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69 results about "Galaxolide" patented technology

Galaxolide (trade name; also known as Abbalide, Pearlide, Astrolide, Musk 50, Polarlide; chemical name 1,3,4,6,7,8-hexahydro-4,6,6,7,8,8,-hexamethyl-cyclopenta[g]benzopyran or HHCB) is a synthetic musk with a clean sweet musky floral woody odor used in fragrances. It is one of the musk components that perfume and cologne manufacturers use to add a musk odor to their products. Galaxolide was first synthesized in 1965, and used in the late 1960s in some fabric softeners and detergents. High concentrations were also incorporated in fine fragrances.

Method for preparing galaxolide under catalysis of superfine aluminum trichloride

The invention relates to a method for preparing galaxolide under catalysis of superfine aluminum trichloride. The method is characterized by comprising the following steps: 1, adding pentamethyl indanand anhydrous aluminum trichloride with particle size of 5 meshes or blow to a solvent, and cooling the solution to subzero 30-subzero 20 DEG C, wherein the mass ratio of the pentamethyl indan to anhydrous aluminum trichloride is (1.5-2):1; 2, dropwise adding propylene oxide to dissolve in the solution in the solvent during stirring, and conducting a reaction at subzero 30-subzero 5 DEG C for 1-2h to produce hexamethyl indanol, wherein the mass ratio of the propylene oxide to pentamethyl indan is (0.3-0.5):1; 3, continuously adding a deactivating agent and formaldehyde or formaldehyde equivalents, heating the mixture to 5-65 DEG C to react for 0.5-4 h to produce galaxolide, wherein the molar ratio of the deactivating agent, the formaldehyde or formaldehyde equivalents to the pentamethylindan is (1-2):1 and (0.5-1):1; and 4, performing purification. The method has the advantages as follows: aluminum trichloride powder with superfine particle size is used, the raw material conversionrate and product yield are significantly increased, the reaction time is shortened, the reaction has good reproducibility, energy is saved, production efficiency is improved, and the production cost is reduced.
Owner:ANHUI JINGHE IND

Method For Selecting Perfume Ingredient, Method For Formulating Fragrance, And Preference-Enhancing Agent

The present invention provides a method for selecting a perfume ingredient that can enhance a preference therefor by continuous use from among arbitrary perfume ingredients; a perfume composition and a preference-enhancing agent that can give a high preference therefor and enhance the preference by continuous use; and a hair cleanser that can offer excellent use texture and improve the use texture by continuous use.
A method for selecting a perfume ingredient comprising; conducting the following evaluation (A) and/or (B) on arbitrary perfume ingredients and making a selection with the evaluation result as an indicator:
  • (A) an evaluation of an impression of the “density” of a fragrance on first exposure and an evaluation of an impression of the “density” of the fragrance after two or more exposures; and
  • (B) an evaluation of an impression of the “cheerfulness” of a fragrance on first exposure and an evaluation of an impression of the “cheerfulness” of the fragrance after two or more exposures. A perfume composition comprising a perfume ingredient selected by the method for selecting a perfume ingredient.
A hair cleanser comprising (i) an amphoteric surfactant, (ii) a cationic polymer, (iii) an N-acyl-N-methyltaurine-based anionic surfactant, and (iv) one or more selected from the group consisting of galaxolide, ambroxan, manzanate, grapefruit oil, marjoram oil, cinnamon oil, aurantiol, tomato leaf extract, spearmint oil, clove oil, chamomile oil, pepper oil, Triplal, Yuzu citron (Citrus junos) oil, octylaldehyde, vanillin, jasmine oil, bergamot oil, armoise oil, strawberry extract, geranium oil, lime oil, nutmeg oil, and allyl caproate.
Owner:SHISEIDO CO LTD

Osmanthus flower essence for water-based ink and preparing method of osmanthus flower essence

The invention relates to osmanthus flower essence for water-based ink. The osmanthus flower essence for the water-based ink consists of the following ingredients in percentage by weight: 1 to 30 percent of osmanthus flower essence, 5 to 55 percent of composite modified oligosaccharide and deionized water, wherein the osmanthus flower essence consists of beta-ionone, dihydro-beta-ionone, linalool, alpha-jasminolene, alpha-amyl cinnamic aldehyde, isoamyl salicylate, benzyl salicylate, benzyl benzoate, galaxolide, citronellol, geraniol, cinnamyl alcohol, cognac oil, tetradecyl aldehyde, para-mentha-8-thiolone with the mass percent concentration being 1 percent, terpilenol, methyl anthranilate, osmanthus flower extracts and ethyl alcohol. The invention also provides a preparing method of the osmanthus flower essence for the water-based ink. The composite modified oligosaccharide is used as a wall material; the osmanthus flower essence is coated to form nanocapsule slow-release essence, so that the fragrance retention and the water solubility of the essence are improved; the preparing method is applicable to the perfuming of the water-based ink. The osmanthus flower essence for the water-based ink has the advantages that the fragrance is exquisite; the natural feeling is high; the fragrance retention is durable.
Owner:SHANGHAI INST OF TECH

Treatment method of recycled pentamethyl indane

The invention relates to a treatment method for recovering pentamethyl indane in galaxolide production. The treatment method comprises the following steps: adding a certain amount of ferrous sulfate into a recovered pentamethyl indane solution, and slowly and dropwise adding a certain amount of concentrated sulfuric acid to provide an acidic environment; after the concentrated sulfuric acid is dropwise added, controlling a certain temperature, dropwise adding hydrogen peroxide and carrying out Fenton oxidation reaction; after dropwise adding is completed, carrying out heating to a certain temperature to continue the reaction, and after the reaction is completed, conducting standing for layering and separating out lower-layer acid water; adding excessive alkaline water into an upper-layer pentamethyl indane phase for neutralization; and after neutralization is completed, separating out lower-layer alkaline water to obtain treated pentamethyl indane. According to the method, the conversion rate of pentamethyl indane is increased, production cost is reduced, production efficiency is greatly improved, the reaction efficiency and the material utilization rate of the whole production process are optimized, and the economic benefits of enterprises are increased.
Owner:安徽金轩科技有限公司
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