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65 results about "Microwave annealing" patented technology

Solid-state microwave annealing is an attractive method for rapid thermal annealing of implanted SiC. Using this technique, annealing temperatures as high as 2100 °C can be reached with a ramp-up rate of 600 °C/s and afall rate of 400 °C/s.

Method for low-temperature preparation of two-dimensional flexible ion-sensitive field effect transistor

The invention belongs to the technical field of manufacturing of electrochemical sensor devices and particularly discloses a method for low-temperature preparation of a two-dimensional flexible ion-sensitive field effect transistor. The method includes: taking a flexible material as a substrate, depositing a graphic metal layer on the substrate to serve as a back electrode, growing an insulating oxide layer on the back electrode, and transferring a two-dimensional semiconductor film on the insulating medium layer to serve as a conductive channel of a device; forming graphic metal layers on the two-dimensional semiconductor film to serve as source and drain regions of the device; depositing a functional layer material above a channel area. By a microwave annealing process for low-temperature treatment, on the one hand, interface characteristics of layers of the device can be improved so as to eliminate delaying and drifting caused by interface defects; on the other hand, by the aid of the microwave absorption function of the functional layer material and a nano-structure functional layer at an interface of the two-dimensional semiconductor film, applicability to sensing detection in different scenes can be realized. The microwave annealing process has advantages of quickness, low thermal budget, short manufacturing period, low cost and the like.
Owner:FUDAN UNIV

Method for forming nickel silicide with microwave annealing

The invention discloses a method for forming nickel silicide with microwave annealing. The method comprises the following steps of: pre-cleaning the surface of exposed silicon for removing natural oxide; depositing nickel or nickel alloy and coating a layer of barrier layer on the surface of the nickel or nickel alloy; utilizing microwave radiation so that a part of the nickel or nickel alloy is reacted with the silicon to form high-resistance one-silication two-nickel in the process of heating a wafer to a first temperature at the same time; removing the barrier layer of the surface of the nickel or nickel alloy and unreacted nickel or nickel alloy; and utilizing microwave radiation so that the high-resistance one-silication two-nickel is changed to low-resistance nickle silicide in the process of heating the wafer to a second temperature at the same time. In the method, the surface of a silicon wafer is radiated by utilizing the microwave during heating at the same time, therefore, the activity of atomic motion is improved, and atomic realignment is promoted. The first temperature for heating is reduced so that the first step of diffusion of nickel is limited. The activity of the atomic motion is improved on the basis of the second temperature, therefore, the atomic realignment is promoted, the uniformity of the nickle silicide is helped to be improved, and the performance of devices is improved.
Owner:SHANGHAI HUALI MICROELECTRONICS CORP

Method of preparing GOI at low temperature by microwave annealing technology

The invention provides a method of preparing GOI at low temperature by a microwave annealing technology. The method at least includes the following steps: providing a substrate and sequentially forming a doped layer and a first Ge layer on the substrate through an epitaxial mode; conducting ion implantation to enable ions to be implanted into the bottom surface of the doped layer below a preset depth; and providing a substrate with an insulating layer on the surface, making the substrate bond with the first Ge layer to form a bonding pad, conducting microwave annealing so that doped layer adsorption ions form micro-cracks and are separated from the bottom surface, and finally obtaining Germanium On Insulator. GOI is prepared through adsorption, peeling and bonding of the doped layer. Microwave annealing is performed on the bonding pad, and during the microwave annealing process, the local temperature of an interface between the doped layer and the substrate is high to cause peeling while the overall temperature of the bonding pad is low. Therefore, doped ions are not liable to be diffused in the first Ge layer, and the low temperature will not have an adverse influence on the first Ge layer and other layers. In this way, preparation of high-quality GOI is facilitated.
Owner:SHANGHAI INST OF MICROSYSTEM & INFORMATION TECH CHINESE ACAD OF SCI

Method of preparing material-over-insulator through adsorption and peeling

The invention provides a method of preparing a material-over-insulator through adsorption and peeling. The method comprises the following steps: providing a substrate, and sequentially forming a doped single crystalline layer, a superlattice structural layer and a to-be-transferred layer on the substrate through an epitaxial mode; conducting ion implantation to enable ions to be implanted into the bottom surface of the doped single crystalline layer below a preset depth; and providing a substrate with an insulating layer on the surface, making the substrate bond with the to-be-transferred layer to form a bonding pad, conducting microwave annealing so that doped layer adsorption ions form micro-cracks and are separated from the bottom surface, and finally obtaining a material-over-insulator. The material-over-insulator is prepared through adsorption, peeling and bonding of a doped layer. The doped layer is formed by laminating a doped single crystalline layer and a non-doped or low-doped superlattice structural layer. The superlattice structural layer enhances the ion adsorption capability of the doped single crystalline layer to enable adsorption and peeling of the doped single crystalline layer with low-doped concentration, and the low-doped concentration enables the probability of diffusion of doped ions into the to-be-transferred layer to be reduced. In this way, the quality of the to-be-transferred layer is guaranteed.
Owner:SHANGHAI INST OF MICROSYSTEM & INFORMATION TECH CHINESE ACAD OF SCI

Preparation method and application of hydrophobic graphene aerogel

The invention discloses a preparation method and application of hydrophobic graphene aerogel. The invention belongs to the field of graphene aerogel. The problems that an existing hydrophobic grapheneaerogel material is high in preparation cost, poor in structural strength and the like can be solved. A hydrothermal reaction method is adopted, a saccharide cross-linking agent which is low in priceand easy to obtain is adopted, an organic auxiliary agent and efficient and cheap modifiers such as trimethylchlorosilane are added, and the hydrophobic and oleophylic graphene aerogel material is obtained through a normal-pressure drying method and a microwave annealing method. It can be seen through scanning electron microscope imaging that the material is structurally a thin-wall porous material formed by three-dimensional crosslinking of thin-layer graphene. The material is definite in synthesis process, short in synthesis time, low in cost, free of heavy metal and organic pollutants, high in structural strength and capable of bearing the heavy pressure which is more than one hundred times of the mass of the material. The material has super-hydrophobicity, and the contact angle measured by experiments is as high as 150 degrees or above. The hydrophobic graphene aerogel can be used in the fields of protection and removal of volatile organic compounds in air and water, and other oil-water separation applications.
Owner:SHANXI DATONG UNIV +1

Low-temperature microwave annealing method for improving optical-electrical characteristic of silicon superlattice film

The invention discloses a low-temperature microwave annealing method for improving the optical-electrical characteristic of a silicon superlattice film. The low-temperature microwave annealing methodcomprises the specific steps that 1, before annealing, inertia gas is introduced into a microwave annealing cavity in advance, so that a pure inertia atmosphere is formed in the cavity; 2, the inertiagas continues being introduced to serve as an annealing atmosphere, the silicon superlattice film is put into the middle of the microwave annealing cavity, the annealing power and the maximum temperature in the annealing process are set, the annealing time with the corresponding duration is set, and microwave annealing is started, wherein the maximum temperature in the annealing process is 300-500 DEG C; and 3, after microwave annealing and after natural cooling of the temperature in the cavity, the modified and optimized silicon superlattice film is obtained. The low-temperature microwave annealing method is high in reliability and repeatability, the finished product rate of the modified and optimized silicon superlattice film prepared through the low-temperature microwave annealing method is high, and the method with guiding significance is provided for low-temperature annealing of the silicon superlattice film.
Owner:FUDAN UNIV

Method for preparing silicon quantum dot films through microwave annealing

The invention relates to a method for preparing silicon quantum dot films through microwave annealing. Specifically, magnetron-sputtering-deposited silicon-rich silicide films are placed in a microwave annealing furnace for annealing at the lower temperature, and the uniform silicon quantum dot films are prepared. The method is good in controllability, high in repeatability, simple, effective and high in operability due to adoption of reliable magnetron co-sputtering and microwave annealing technologies. According to the main technical scheme, the method comprises steps as follows: firstly, magnetron co-sputtering is performed on Si targets and SiO2 (or Si3N4 or SiC) targets through Ar ions, sputtering power of all the targets is optimized, and silicon-rich silicide films are deposited on monocrystalline silicon and quartz substrates; then silicon quantum dots are formed through annealing treatment at the temperature of 700-900 DEG C in a nitrogen atmosphere or an argon atmosphere by the aid of microwave annealing equipment. Compared with traditional methods for growing silicon quantum dots through tube furnace annealing or rapid photo-thermal annealing, the method has the advantages that the annealing temperature is decreased, the process is simple and the cost is low. The method is applicable to the field of a new generation of high-efficiency solar cells.
Owner:YUNNAN NORMAL UNIV
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