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45results about How to "High resistance to laser damage threshold" patented technology

Ultraviolet-transmittance and high-damage-threshold fluoride phosphate laser glass and preparation method thereof

The invention provides high-damage-threshold fluoride phosphate laser glass as a material for preparing an ultraviolet-transmittance window, and a preparation method of the high-damage-threshold fluoride phosphate laser glass. The preparation method comprises the steps of adopting an alkali metal oxide, an alkaline earth metal oxide, alumina, zinc oxide and phosphoric pentoxide as main raw materials, adding a small amount of rare earth fluoride, molding and preparing glass pressing blanks based on the drip injection method after the treatments of high-temperature melting, clarification and homogenizing, and finally obtaining the high-damage-threshold fluoride phosphate laser glass material through the annealing treatment. The fused quartz material can be replaced by the above glass material for preparing lenses, plane windows, prisms and other optical components applied to high-energy and high-power laser systems. In this way, the laser-induced damage problems of ultraviolet optical components made of the fused quartz material in existing high-energy and high-power laser systems can be solved. The load output capability of a laser is further improved. Therefore, the above material can be used for preparing the ultraviolet-transmittance optical components of high-power lasers for laser-driven inertial confinement fusion experiments.
Owner:XI'AN INST OF OPTICS & FINE MECHANICS - CHINESE ACAD OF SCI

Photoinduced stable nonlinear sulfur film, and preparation method thereof

The invention discloses a photoinduced stable nonlinear sulfur film, and a preparation method thereof, and belongs to an optical film and a nonlinear optical material. The chemical composition of the film is GexAsySzSe(100-x-y-z), wherein x is smaller than or equal to 14 and greater than or equal to 10; y is smaller than or equal to 28 and greater than or equal to 20; z is smaller than or equal to 50 and greater than or equal to 16. A vacuum thermal evaporation method is adopted in preparation of the film; the vacuum degree is 10<-4> to 10<-6> torr; the evaporation rate is 3-20 nm/min; the refractive index of the sulfur film prepared by the method at wavelength of 1.55 microns is 2.20-2.56; the refractive index change of the film under thermal annealing and sub-band gap illumination is 10<-3>; an optical band gap is 1.98-2.48ev; the loss of the film at the wavelength of 1.55 microns is smaller than 0.2 dB/cm; the third-order nonlinear refractive index at the wavelength of 1.55 microns is 2.0-6.0*10<-14> cm<2>/W; no significant two-photon is absorbed; a laser-damaged threshold is greater than 200 GW/cm<2> (5.3 microns, 150fs, 1kHz). The photoinduced stable nonlinear sulfur film has the advantages that 1, the photoinduced refractive index change is tiny, and the optical performance of an apparatus is stable; 2, the anti-laser damage threshold of the film is high, and application of the apparatus in the field of nonlinear optics is facilitated; 3, the composition and the refractive index of the film obtained by vacuum evaporation are consistent with those of adopted block raw materials, and the films produced in different batches are consistent in performance, and easy to control.
Owner:XUZHOU NORMAL UNIVERSITY

High-performance chalcogenide glass microsphere and preparation method thereof

ActiveCN103613276AGood spherical shapeLight-induced refractive index change is smallGlass shaping apparatusMicrosphereRefractive index
The invention discloses a high-performance chalcogenide glass microsphere and a preparation method thereof, wherein the glass microsphere belongs to an optical microsphere and an infrared sensing material. The chemical composition of the glass microsphere is GexAsyS100-x-y, wherein x is greater than or equal to 8 and smaller than or equal to 12, while y is greater than or equal to 20 and smaller than or equal to 32. The glass microsphere is obtained by means of heat treating 'chalcogenide glass/polymer' composite optical fibers, and the composite optical fibers are obtained by means of drawing 'chalcogenide glass/polymer' preform rods on an optical fiber drawing tower. The chalcogenide glass microsphere prepared by the method has a diameter of 8-300 micrometers, an eccentricity degree smaller than or equal to 1%, surface smoothness smaller than or equal to 1nm, a microcavity quality factor Q greater than or equal to 1x10<5> and a laser induced damage threshold greater than or equal to 400GW/cm<2>(5.3micrometers, 150fs and 1kHz). The chalcogenide glass microsphere can be applied to the fields of molecular sensing and infrared optics. The chalcogenide glass microsphere and the preparation method have the following advantages that 1. the photon-induced refractive index change of glass is extremely small and the optical stability is good; 2. the laser induced damage resisting threshold of the glass microsphere is relatively high and the glass microsphere serving as an optical microcavity is capable of transmitting relatively high laser power; 3. the preparation technology is simple, the cost is very low and a large number of high-quality microspheres with uniform size can be prepared at a time.
Owner:NANJING WAVELENGTH OPTO ELECTRONICS SCI & TECH CO LTD

Chromium-nitride-stabilized zirconium oxide vacuum coating material and manufacturing method thereof

The invention provides a chromium-nitride-stabilized zirconium oxide vacuum coating material and a manufacturing method thereof. Raw materials of the chromium-nitride-stabilized zirconium oxide vacuum coating material comprise, by mole, 75% to 98% of zirconium oxide and 2% to 25% of chromium nitride, and a proper amount of a polyvinyl alcohol bonding agent is added. The manufacturing method of the chromium-nitride-stabilized zirconium oxide vacuum coating material includes the following steps that firstly, zirconium oxide powder and chromium nitride powder serve as the raw materials, the raw materials are weighed according to the selected mole percents and evenly mixed, the polyvinyl alcohol bonding agent is then added, and the powder is agglomerated, pelletized and formed; secondly, the particle materials are pre-sintered, wherein the pre-sintering temperature is 1200 DEG C; and thirdly, the materials are sintered in a vacuum sintering furnace and then naturally cooled to the indoor temperature. By the adoption of the chromium-nitride-stabilized zirconium oxide vacuum coating material, the problems that a traditional zirconium oxide coating material is unstable and the refraction rate of the traditional zirconium oxide coating material is uneven in the coating process are solved, and the damage threshold value of a zirconium oxide film is increased.
Owner:WUXI HUIMING ELECTRONICS TECH

Ultraviolet band ultra-low absorption double-sided antireflection film and preparation method thereof

The invention discloses an ultraviolet band ultra-low absorption double-sided antireflection film and a preparation method thereof, and the structure of the ultraviolet band ultra-low absorption double-sided antireflection film is Air / (biLaiH) m / Sub / (aiHbiL) m / Air, wherein Sub represents a substrate; m is the number of cycles, and m is an integer from 2 to 6; H represents a high-refractive-index film layer, and the refractive index of the high-refractive-index film layer is 1.5-3; L represents a low-refractive-index film layer, and the refractive index of the low-refractive-index film layer is 1-1.5; ai and bi respectively represent the optical thickness coefficient of each film layer, the numerical values are related to the reference wavelength lambda, (ai lambda) is more than or equal to 0 and less than or equal to 200, and (bi lambda) is more than or equal to 0 and less than or equal to 200. According to the ultraviolet band ultra-low absorption double-sided antireflection film, the film system design and the process are improved, 355nm ultraviolet antireflection is realized by plating the film systems on the surfaces of the two sides of the ultraviolet window glass substrate with the thickness of 5mm, the absorption is reduced, the transmittance is improved, the average transmittance is greater than 99.5%, and the single-sided reflection is less than 0.15%.
Owner:NANJING WAVELENGTH OPTO ELECTRONICS SCI & TECH CO LTD

An Evaporation Method for Improving the Anti-laser Damage Threshold of Oxide Thin Films

The invention belongs to the field of thin film optics, and in particular relates to an evaporation method for improving a laser induced damage threshold of an oxide film, mainly aiming at the key factors, which comprise the absorption and defects in films, and causes the damage in laser-induced film. The ineffective evaporation materials are blocked and adsorbed by adding an isolation baffle between the evaporation source and the substrate, thereby reducing the pollution to the vicinity of the substrate and decreasing the probability for defects formation in the film; oxygen radicals, which have stronger oxidization capability than conventional molecular oxygen and ions oxygen, are introduced into the vacuum chamber to allow oxygen radicals to be incident on the surface of the substrate so that the deposition material is possibly sufficiently oxidized under high vacuum conditions, and the absorption of the film is reduced, thereby obtaining the oxide film having higher threshold. The method not only retains the unique beneficial properties of the electron beam thermal evaporation method for plating a laser film and but also improves the intrinsic absorption and the defect density of the film; and the preparation method has the characteristics of strong pertinence, high quality and simplicity and feasibility.
Owner:润坤(上海)光学科技有限公司

A kind of preparation method of photo-stable nonlinear chalcogenide thin film

A light-induced stable nonlinear chalcogenide thin film and a preparation method thereof belong to optical thin films and nonlinear optical materials. The chemical composition of the film is Ge x As y S z Se 100‑x‑y‑z , wherein 10≤x≤14, 20≤y≤28, 16≤z≤50; its preparation adopts vacuum thermal evaporation method, and the vacuum degree is 10 ‑4 ~10 ‑6 torr, the evaporation rate is 3~20nm / min. The chalcogenide film prepared by the present invention has a refractive index of 2.20 to 2.56 at a wavelength of 1.55 μm, and the change of the film’s refractive index under thermal annealing and sub-band gap light is less than 10 ‑3 ; The optical band gap is 1.98~2.48ev; the loss of the film at 1.55μm wavelength is less than 0.2dB / cm; the third-order nonlinear refractive index at 1.55μm wavelength is 2.0~6.0x10 ‑14 cm 2 / W, no significant two-photon absorption; laser damage threshold greater than 200GW / cm 2 (5.3μm, 150fs, 1kHz). Advantages: 1. The light-induced refractive index change is extremely small, and the optical performance of the device is stable; 2. The anti-laser damage threshold of the film is high, which is conducive to the application of the device in the field of nonlinear optics; 3. The film composition and The refractive index is consistent with the bulk raw material used, and the consistency of film properties prepared in different batches is easy to control.
Owner:XUZHOU NORMAL UNIVERSITY
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