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37results about How to "No obvious deformation" patented technology

Tungsten/transition layer/steel composite material and low-temperature and low-pressure active diffusion connection preparation method thereof

The invention relates to a tungsten / transition layer / steel composite material and a low-temperature and low-pressure active diffusion connection preparation method thereof, and belongs to the technical field of preparation of composite materials. Raw materials used for preparing the tungsten / transition layer / steel composite material comprise a tungsten substrate, an active metal Ti layer, a soft interface layer and a steel substrate. The method comprises the following steps: welding the soft interface layer and the steel substrate through a traditional welding process, sequentially superposing the obtained layer to the active metal Ti layer and the tungsten substrate, and carrying out vacuum diffusion connection to prepare a tungsten substrate / titanium layer / soft interface layer / steel substrate connecting piece which is the high-performance tungsten / steel composite material. The tensile strength of the composite material is greater than or equal to 386MPa. The composite material has a reasonably designed structure, and the problems of large joint residual stress, low strength and high requirements of welding conditions of present tungsten / steel connecting pieces are solved through matching of the structure with the method. The preparation method is simple, and is convenient for industrial application.
Owner:CENT SOUTH UNIV

High-performance tungsten/steel composite material based on high-temperature application and preparation method thereof

The invention relates to a high-performance tungsten / steel composite material based on high-temperature application and a preparation method thereof and belongs to the technical field of preparation of composite materials. By adoption of the high-performance tungsten / steel composite material, the problems of large residual joint stress, low strength, poor heat resistance and high connection temperature in an existing tungsten / steel connector are solved. The high-performance tungsten / steel composite material is prepared from a tungsten-based layer, a titanium layer, a niobium layer, a nickle layer and a steel-based layer which are arranged in sequence and prepared by adopting a welding method. The high-performance tungsten / steel composite material is obtained by superposing the tungsten-based layer, the titanium layer, the niobium layer, the nickle layer and the steel-based layer in sequence according to the superposition mode of the tungsten-based layer, the titanium layer, the niobium layer, the nickle layer and the steel-based layer and carrying out vacuum diffusion bonding. The high-performance tungsten / steel composite material has the advantages that the room-temperature tensile strength is larger than or equal to 352MPa, and the tensile strength at the temperature of 650DEG C is larger than or equal to 338MPa; the structure design is reasonable, the process is simple, the large-scale application is convenient, and simultaneously, the high-performance tungsten / steel composite material can be widely applied in diffusion bonding of refractory metal and other dissimilar metal materials.
Owner:CENT SOUTH UNIV

Aluminum-based density gradient material and preparation method and application thereof

The invention relates to an aluminum-based density gradient material and a preparation method and application thereof. A region with density in gradient change and (or) a region with density in continuous change exist in the aluminum-based density gradient material, and the materials of all the regions in the aluminum-based density gradient material are consistent. The preparation method comprises the following steps: water-soluble pole-forming agent powder and aluminum alloy powder are proportioned according to the volume ratio of the water-soluble pole-forming agent powder to the aluminum alloy powder being X to (100-X), and then are mixed uniformly to obtain mixed powder containing different amounts of pole-forming agents; die forming is carried out on laminated spread powder, and a prefabricated blank is sintered in a vacuum environment at 575-675 DEG c to obtain a sintered body; and water soaking treatment is carried out to obtain the aluminum-based density gradient material. The aluminum-based density gradient material prepared by the method has no obvious deformation, and the density from 1.1 g / cm<3>-2.7g / cm<3> in gradient distribution is achieved through adjusting porosity; and the aluminum-based density gradient material is excellent in performance and is suitable for being used as an aerospace material.
Owner:CENT SOUTH UNIV

Simultaneous monitoring device for femtosecond laser micromachining

A simultaneous monitoring device for femtosecond laser micromachining comprises a femtosecond laser, wherein two parallel holophotes, an attenuation piece, a polarizing film, a beam splitter prism, two diaphragms, a shutter, a focusing lens and a machining object are sequentially arranged along a femtosecond laser light path outputted by the femtosecond laser. The machining object is fixed on a rotating translation device, and the centers of the diaphragms and the vertical central line of the machining object are on the same plane. An L-type support is further fixed on the rotating translation device, and the L-type support is provided with a CCD for monitoring. The rotating translation device, the CCD and the L-type support are all connected with a computer through signal lines. The beam splitter prism divides femtosecond laser into two light beams having completely same energy, one light beam is used for machining along the femtosecond laser light path, and the other light beam enters a power meter along the other light path to measure the energy of the femtosecond laser. Real-time simultaneous monitoring for changes generated on the surface of the machining object is achieved, and errors caused by multimetering are reduced. The two diaphragms are the same in height and collinear, and the light beams are kept fixed.
Owner:BEIJING UNIV OF TECH

Low-viscosity 3D (three-dimensional) printing photo-curing material

The invention discloses a low-viscosity 3D (three-dimensional) printing photo-curing material. The low-viscosity 3D printing photo-curing material comprises, by weight, 60-75 parts of urethane acrylate, 15-25 parts of polyethylene glycol, 25-40 parts of cationic monomers, 0.5-2 parts of initiators, 2.5-4 parts of accelerators and 0.5-2 parts of auxiliaries. The density of the urethane acrylate at the temperature of 25 DEG C is 1.09 g / cm<3>, the viscosity of the urethane acrylate is 150-175 mPs.s, and surface tension of the urethane acrylate is 39.5-39.1 mN / m under the condition that the working temperatures of sprayers are 50-55 DEG C in 3D printing procedures; the accelerators are added into the cationic monomers when materials are prepared, the low-viscosity 3D printing photo-curing material can be used after the accelerators and the cationic monomers are uniformly mixed with one another, and a mass ratio of the cationic monomers to the accelerators is 10:1. The low-viscosity 3D printing photo-curing material has the advantages that reactive diluents can be omitted, and the low-viscosity 3D printing photo-curing material is high in photo-curing speed; the low-viscosity 3D printing photo-curing material is good in mechanical property after being photo-cured, and the relative cost of the low-viscosity 3D printing photo-curing material can be reduced.
Owner:SUZHOU BC TECH

Forming method of variable cross section special-shaped single tube of thrust chamber body of liquid-propellant rocket engine

The invention discloses a forming method of a variable cross section special-shaped single tube of a thrust chamber body of a liquid-propellant rocket engine. The method comprises the following stepsthat (1), bend shaping is conducted, specifically, a single tube workpiece in the annealing state and filled with filling materials is placed in a bend shaping tool for bend shaping machining, so thatthe workpiece can be bent along an inner molding surface curve of a theoretical single tube; (2) preforming is conducted, specifically, the single tube workpiece is placed in a preforming tool of a hinge pressing plate structure, the preforming tool is adopted to press the single tube workpiece in an oblateness shape with plane included angles of two sides being the same as the theoretical singletube; (3), hydraulic bulging is conducted, specifically, an internal high pressure forming mold with a high pressure forming inner cavity being completely attached to the outer surface of the theoretical single tube is adopted to apply high pressure from the interior of the single tube workpiece to the outside to conduct bulging; (4), annealing is conducted and the single tube workpiece is back into the annealing state; and (5), the step (3) and the step (4) are repeated until the single tube workpiece is completely attached to the wall surface of the high pressure forming inner cavity, and asingle tube finished product is obtained. Machining accuracy and yield of single tube products can be obviously improved with the method.
Owner:湖北三江航天江北机械工程有限公司

Pressure cavity structure for comprehensive dielectric property measurement under high pressure and measurement method thereof

The invention relates to a pressure cavity structure for comprehensive dielectric property measurement under high pressure and a measurement method thereof. The pressure cavity structure comprises a ceramic ring, a die steel sleeve, a basalt fiber sleeve and an anti-expansion protection steel sleeve. The anti-expansion protective steel sleeve is arranged on the outer side of the basalt fiber sleeve in a sleeving manner; a through hole is formed in the basalt fiber sleeve; the side wall of the through hole is connected with the ceramic ring and the die steel sleeve, the lower end of the ceramicring is supported by the side wall of the through hole, the upper end of the ceramic ring is connected with the die steel sleeve, the pressure cavity structure is provided with a low-pressure hole and a high-pressure hole, and the low-pressure hole and the high-pressure hole penetrate through the through hole in the basalt fiber sleeve from the outer side of the pressure cavity structure. Compared with the prior art, the pressure cavity structure can bear higher pressure and can be used for measuring various dielectric properties and has the advantages of convenience in measurement, firmness,reliability, low manufacturing cost and the like.
Owner:TONGJI UNIV +2

Universal method for preparing nitrogen-doped graphene by recycling metal salt through 3d printing

The invention discloses a universal method for preparing nitrogen-doped graphene by recycling metal salt through 3d printing, and belongs to the technical field of energy and environmental materials. Firstly, a double-helix structure template is designed through computer software; the preparation method comprises the following steps: firstly, preparing a metal salt, then mixing and stirring metal salt, Variquat CC 42NS, hexanediol diacrylate, ethoxylated trimethylolpropane triacrylate and diphenyl-(2, 4, 6-trimethylbenzoyl) phosphorus oxide to obtain uniform metal salt resin, and then printing the metal salt resin into a double-helix structure by adopting a digital light processing technology; sintering in air to obtain a metal oxide template; heating and reacting the metal oxide template to obtain a metal template; heating and reacting the metal template, and removing the metal template by using dilute acid; cleaning the obtained graphene with deionized water, and then drying to obtain nitrogen-doped graphene; the excellent mechanical property of the composite material is about 16000 times of load of the weight of the composite material without obvious deformation. And under the conditions that the compression is 75% and the compression strength is 100kpa, circulation is performed for 100 times, and the structure is kept.
Owner:NORTHWESTERN POLYTECHNICAL UNIV

Preparation and application of a polymer vesicle hydrogel drug carrier

The invention discloses preparation and application of a high-molecular vesicle hydrogel drug carrier. The preparation method comprises the following steps of preparing a high-molecular polymer solution, preparing a high-molecular vesicle solution, preparing high-molecular vesicle composite hydrogel and loading a drug into the high-molecular vesicle composite hydrogel. According to the preparation and application of the high-molecular vesicle hydrogel drug carrier, a macromolecule and monomer pair method is used for assembling high-molecular vesicles, the assembled high-molecular vesicles are composed of two parts, the first part is biomacromolecules with sulfonate radicals and carboxylate radicals, and the second part is poly(2-(diethylamino)ethyl methacrylate) with tertiary amino; an aqueous solution containing the high-molecular vesicles is mixed with hydroxyethyl methacrylate monomers, a photoinitiator I2959 is added for initiated polymerization, the composite hydrogel drug carrier is formed, and the drug is loaded into the hydrogel drug carrier in an adsorption mode. Meanwhile, the invention discloses application of the high-molecular vesicle hydrogel drug carrier in medicament for the eyes, and good drug controlled-release capacity is embodied.
Owner:湖南知时生物科技有限公司

A kind of tungsten/steel composite material based on high temperature application and its preparation method

The invention relates to a high-performance tungsten / steel composite material based on high-temperature application and a preparation method thereof and belongs to the technical field of preparation of composite materials. By adoption of the high-performance tungsten / steel composite material, the problems of large residual joint stress, low strength, poor heat resistance and high connection temperature in an existing tungsten / steel connector are solved. The high-performance tungsten / steel composite material is prepared from a tungsten-based layer, a titanium layer, a niobium layer, a nickle layer and a steel-based layer which are arranged in sequence and prepared by adopting a welding method. The high-performance tungsten / steel composite material is obtained by superposing the tungsten-based layer, the titanium layer, the niobium layer, the nickle layer and the steel-based layer in sequence according to the superposition mode of the tungsten-based layer, the titanium layer, the niobium layer, the nickle layer and the steel-based layer and carrying out vacuum diffusion bonding. The high-performance tungsten / steel composite material has the advantages that the room-temperature tensile strength is larger than or equal to 352MPa, and the tensile strength at the temperature of 650DEG C is larger than or equal to 338MPa; the structure design is reasonable, the process is simple, the large-scale application is convenient, and simultaneously, the high-performance tungsten / steel composite material can be widely applied in diffusion bonding of refractory metal and other dissimilar metal materials.
Owner:CENT SOUTH UNIV

Forming method of variable cross-section special-shaped single tube for thrust chamber of liquid rocket engine

The invention discloses a forming method of a variable cross section special-shaped single tube of a thrust chamber body of a liquid-propellant rocket engine. The method comprises the following stepsthat (1), bend shaping is conducted, specifically, a single tube workpiece in the annealing state and filled with filling materials is placed in a bend shaping tool for bend shaping machining, so thatthe workpiece can be bent along an inner molding surface curve of a theoretical single tube; (2) preforming is conducted, specifically, the single tube workpiece is placed in a preforming tool of a hinge pressing plate structure, the preforming tool is adopted to press the single tube workpiece in an oblateness shape with plane included angles of two sides being the same as the theoretical singletube; (3), hydraulic bulging is conducted, specifically, an internal high pressure forming mold with a high pressure forming inner cavity being completely attached to the outer surface of the theoretical single tube is adopted to apply high pressure from the interior of the single tube workpiece to the outside to conduct bulging; (4), annealing is conducted and the single tube workpiece is back into the annealing state; and (5), the step (3) and the step (4) are repeated until the single tube workpiece is completely attached to the wall surface of the high pressure forming inner cavity, and asingle tube finished product is obtained. Machining accuracy and yield of single tube products can be obviously improved with the method.
Owner:湖北三江航天江北机械工程有限公司

A kind of tungsten/transition layer/steel composite material and its preparation method of low temperature and low pressure active diffusion connection

The invention relates to a tungsten / transition layer / steel composite material and a low-temperature and low-pressure active diffusion connection preparation method thereof, and belongs to the technical field of preparation of composite materials. Raw materials used for preparing the tungsten / transition layer / steel composite material comprise a tungsten substrate, an active metal Ti layer, a soft interface layer and a steel substrate. The method comprises the following steps: welding the soft interface layer and the steel substrate through a traditional welding process, sequentially superposing the obtained layer to the active metal Ti layer and the tungsten substrate, and carrying out vacuum diffusion connection to prepare a tungsten substrate / titanium layer / soft interface layer / steel substrate connecting piece which is the high-performance tungsten / steel composite material. The tensile strength of the composite material is greater than or equal to 386MPa. The composite material has a reasonably designed structure, and the problems of large joint residual stress, low strength and high requirements of welding conditions of present tungsten / steel connecting pieces are solved through matching of the structure with the method. The preparation method is simple, and is convenient for industrial application.
Owner:CENT SOUTH UNIV

Device and method for preparing wear-resistant and anti-rust coating on inner wall of pipe

The invention discloses a device and a method for preparing wear-resistant and rust-proof coatings on the inner walls of large-diameter pipes. The device comprises a to-be-sprayed matrix tube externally sleeved with an energy absorption tube, a lining tube is arranged in the to-be-sprayed matrix tube, an annular explosive loading layer is wound around the external surface of the lining tube, a tapered slot is carved on the surface of the annular explosive loading layer, to-be-sprayed powder is filled in the annular explosive loading layer, and the to-be-sprayed powder is composed of 70-80 parts by weight of WC-Co composite powder and 20-30 parts by weight of a gas generating agent. After one end of the annular explosive loading layer is detonated by a detonating device, the to-be-sprayed powder is driven by explosion to impact the inner wall of the to-be-sprayed matrix tube at a high speed, so that a wear-resistant and rust-proof coating is formed on the internal surface of the to-be-sprayed matrix tube. Compared with conventional methods, a hard wear-resistant and rust-proof coating prepared according to the device and method disclosed by the invention has the characteristics of good bonding strength, low porosity, high hardness, wear resistance, rust prevention, and the like, and can raise the strength of body materials; and a good hard wear-resistant and rust-proof coating can be obtained on the inner wall of a large-diameter pipe.
Owner:ZHONGBEI UNIV

Synchronous monitoring device for femtosecond laser micromachining

A simultaneous monitoring device for femtosecond laser micromachining comprises a femtosecond laser, wherein two parallel holophotes, an attenuation piece, a polarizing film, a beam splitter prism, two diaphragms, a shutter, a focusing lens and a machining object are sequentially arranged along a femtosecond laser light path outputted by the femtosecond laser. The machining object is fixed on a rotating translation device, and the centers of the diaphragms and the vertical central line of the machining object are on the same plane. An L-type support is further fixed on the rotating translation device, and the L-type support is provided with a CCD for monitoring. The rotating translation device, the CCD and the L-type support are all connected with a computer through signal lines. The beam splitter prism divides femtosecond laser into two light beams having completely same energy, one light beam is used for machining along the femtosecond laser light path, and the other light beam enters a power meter along the other light path to measure the energy of the femtosecond laser. Real-time simultaneous monitoring for changes generated on the surface of the machining object is achieved, and errors caused by multimetering are reduced. The two diaphragms are the same in height and collinear, and the light beams are kept fixed.
Owner:BEIJING UNIV OF TECH

A photolithographic method for preventing silicon wafer from warping

The invention discloses a photoetching method capable of preventing a silicon wafer from being warped. The photoetching method comprises the following steps of cleaning the silicon wafer, evenly spreading front glue, prebaking, exposing, developing, drying, evenly spreading glue at the edge of the front side of the silicon wafer, evenly spreading glue on the back side of the silicon wafer, hardening and corroding. A circle of photoetching glue is evenly spread on the periphery of a figure face after photoetching procedure developing, so that the position of the circle which is coated by the glue is prevented from being corroded, no small notch is formed at the edge of the silicon wafer, and trouble in operation of blade coating glass slurry is avoided; meanwhile, the edge of the silicon wafer is not corroded, so that the mechanical strength of the silicon wafer is improved to a certain extent; furthermore, the uncorroded surface of the circle can reduce effects of glass shrinkage stress on a shape of the silicon wafer in glass shaping; after the glass is shaped, the silicon wafer has no obvious deformation, the surface of the silicon wafer is flat, and operation of following-up procedures is not prone to generating fragments.
Owner:CHINA ZHENHUA GRP YONGGUANG ELECTRONICS CO LTD STATE OWNED NO 873 FACTORY
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