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51results about How to "Enhanced hydrophobic association" patented technology

Temperature-resistant salt-resistant efficient gel, and preparation and use thereof

The invention discloses a temperature resistant salt tolerant high efficiency gel and a preparation method and application thereof. The preparation method is characterized in that the preparation method comprises the following steps: preparing a comb-shaped associated copolymer PAH containing macromonomers and functional hydrophobic monomers into an aqueous solution having the concentration of 0.1 to 4g / L, the crosslinking agent concentration of 0.01 to 1.0g / L, the surfactant concentration of 0.01 to 8mmol / L and the sodium sulfite thermal stabilizer concentration of 0.005 to 1.0g / L; adding the aqueous solution into a mixing container with a stirring device; stirring the aqueous solution evenly at the room temperature; regulating the pH value of the solution to be equal to between 4 and 11, and obtaining a temperature resistant salt tolerant high efficiency gel polymer solution system used for tertiary oil recovery and scavenge, displacement modification, profile modification or water shutoff. The polymer solution system has micro-crosslinking to form the gel during the flowage inside the oil reservoir. The gel has good elasticity, not easy dehydration, stable gelling performance, and excellent tackification, temperature resistance, salt tolerance, shearing resistance and ageing resistance.
Owner:CHENGDU UNIVERSITY OF TECHNOLOGY

Acrylic amide modified polymer micro-crosslinking gel and preparation thereof

The invention discloses acrylamide modified polymer micro-crosslinking gel and a preparation method thereof. The preparation method is characterized in that the method comprises the following steps that: acrylamide modified polymer PAE containing functional macro monomer is prepared into an aqueous solution with the concentration between 0.1 and 4g / L, the concentration of crosslinking agent between 0.01 and 1.0g / L, the concentration of surface active agent between 0.01 and 8mmol / L and the concentration of heat stabilizer sodium sulfite between 0.005 and 1.0g / L; the aqueous solution is added in a mixing container with a stirring device and is stirred evenly at room temperature; the pH value of the solution is adjusted between 4 and 11 to prepare a polymer solution system of the acrylamide modified polymer micro-crosslinking gel used for tertiary oil recovery and displacement, oil displacement modification, profile modification or water plugging; and the polymer solution system undergoes micro crosslinking during flowing inside an oil layer to form the gel. The acrylamide modified polymer micro-crosslinking gel has ideal elasticity, difficult dehydration, stable performance and excellent performances on tackifying, temperature resistance, salt resistance, shearing resistance and ageing resistance.
Owner:CHENGDU UNIVERSITY OF TECHNOLOGY

Polyurethane associated thickener, and preparation method and application thereof

The invention discloses a polyurethane associated thickener, and a preparation method and application thereof. The preparation method comprises the following steps: adding polyether polyol and methylbenzene to a reaction container under protection of nitrogen, heating up to 110-130 DEG C, and drying and dewatering in vacuum for 2-4 hours; adding a catalyst and diisocyanate after cooling to 30-50 DEG C, heating up to 50-80 DEG C and reacting for 2-6 hours, so as to obtain a methylbenzene solution of a polyurethane prepolymer; adding a chain extender to expand the chain, reacting for 2-6 hours, and then adding a hydroxyl-containing dendric molecule capping agent; heating up to 60-100 DEG C and reacting for 2-8 hours, and then adding a precipitator petroleum ether or normal hexane; drying the sediment in vacuum to finally obtain white solid powder, namely the polyurethane associated thickener. By adopting the polyurethane associated thickener, the viscosity of an emulsion paint can be effectively improved at low dosage, so that the emulsion paint has high viscosity in a low shear state, and also has the characteristic of low construction viscosity in a high shear state; the polyurethane associated thickener has a better application prospect.
Owner:SOUTH CHINA UNIV OF TECH

Temperature and salt-resistant AM/ACD/AE copolymer and its preparation method

The invention relates to a temperature and salt-resistant AM / ACD / AE copolymer used as an oil displacement agent in the petroleum exploitation and a preparation method thereof. The temperature and salt-resistant AM / ACD / AE copolymer can meet the requirements of the injected liquid viscosity with the incessant increasing of the oil reservoir temperature and the stratum mineralization. The technical scheme of the invention is characterized in that the mole ratio of the raw materials used in the preparation of the copolymer comprises, by mole percentage, 88.2-91.4% of an AM monomer, 8-11% of an ACD monomer, 0.6-0.8% of an AE monomer, an oxidizing agent potassium persulphate which accounts for 0.3-0.5% of the total weight of the monomers, and a reducing agent sodium bisulfite which accounts for0.35-0.45% of the total weight of the monomers. The preparation method provided by the invention comprises the following steps of: adding AM, ACD and AE into a container, adding water to produce a solution at the concentration of 15%, dissolving with stirring, adding the oxidizing agent and the reducing agent with uniformly blending, deoxygenizing by filling nitrogen, reacting at the temperature of 40-50 DEG C for 4-5 hours, washing and drying to obtain the AM / ACD / AE copolymer. The preparation method provided by the invention is simple and feasible with mild reaction conditions; the product prepared by the method has inclusion and aggregation functions as well as temperature and salt-resistant performance, and can be used in tertiary oil extraction.
Owner:SOUTHWEST PETROLEUM UNIV

Surface-active two-tailed hydrophobic associated polymer and preparation method thereof

The invention discloses a surface-active two-tailed hydrophobic associated polymer and a preparation method thereof; the surface-active two-tailed hydrophobic associated polymer is prepared via micellar free radical copolymerization: adding a surfactant, sodium lauryl sulfate, and a hydrophobic monomer, N-phenethyl-N-alkyl (methyl) acrylamide or N-benzyl-N-alkyl (methyl) acrylamide into the aqueous solution of acrylamide, acrylic acid, 2-acrylamide-2-methylpropanesulfonic acid, and surface-active macromonomer polyoxyethylene lauryl ether (methyl) acrylate, using the surfactant to solubilize the hydrophobic monomer in the formed micelle, using sodium hydroxide to adjust pH to 6-8, and copolymerizing the hydrophobic monomer and a water-soluble monomer by means of photo-initiation. The properties, such as tackifying performance, temperature resistance, salt resistance and hydrolysis resistance, of the polymer can be effectively improved, the preparation method and principle of the polymer are reliable, and the preparation method is simple to perform and has a promising application prospect.
Owner:SOUTHWEST PETROLEUM UNIV

Anti-high-salinity comb-type micro-segmented hydrophobic associated polymer and preparation method thereof

InactiveCN106397694AIncrease viscosityReduces the effect of hydrophobic associationsDrilling compositionArylSalt resistance
The invention discloses an anti-high-salinity comb-type micro-segmented hydrophobic associated polymer and a preparation method thereof. The preparation method includes: adopting a mixed micelle polymerization method to prepare the comb-type micro-segmented hydrophobic associated polymer: adding a surfactant (SDS), a cationic hydrophobic monomer and a nonionic surface activity monomer into a water solution containing water-soluble monomers like acrylamide and acrylic acid to form mixed micelle; solubilizing a double-tail hydrophobic monomer N-aryl-N-alkyl(methyl) acrylamide(PEMAM) in the mixed micelle; copolymerizing the hydrophobic monomer and the water-soluble monomer by means of photo-initiation to obtain the comb-type micro-segmented hydrophobic associated polymer. The polymer has a comb-type structure, so that temperature resistance, tackifying performance and salt resistance of the polymer are improved; a micro-segmented hydrophobic structure endows the polymer with excellent salt resistance and tackifying performance, and consumption of the polymer can be effectively lowered; the temperature-resistant salt-resistant polymer which can be used for chemical flooding of oil fields is prepared by combining advantages of the comb-type structure and the micro-segmented hydrophobic structure.
Owner:SOUTHWEST PETROLEUM UNIV

Preparation method for antibacterial hemostatic microspheres based on cellulose

The invention relates to a preparation method for antibacterial hemostatic microspheres based on cellulose, and belongs to the field of functional polymer materials. The preparation method for the antibacterial hemostatic microspheres comprises the steps: firstly, dissolving amphiphilic cellulose derivatives in an organic solvent, dissolving alginate in water, and mixing the two solutions; then adding an oil-in-water type emulsifier and tea tree oil into the mixed solution, and then carrying out heating and stirring reaction for 1-10 h under a condition of the temperature of 30-80 DEG C; and finally, separating microspheres by centrifugation, washing with a washing auxiliary agent, and filtering and drying to obtain the microsphere product. The method avoids toxic effects generated from microsphere crosslinking with a chemical crosslinking agent, and the obtained microspheres have certain hydrophilicity and have good hemostatic and antibacterial effects.
Owner:BEIJING INSTITUTE OF TECHNOLOGYGY

Sulfonate lycine type hydrophobic associated polymer and preparation method thereof

The invention discloses a sulfonate lycine type hydrophobic associated polymer and a preparation method thereof. A preparation process of the sulfonate lycine type hydrophobic associated polymer comprises the following steps that firstly, acrylamide and acrylic acid are mixed in an aqueous solution, and the pH of a system is regulated to be around 6 to 8; secondly, 3-(dimethylamino propyl methacrylamide)propanesulfonate, N-aryl-N-alkyl(methyl)acrylamide and lauryl sodium sulfate are added and stirred until the solution is clear; and thirdly, after nitrogen is led in for deoxidization, a photoinitiator azobis(isobutylamidine hydrochloride) is added for polymerization under photoinitiation conditions. Since advantages of a double-tail hydrophobic associated polymer and advantages of a lycine type polymer are combined, the viscosifying capability, the temperature endurance, the salt resistance and the hydrolysis resistance of the sulfonate lycine type hydrophobic associated polymer are remarkably improved, the sulfonate lycine type hydrophobic associated polymer can be used for an oil-displacing agent or an acidizing and fracturing thickener used for increasing a crude oil recovery rate in oilfield development, and the preparation method of the sulfonate lycine type hydrophobic associated polymer has the advantages of reliable principle, easiness in operation and wide market prospect.
Owner:SOUTHWEST PETROLEUM UNIV

Polymer having surface active function and preparation method and application thereof

The invention relates to the field of crude oil recovery and discloses polymer having a surface active function and a preparation method and application thereof. The polymer comprises a structural unit A, a structural unit B and a structural unit C, the structural unit A is shown as a formula (1), the structural unit B is shown as a formula (2), the structural unit C is shown as a formula (3), andviscosity average molecular weight of the polymer is 27-32 million. Functional monomer having surface activity and containing polymerizable acrylamide is introduced into acrylamide copolymer, so thatsurface activity, viscosifying performance and resistance to temperature and salt of a polyacrylamide solution are improved.
Owner:CHINA PETROLEUM & CHEM CORP +1

Terpolymer used for resisting temperature and displacing oil and preparation method thereof

The invention relates to a terpolymer used for resisting temperature and displacing oil and a preparation method thereof, the method comprises the following steps: introducing a hydrophobic monomer containing triphenyl in an acrylamide copolymer, preparing acrylamide, a sulfonic acid monomer and a hydrophobic monomer to obtain an aqueous solution, adding a complexing agent and an urea aqueous solution, then adding an emulsifier to prepare an emulsion, adding an initiator in the emulsion, polymerizing to obtain a rubber block, removing the rubber block, cutting, granulating, crushing, and sieving to obtain the terpolymer finished product. According to the terpolymer and the preparation method, the hydrophobic monomer containing triphenyl is introduced in a macromolecular chain, and thereby the viscosifying capacity and heatproof performance of the polymer can be increased.
Owner:CHINA PETROLEUM & CHEM CORP +1

Acid liquid thickener and preparation method thereof

The invention discloses an acid liquid thickener and a preparation method thereof, and belongs to the technical field of oil field acidification. The acid liquid thickener has the following chemical structure formula described in the specification, wherein the value of x to y to z is (200000-300000) to (50-500) to (2-13), and n is an integer of 5-25. The viscosity-average molecular weight of the acid liquid thickener is 6000000-12000000. The acid liquid thickener has the characteristics of being capable of reduction of the friction resistance with an acid liquid pump, good high-temperature resistance, good shear resistance and the like.
Owner:PETROCHINA CO LTD

Hydrophobic modified organic/inorganic composite flocculant and preparation method and application thereof

The invention discloses a hydrophobic modified organic / inorganic composite flocculant and a preparation method and application thereof. The structural formula of the hydrophobic modified organic / inorganic composite flocculant is as follows: R1 is Al or Fe or Ti, R2 is-NH (CH2) 2CH3 or-NHCH (CH3) 2, n ranges from 4.012 to 19.47, and the value range of x: y is (3.1 to 12.4): 1. The flocculant has both inorganic groups and organic groups, improves the defect of insufficient charge density of a single flocculating agent, and improves the electric neutralization characteristic so that the flocculation speed of the composite flocculating agent is increased, the effective flocculation range is widened, and the floc settling performance is good; the nanocrystallization flocculant has the advantages of multiple surface atoms, large particle specific surface area, high specific surface energy and the like, and the flocculation performance of the flocculant on pollutants is further improved; in addition, the flocculating agent subjected to moderate hydrophobic modification has excellent flocculation performance on micromolecular organic pollutants containing hydrophobic functional groups in awater body, and is wide in application range.
Owner:NANJING NORMAL UNIVERSITY

Benzyl-contained cationic polymerizable surface activated monomer and preparation method and ionic copolymer

The invention provides benzyl-contained cationic polymerizable surface activated monomer, which comprises the following molecular structure: in the formula, X is of a halogen anion; and R1 to R4 are respectively alkyl with 1-8 hydrogen atoms and carbon atoms, alkoxy or substituted phenyl with 1-8 carbon atoms. The invention further provides a preparation method for benzyl-contained cationic polymerizable surface activated monomer and ionic copolymer containing the benzyl-contained cationic polymerizable surface activated monomer unit. The benzyl-contained cationic polymerizable surface activated monomer has surface activity, and can be aggregated to form micelle in aqueous solution, and carries out copolymerization with hydrophilic monomer on the concentration of the aggregated micelle to obtain microblock property of the ionic copolymer; and the benzyl-contained cationic polymerizable surface activated monomer can also be used as emulsifier for carrying out emulsion copolymerization with hydrophobic monomer in the aqueous solution so as to prepare functionally ionic copolymer.
Owner:TECHNICAL INST OF PHYSICS & CHEMISTRY - CHINESE ACAD OF SCI

Polymer having surface activity function, and preparation method and application thereof

The invention relates to the field of crude oil recovery, and discloses a polymer having a surface activity function, and a preparation method and application thereof. The polymer contains a structural unit A, a structural unit B and a structural unit C, wherein the structural unit A is a structural unit having a structure shown in Formula (1); the structural unit B is a structural unit having a structure shown in Formula (2); and the structural unit C is a structural unit having a structure shown in Formula (3). According to the invention, a polymerizable monomer having surface activity is introduced onto a macromolecular chain, and the ether chain structure determines that the synthesized copolymer has high hydrolysis resistance and thermal stability, thereby improving the aging resistance of the polymer; and meanwhile, the surface tension and interfacial tension of the polymer solution are greatly reduced, so that the polymer has favorable surface activity and fine compatibilization, emulsification and oil washing capabilities, thereby improving the crude oil recovery factor. The Formula (1), the Formula (2) and the Formula (3) are shown in the specification.
Owner:CHINA PETROLEUM & CHEM CORP +1

Benzene-ring-containing modified acrylamide water-soluble amphoteric polymer and preparation method thereof

The invention relates to a benzene-ring-containing modified acrylamide water-soluble amphoteric polymer and a preparation method thereof. Amphoteric monomer methylacryloyloxyethyl-N,N-dimethylpropyl sulfonate (DMAPS), hydrophobic monomer methyl styrene (alpha-MST) and acrylamide (AM) are copolymerized in a lauryl sodium sulfate (SDS) emulsion by using potassium persulfate (KPS) as an initiator. Due to the introduction of the benzene ring structure comprising large steric hindrance, the water-soluble hydrophobic association polymer prepared by the method has the advantages of excellent hydrophobic associativity, excellent surface activity and excellent temperature / salt / shear resistance, can be used as a high molecular surfactant, and has wide application potential in the fields of oil-gas exploitation, paints, medicine and the like.
Owner:SHANDONG UNIV

Polymer having surface active function and preparation method and application thereof

The invention relates to the field of crude oil recovery and discloses polymer having a surface active function and a preparation method and application thereof. The polymer comprises a structural unit A, a structural unit B and a structural unit C, the structural unit A is shown as a formula (1), the structural unit B is shown as a formula (2), the structural unit C is shown as a formula (3), andviscosity average molecular weight of the polymer is 27-31.5 million. Functional monomer having surface activity and containing polymerizable acrylamide is introduced into acrylamide copolymer, so that surface activity, viscosifying performance and resistance to temperature and salt of a polyacrylamide solution are improved.
Owner:CHINA PETROLEUM & CHEM CORP +1

Supramolecular star polymer taking beta-CD (beta-cyclodextrin) as core and preparation method of supramolecular star polymer

The invention relates to a supramolecular star polymer taking beta-CD as a core and a preparation method of the supramolecular star polymer. The supramolecular star polymer takes a beta-cyclodextrin modified branched monomer F-beta-CD as an inner core and is grafted with acrylamide, acrylic acid, a hydrophobic monomer and a surface active macromonomer; the hydrophobic monomer is one or more of N-benzyl-N alkyl (methyl) acrylamide and N-phenethyl-N alkyl (methyl) acrylamide; the surface active macromonomer is one or more of allyl polyoxyethylene ether, alkylphenol polyoxyethylene ether (methyl) acrylate, alkylphenol polyoxyethylene ether allyl ether, alkyl alcohol polyoxyethylene ether (methyl) acrylate and alkyl alcohol polyoxyethylene ether allyl ether. The preparation method has the advantages of cheap and easily available raw materials, easily controllable synthesis conditions and high yield. The tackifying agent has excellent tackifying performance, temperature resistance, salt resistance and hydrolysis resistance, and shows good application prospects in the aspects of oil field recovery efficiency improvement and hydraulic fracturing.
Owner:SOUTHWEST PETROLEUM UNIV

Acrylic amide modified polymer micro-crosslinking gel and preparation thereof

The invention discloses acrylamide modified polymer micro-crosslinking gel and a preparation method thereof. The preparation method is characterized in that the method comprises the following steps that: acrylamide modified polymer PAE containing functional macro monomer is prepared into an aqueous solution with the concentration between 0.1 and 4g / L, the concentration of crosslinking agent between 0.01 and 1.0g / L, the concentration of surface active agent between 0.01 and 8mmol / L and the concentration of heat stabilizer sodium sulfite between 0.005 and 1.0g / L; the aqueous solution is added in a mixing container with a stirring device and is stirred evenly at room temperature; the pH value of the solution is adjusted between 4 and 11 to prepare a polymer solution system of the acrylamide modified polymer micro-crosslinking gel used for tertiary oil recovery and displacement, oil displacement modification, profile modification or water plugging; and the polymer solution system undergoes micro crosslinking during flowing inside an oil layer to form the gel. The acrylamide modified polymer micro-crosslinking gel has ideal elasticity, difficult dehydration, stable performance and excellent performances on tackifying, temperature resistance, salt resistance, shearing resistance and ageing resistance.
Owner:CHENGDU UNIVERSITY OF TECHNOLOGY

Preparation method of hydrophobic chitosan-based flocculating agent

The invention discloses a preparation method of a hydrophobic chitosan-based flocculating agent. The method, adopting chitosan, acrylamide (AM) and valencene as raw materials, comprises the followingsteps: sequentially adding the chitosan, acrylamide, and valencene into a reactor, adding an appropriate amount of water, and performing sufficient uniform mixing under a rapid stirring condition in order to achieve complete dissolving; placing a reactor, introducing nitrogen, and performing plasma functionalization under the action of low-pressure microwave-induced plasma; placing the reactor ina plasma reaction instrument, and turning on a radiofrequency generator to initiate a polymerization reaction; and performing discharging, performing stirring at a proper post-polymerization temperature for a certain period of time to obtain a mixture, and purifying the obtained product to obtain the hydrophobic chitosan-based flocculating agent. The preparation method has the advantages of stablereaction, easiness in control, and no addition of an initiator, and the obtained chitosan-based flocculating agent has a good solubility, is pure, has high hydrophobic association due to the introduction of a hydrophobic groups, is in favor of settling flocs during flocculation, and is an efficient water treatment flocculating agent.
Owner:CHONGQING TECH & BUSINESS UNIV

Polymer having surface activity function, preparation method and application thereof

The invention discloses a polymer having surface activity function, a preparation method and an application thereof. The polymer contains a structural unit A, a structural unit B and a structural unit C, the structural unit A is shown in a formula (1), the structural unit B is shown in a formula (2), the structural unit C is shown in a formula (3), by taking the weight of the polymer as a reference, the content of the structural unit A is 5-60 wt%, the content of the structural unit B is 30-90 wt%, the content of the structural unit C is 0.1-10 wt%; and the viscosity average molecular weight of the polymer is 18 million-28 million. The polymer has the advantages of good water solubility, strong tackifying ability, and heatproof salt-resistance performance and good surface activity, so that the polymer has good oil-washing effect, and can be used as an oil displacement polymer of mid-low permeability reservoir.
Owner:CHINA PETROLEUM & CHEM CORP +1

Oil displacing polymer with surface activity and preparing method and application thereof

The invention relates to the field of crude oil extraction, and discloses an oil displacing polymer with the surface activity and a preparing method and application thereof. The polymer comprises a structural unit A, a structural unit B and a structural unit C, wherein the structural unit A is a structural unit with the structure shown in the formula (1), the structural unit B is a structural unitwith the structure shown in the formula (2), and the structural unit C is a structural unit with the structure shown in the formula (3). According to the oil displacing polymer with the surface activity and the preparing method and application thereof, a hydrophobic monomer and a hydrophilic monomer are jointly introduced into a macromolecular chain of polyacrylamide to prepare a novel polymer with the surface activity, and the obtained novel polymer with the surface activity has the improved tackifying performance and emulsifying performance, the reduced surface and interfacial tension and the like. The formulas are defined in the description.
Owner:CHINA PETROLEUM & CHEM CORP +1

Water-based drilling fluid filtrate loss reducer based on modified plantain seed husks and preparation method thereof

The present invention provides a water-based drilling fluid filtrate loss reducer based on modified plantain seed husks and a preparation method thereof. The water-based drilling fluid filtrate loss reducer based on the modified plantain seed husks includes plantain seed husk powder, NaOH, 95% ethanol, chloroacetic acid, hydrophobic nano-calcium carbonate and water. The water-based drilling fluid filtrate loss reducer is prepared by crushing, purification, alkalization and carboxymethylation of the plantain seed husks with high filtrate loss reducing effect and plugging performance, and combination with the hydrophobic nano-calcium carbonate, and the water-based drilling fluid filtrate loss reducer based on the modified plantain seed husks is finally formed by hydrophobic interaction to improve system anti-temperature ability and filtrate loss reducing effect. The water-based drilling fluid filtrate loss reducer has obvious effects. After the water-based drilling fluid filtrate loss reducer is aged at 150 DEG C for 24 hours, the filter loss is remained at a relatively low level (4.3 mL). At the same time, the water-based drilling fluid filtrate loss reducer is non-toxic and has no adverse effect on the environment. The acute toxicity EC50 is greater than 50,000, and the water-based drilling fluid filtrate loss reducer can be completely degraded. The water-based drilling fluid filtrate loss reducer is an efficient drilling fluid filtrate loss reducer. The method has the advantages of being simple, easy in operation and easy in popularization.
Owner:中石化石油工程技术服务有限公司 +2

Ultrahigh-temperature organic crosslinking fracturing fluid system

The invention relates to a superhigh-temperature organic crosslinking fracturing fluid system which is prepared from the following components in percentage by mass: 0.6 wt% of a supramolecular star polymer, 0.5-1.0 wt% of a formaldehyde solution, 0.02-0.04 wt% of resorcinol, 0.05-0.2 wt% of an ammonium salt catalyst and the balance of water, the supramolecular star polymer is a supramolecular star polymer formed by taking a beta-cyclodextrin modified branched monomer F-beta-CD as an inner core and grafting acrylamide, acrylic acid, a hydrophobic monomer and a surface active macromonomer, the ammonium salt catalyst is one or more of ammonium chloride, ammonium bicarbonate, ammonium acetate, ammonium citrate, ammonium benzoate and ammonium oleate. The supramolecular star polymer is used as a thickening agent, the organic cross-linking agent is used as a cross-linking agent, and the ammonium salt is used as a catalyst, so that the fracturing fluid which is low in cost, appropriate in cross-linking time and stable in viscosity under an ultrahigh-temperature condition is formed, and the fracturing fluid is suitable for field large-scale popularization and application and has a wide market prospect.
Owner:SOUTHWEST PETROLEUM UNIV

A fluid loss reducer for water-based drilling fluid based on modified psyllium seed husk and its preparation method

The present invention provides a water-based drilling fluid filtrate loss reducer based on modified plantain seed husks and a preparation method thereof. The water-based drilling fluid filtrate loss reducer based on the modified plantain seed husks includes plantain seed husk powder, NaOH, 95% ethanol, chloroacetic acid, hydrophobic nano-calcium carbonate and water. The water-based drilling fluid filtrate loss reducer is prepared by crushing, purification, alkalization and carboxymethylation of the plantain seed husks with high filtrate loss reducing effect and plugging performance, and combination with the hydrophobic nano-calcium carbonate, and the water-based drilling fluid filtrate loss reducer based on the modified plantain seed husks is finally formed by hydrophobic interaction to improve system anti-temperature ability and filtrate loss reducing effect. The water-based drilling fluid filtrate loss reducer has obvious effects. After the water-based drilling fluid filtrate loss reducer is aged at 150 DEG C for 24 hours, the filter loss is remained at a relatively low level (4.3 mL). At the same time, the water-based drilling fluid filtrate loss reducer is non-toxic and has no adverse effect on the environment. The acute toxicity EC50 is greater than 50,000, and the water-based drilling fluid filtrate loss reducer can be completely degraded. The water-based drilling fluid filtrate loss reducer is an efficient drilling fluid filtrate loss reducer. The method has the advantages of being simple, easy in operation and easy in popularization.
Owner:中石化石油工程技术服务有限公司 +2
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