The invention discloses a method for manufacturing
tungsten /
cobalt carbide composite
powder with a
nanostructure. The method includes steps of firstly, dissolving, by
mass, 55-92% of water-soluble
tungsten salt, 3-40% of water-soluble
cobalt salt, 3-6% of water-soluble
carburizing and nodulizing agents and 0.1-2% of water-soluble composite
grain growth inhibitors into water with the
mass 3-5 times that of a mixture of the water-soluble
tungsten salt, the water-soluble
cobalt salt, the water-soluble
carburizing and nodulizing agents and the water-soluble composite
grain growth inhibitors to prepare mixed
aqueous solution; secondly, quickly crystallizing the mixed
aqueous solution obtained in the first step; thirdly, pre-treating crystalline, which is obtained in the second step, at the pretreatment temperature
ranging from 500 DEG C to 700 DEG C to obtain nodular
powder; and fourthly, performing reduction synthesis and carbon conditioning for
powder materials, which are obtained in the third step, at the temperature
ranging from 900 DEG C to 1000 DEG C to manufacture tungsten /
cobalt carbide composite powder materials with nanostructures. The method has the advantages that a process is simple, and the hard
alloy powder materials with the nanostructures can be produced in an industrialized manner.