The invention discloses an in-situ X-
ray scattering characterization method for a volatilization-induced dynamic process and a liquid sample
cell, and belongs to the technical field of liquid X-
ray scattering experiments. A liquid
sample pool with a conical front end and a detection area and a volatilization opening is prepared by drawing a capillary tube through program-controlled
laser, a liquid sample is injected into the liquid
sample pool, and the rear end of the liquid
sample pool is sealed; then in-situ X-
ray scattering monitoring is conducted on the detection area in the sample volatilization process, so that sample dynamic structure evolution information is obtained. Different from an existing liquid sample
cell which is completely sealed or approximately completely sealed, the continuous in-situ characterization of the liquid sample under the limited volatilization condition is realized by reserving the volatilization opening with the preset size. The method is simple in preparation and low in cost, the sample
pool can be repeatedly loaded and sealed again, and the method is compatible with laboratory X-ray scattering equipment and a
synchrotron radiation X-ray scattering platform and is suitable for dynamic structure research of a
liquid system and a soft
material system in the volatilization induction process.