The application belongs to the technical field of two-dimensional
transition metal nanomaterial post-
processing, and particularly discloses a Ti3C2T x The
microwave annealing method for film strengthening and
toughening comprises the following steps: Ti3AlC2 is treated by physical and
chemical reaction to obtain a
titanium carbide suspension, and then vacuum-assisted
filtration drying is performed to obtain Ti3C2T x Film; the prepared Ti3C2T x Film sample is placed in a
microwave reaction cavity;
inert protective gas is introduced into the
microwave reaction cavity, and the gas in the reaction cavity is discharged until the air in the cavity is completely discharged; the microwave loading power is adjusted to perform
microwave annealing on the
titanium carbide film, the total length of the loaded
microwave power is controlled, and the power loading period and the power stopping period in each cycle are controlled to obtain Ti3C2T x Film with low defect density, compactness and high strength and
toughness. The annealing device for microwave heating has the characteristics of rapid heating and
high energy transmission, can greatly shorten the time required by the annealing process, improve the production efficiency, and can reduce the generation of
temperature gradient and thermal stress.