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The application relates to a cyhalofop-butyl intelligent phase separation monitoring control system and method. The cyhalofop-butyl intelligent phase separation monitoring control system comprises a visual monitoring unit (101) for collecting liquid surface stratification images in real time and detecting a cyhalofop-butyl concentration gradient; a discharge threshold setting and control unit (102) according to visual data; an execution unit (103) for automatic discharge of stratified liquid; and a warning unit (104) for identifying emulsification risks. The method comprises water washing, standing and interface monitoring, automatic discharge of stratified liquid and emulsification risk identification. Through intelligent sensing, multi-parameter collaborative control and data closed-loop management, the problems of low precision, high emulsification risk and high energy consumption in cyhalofop-butyl phase separation are solved, the product quality and production efficiency are significantly improved, and the method is suitable for large-scale industrial production.