticle powder in water through ultrasonic dispersion to form an Al2O3 nanoparticle water solution; 2) adding ammonium metatungstate into the Al2O3 nanoparticle water solution, performing ultrasonic treatment to form a precursor composite solution; 3) adding ethanol and polyethyleneglycol into the precursor composite solution, and performing ultrasonic treatment to regulate the viscosity and surface tension of the solution; 4) preparing a wet film on a conductive substrate through a spin coating method or a pulling method or a spray coating method; and 5) performing heat treatment on the wet film in air to obtain the Al2O3 / WO3 nano composite electrochromic film. The invention also discloses the Al2O3 / WO3 nano composite electrochromic film prepared through the above method. The preparation method disclosed by the invention is simple, can easily realize film forming on various substrates of different shapes, is low in material consumption and is low in cost, thereby being suitable for industrial production.
Owner:ZHEJIANG UNIV

Preparation method of low-energy-consumption screen-printed molybdenum-doped tungsten oxide nano-structure electrochromic film

The invention discloses a preparation method of a low-energy-consumption screen-printed molybdenum-doped tungsten oxide nano-structure electrochromic film. According to the technical scheme, the method is characterized by comprising the following steps of: dissolving tungstic acid in hydrogen peroxide, performing oil bath heating and stirring until a clear solution is obtained, adding molybdenum oxide, ethylene glycol and deionized water into the clear solution, heating an oil bath pot, conducting reflux condensation to obtain a molybdenum-doped tungsten oxide nano sol, and conducting centrifugation and washing for standby use; dissolving ethyl cellulose in ethanol at room temperature, performing stirring to obtain a clear and transparent sol, adding terpilenol and the molybdenum-doped tungsten oxide nano sol prepared in the previous step into the sol, and carrying out rotary evaporation of an organic solvent to obtain a molybdenum-doped tungsten oxide nano slurry; and uniformly attaching the molybdenum-doped tungsten oxide nano slurry to an ITO or FTO conductive glass substrate by adopting a silk-screen printing or blade coating method, conducting calcining by using a muffle furnace, and performing natural cooling to obtain the low-energy-consumption screen-printed molybdenum-doped tungsten oxide nano-structure electrochromic film.
Owner:JIEYANG HONGGUANG COATED GLASS +1
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