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35results about How to "High softening point under load" patented technology

High-crystal mullite-iolite high-temperature industrial ceramic and production method for same

The invention relates to a high-crystal mullite-iolite high-temperature industrial ceramic and a production method for the same. Raw materials comprise, by weight, 40-80 parts of main crystal phase materials, 20-60 parts of combined composite substrate materials and an appropriate amount of composite microcrystal nucleating agent. A roasting process of the production method includes a two-stage constant-temperature roasting method and a two-stage composite crystallization synthetic reaction characteristic enhancing process, wherein the two-stage constant-temperature roasting method includes the steps of performing constant-temperature heat preservation for 10-15 hours at the temperature of 200 DEG C, and performing constant-temperature heat preservation for 10-15 hours at the temperature of 500 DEG C; and the two-stage composite crystallization synthetic reaction characteristic enhancing process includes the steps of sintering for 10-15 hours under the ordinary pressure and at the temperature ranging from 1100 DEG C to 1150 DEG C, and sintering for 20-25 hours under the ordinary pressure and at the temperature ranging from 1420 DEG C to 1430 DEG C. A refractory product produced bythe method has the advantages of excellent oxidation resistance, high refractoriness, high usage temperature, low thermal expansion coefficient, high compression strength, hypobarism, excellent heat stability, anti-strip performance and high high-temperature bending strength. The process of the method has the advantages of simple process, low cost and suitability for mass production, and is applicable to preparing kiln furniture, industrial ceramics and structural materials.
Owner:GUANGDONG REJINBAO NEW MATERIAL TECH +2

Metal-based aluminum-magnesium spinel sliding plate and preparation method thereof

The invention discloses a metal-based aluminum-magnesium spinel sliding plate and a preparation method thereof. The metal-based aluminum-magnesium spinel sliding plate consists of a dry material and an additional binding agent; and the dry material comprises: high-purity corundum particles and fine powder, aluminum-magnesium spinel particles and fine powder, magnesia fine powder, alpha-Al2O3 finepowder and a metal powder additive. The specific preparation method comprises the following steps: firstly, taking the high-purity corundum fine powder, the magnesia fine powder, aluminum-magnesium spinel fine powder, the alpha-Al2O3 fine powder and the metal powder in the dry material to sufficiently mix so as to obtain pre-mixed powder; then taking the high-purity corundum particles and the aluminum-magnesium spinel particles to sufficiently mix, adding the binding agent into the mixed particles to remix, and then adding the pre-mixed powder into the mixture to carry out mixed milling; and carrying out ageing, forming, thermal treatment and impregnation on the obtained mixture, and then carrying out processes of drying, strapping, grinding and surface coating on the obtained semi-finished product so as to obtain the finished product. The invention provides the iron and steel smelting sliding plate which is safe and reliable and has high-temperature resistance, erosion resistance anda long service life; and the metal-based aluminum-magnesium spinel sliding plate is simple in preparation process, does not require a high temperature, and is low in production energy consumption andgood in operation environment.
Owner:LUOYANG KECHUANG NEW MATERIAL CO LTD

Micro-expansive brick for carbon anode baking furnace and preparation method thereof

The invention discloses a micro-expansive brick for a carbon anode baking furnace and a preparation method thereof. The micro-expansive brick is prepared from the following components in percentage by weight: 6-8% of calcined bauxite clinker having the granularity of 3-5mm, 29-32% of calcined bauxite clinker having the granularity of 1-3mm, 15-20% of calcined flint clay clinker having the granularity of 0-1mm, 10-15% of Guangxi clay powder having the fineness less than or equal to 0.074mm, 14-15% of kyanite powder having the fineness less than or equal to 0.088mm, and 12-18% of calcined bauxite clinker powder having the fineness less than or equal to 0.088mm. The preparation method comprises the following steps: 1, crushing and screening the calcined bauxite clinker and the calcined flint clay clinker; 2, grinding the Guangxi clay, the kyanite and the calcined bauxite clinker; 3, mixing and stirring; 4, adding a paper pulp waste liquid and mixing; 5, pressing brick blanks; 6, drying and calcining to obtain the finished products. The prepared micro-expansive brick for the carbon anode baking furnace is low in creep rate, high in refractoriness under load, high in high-temperature bending strength and longer in service life, and therefore, the service life of the carbon anode baking furnace can be increased to the utmost extent and the maintenance cost can be reduced.
Owner:河南鑫诚耐火材料股份有限公司

Nitride bonded sandwich load bearing board and preparation method thereof

The invention relates to a nitride bonded sandwich load bearing board and a preparation method thereof, and belongs to the technical field of fireproof materials. The nitride bonded sandwich load bearing board comprises a mullite surface protection layer and a silicon nitride bonded silicon carbide middle layer, wherein the mullite surface protection layer is prepared from the following raw materials: mullite of which the coarseness is 0.2 to 1mm, mullite fine powder of which the particle size is 200 meshes, mullite of which the density is 325 meshes, clay and an organic bonding agent; the silicon nitride bonded silicon carbide middle layer is prepared from silicon carbide of which the coarseness is 1 to 3mm, silicon carbide of which the coarseness is 0.5 to 1, silicon carbide fine powder of which the coarsness is 0.5 to 1mm and the particle size is 325 meshes, silicon carbide ultrafine powder, the clay, metal silicon powder of which the particle size is 325 meshes and the organic bonding agent. According to the nitride bonded sandwich load bearing board disclosed by the invention, silicon nitride bonded silicon carbide is adopted as the middle layer, the high temperature bending strength of the silicon nitride bonded silicon carbide is high and is not reduced but increased under a high temperature, reaction between a magnetic material and the load bearing board is avoided during sintering of the magnetic material, and the service life of the load bearing board is indirectly prolonged.
Owner:宜兴市锦泰耐火材料有限公司

High-aluminum pull brick for carbon anode roasting furnace flame paths and preparation method thereof

ActiveCN104276830AIncrease the service life of the furnaceLow creep rateBrickMullite
The invention discloses a high-aluminum pull brick for carbon anode roasting furnace flame paths and a preparation method thereof. The high-aluminum pull brick for carbon anode roasting furnace flame paths is prepared by mixing, calcining and pressing calcined mullite, calcined high-aluminum bauxite, andalusite granules, alumina powder, Gangxi clay powder and andalusite fine powder. The preparation method comprises the following steps: 1. crushing and screening the calcined mullite and calcined high-aluminum bauxite; 2. selecting 10-16 wt% of alumina powder, 10-12 wt% of Gangxi clay powder and 15-21 wt% of andalusite fine powder, mixing and grinding; 3. mixing the co-ground powder with 8-12 wt% of calcined mullite, 17-23 wt% of calcined high-aluminum bauxite and 25-29 wt% of andalusite granules; 4. adding pulp waste, and compounding; 5. pressing to be green bricks; and 6. drying and calcining to obtain the finished product. The high-aluminum pull brick for carbon anode roasting furnace flame paths has the advantages of low creep rate, high refractoriness under load, favorable high-temperature folding strength and small physical dimension deformation, and can prolong the service life of the carbon anode roasting furnace and lower the maintenance cost.
Owner:河南鑫诚耐火材料股份有限公司

Electric cast mullite brick and preparation method thereof

The invention relates to an electric cast mullite brick, which comprises the following raw materials with the granularity distribution in percentage by weight: 55 to 80 percent of electric cast mullite with the granularity distribution being smaller than or equal to 3.5mm, 10 to 20 percent of kyanite with the granularity distribution being smaller than or equal to 0.1mm, 10 to 20 percent of quartz with the granularity distribution being 0.1 to 1.5mm, 0 to 5 percent of clay with the granularity distribution being smaller than or equal to 0.1mm and 0 to 1 percent of titanium dioxide with the granularity distribution being 2 to 10mum. A preparation method of the electric cast mullite brick comprises the following steps that: crushing, sieving and magnetic separation are carried out; the kyanite, the quartz, the clay, the titanium dioxide and partial electric cast mullite are mixed with oleic acid and are subjected to ball milling to obtain ball milling materials; bonding agents are dissolved in water to be mixed with the rest electric cast mullite to obtain particle materials; the ball milling materials and the particle materials are mixed and are subjected to mixed milling, aging decaying and secondary mixing; green bricks are obtained through pressure forming, and the green bricks are dried and fired. The electric cast mullite brick and the preparation method have the advantages that the process is simple, the cost is low, the operability is high, and the obtained electric cast mullite brick body has high density, good acid resistance, high normal-temperature bending-resistant intensity and excellent thermal shock stability.
Owner:JIANGSU PROVINCE YIXING NONMETALLIC CHEM MACHINERY FACTORY

Method of improving high-temperature strength of integral alumina-based ceramic mold through chemical vapor infiltration

The invention discloses a method of improving high-temperature strength of an integral alumina-based ceramic mold through chemical vapor infiltration, and belongs to the field of photocuring forming technology quick casting. The method includes the steps that 1, a resin mold is manufactured through the photocuring quick forming technology; 2, ceramic slurry is poured into a resin mold prototype of turbine blades through a gelcasting method to obtain a cast blank; 3, a porous alumina-based ceramic mold is obtained after vacuum freeze drying and ungrease treatment; 4, the alumina-based ceramic mold is subjected to chemical vapor infiltration, SiO2 generated after pyrolytic reaction of a silicon source precursor and matrix alumina react chemically to generate high-temperature strengthened phase mullite, the pore structure of the mold is filled with SiC generated through the pyrolytic reaction, a functional gradient material with the porosity gradually improved from the surface layer to the core part of the mold, and the porosity of the mold is reduced to improve the high-temperature strength of the mold. The method is reasonable in design and convenient to operate, and the high-temperature strength of the alumina-based ceramic mold is enhanced remarkably.
Owner:XI AN JIAOTONG UNIV

A kind of in-situ synthesis mullite whisker toughened 90 alumina ceramics and its preparation method

ActiveCN106167413BWiden the scope of selectionStimulating developmental effectsPolyvinyl alcoholAdhesive
The invention discloses a preparation method of an in-situ synthesized mullite whisker toughened 90 alumina ceramic. The method consists of: taking 85-95wt% of highly dispersed alpha-alumina powder and 5-15wt% of highly dispersed silicon dioxide powder as the raw materials, adopting aluminum fluoride trihydrate powder accounting for 4-18% of the weight of the raw materials and dry basis titanium dioxide accounting for 0.5-3% of the weight of the raw materials as the catalysts, mixing the raw materials with the catalysts, then using water as the medium to perform ball-milling so as to form an Al2O3-SiO2 precursor containing AlF3 and TiO2, then adding polyvinyl alcohol accounting for 1-3% of the weight of the raw materials to serve as the adhesive, conducting mixing, then employing spray drying process to perform granulation and ageing, then conducting isostatic pressing dry process forming, and performing high temperature firing so as to obtain the mullite whisker toughened 90 alumina ceramic. According to the invention, adding of expensive whiskers is unnecessary, a complicated dispersion process of additional adding of whiskers is omitted, also the preparation process is simple, the obtained whiskers have large length, high length-diameter ratio and uniform dispersion, and the method is suitable for industrial production.
Owner:江西省工业陶瓷工程技术研究中心

Novel prefabricated iron tap channel and preparation method thereof

The invention discloses a prefabricated iron tap channel. The novel prefabricated iron tap channel comprises an outer steel shell, a permanent layer and a working layer, wherein the permanent layer and the working layer are arranged in the outer steel shell, the permanent layer comprises a permanent pouring layer, a prefabricated base and prefabricated side plates, the working layer is arranged ina space defined by the permanent pouring layer, the prefabricated base and the prefabricated side plates, and the prefabricated side plates are fixedly connected with the prefabricated base in an inserted mode; arc-shaped protrusions are arranged at the lower ends of the prefabricated side plates, and arc-shaped grooves matched with the arc-shaped protrusions are formed in the prefabricated base.The invention further discloses a preparation method of the novel prefabricated iron tap channel. The preparation method is simple in process. The prepared novel prefabricated iron tap channel blocksmelts penetrating the working layer effectively, so that the safety risk is reduced greatly. The novel prefabricated iron tap channel is convenient to replace and short in time. Normal switching useof the iron tap channel is not affected completely in a maintenance repair process.
Owner:YIXING REFRACTORY EQUIP & MATERIAL FACTORY +1

High temperature ceramic fiber membrane microfiltration tube

The invention discloses a high temperature ceramic fiber membrane microfiltration tube which is prepared by the following steps: main materials mullite, alumina, titanium aluminum carbide, zirconium oxide, potassium feldspar and walnut shell powder are mixed in a kneader, carboxymethyl cellulose and vegetable oil are added for mixing, a blank is extruded and dried, fired at 1350 DEG C under heat insulation, and cooled to obtain a supporting tube body for standby use; zirconia aluminosilicate ceramic fiber, aluminum titanate, mullite, magnesium oxide, cerium oxide and feldspar are mixed evenly in kneader to obtain a mixture, and an additive is added into the mixture to obtain a film material to form a fiber membrane on the outer surface of the supporting tube body by high temperature firing. The high temperature ceramic fiber membrane microfiltration tube has high mechanical strength and thermal denaturation, membrane layer micro pore distribution is good, specific surface area is large, pore connectivity is good, filtering accuracy can reaches 0.1 mum, the service life is increased by more than 30%, the dust removal efficiency reaches 99.99%, and the dust concentration after filteration is less than 10mg / Nm3, and is far better than that of the national standard.
Owner:萍乡市三盈科技有限公司

A kind of high-alumina drawn brick for carbon anode roasting furnace flue channel and preparation method thereof

ActiveCN104276830BIncrease the service life of the furnaceLow creep rateBrickMullite
The invention discloses a high-aluminum pull brick for carbon anode roasting furnace flame paths and a preparation method thereof. The high-aluminum pull brick for carbon anode roasting furnace flame paths is prepared by mixing, calcining and pressing calcined mullite, calcined high-aluminum bauxite, andalusite granules, alumina powder, Gangxi clay powder and andalusite fine powder. The preparation method comprises the following steps: 1. crushing and screening the calcined mullite and calcined high-aluminum bauxite; 2. selecting 10-16 wt% of alumina powder, 10-12 wt% of Gangxi clay powder and 15-21 wt% of andalusite fine powder, mixing and grinding; 3. mixing the co-ground powder with 8-12 wt% of calcined mullite, 17-23 wt% of calcined high-aluminum bauxite and 25-29 wt% of andalusite granules; 4. adding pulp waste, and compounding; 5. pressing to be green bricks; and 6. drying and calcining to obtain the finished product. The high-aluminum pull brick for carbon anode roasting furnace flame paths has the advantages of low creep rate, high refractoriness under load, favorable high-temperature folding strength and small physical dimension deformation, and can prolong the service life of the carbon anode roasting furnace and lower the maintenance cost.
Owner:河南鑫诚耐火材料股份有限公司

Electric cast mullite brick and preparation method thereof

The invention relates to an electric cast mullite brick, which comprises the following raw materials with the granularity distribution in percentage by weight: 55 to 80 percent of electric cast mullite with the granularity distribution being smaller than or equal to 3.5mm, 10 to 20 percent of kyanite with the granularity distribution being smaller than or equal to 0.1mm, 10 to 20 percent of quartz with the granularity distribution being 0.1 to 1.5mm, 0 to 5 percent of clay with the granularity distribution being smaller than or equal to 0.1mm and 0 to 1 percent of titanium dioxide with the granularity distribution being 2 to 10mum. A preparation method of the electric cast mullite brick comprises the following steps that: crushing, sieving and magnetic separation are carried out; the kyanite, the quartz, the clay, the titanium dioxide and partial electric cast mullite are mixed with oleic acid and are subjected to ball milling to obtain ball milling materials; bonding agents are dissolved in water to be mixed with the rest electric cast mullite to obtain particle materials; the ball milling materials and the particle materials are mixed and are subjected to mixed milling, aging decaying and secondary mixing; green bricks are obtained through pressure forming, and the green bricks are dried and fired. The electric cast mullite brick and the preparation method have the advantages that the process is simple, the cost is low, the operability is high, and the obtained electric cast mullite brick body has high density, good acid resistance, high normal-temperature bending-resistant intensity and excellent thermal shock stability.
Owner:JIANGSU PROVINCE YIXING NONMETALLIC CHEM MACHINERY FACTORY

Micro-expansion brick for carbon anode roasting furnace and preparation method thereof

The invention discloses a micro-expansive brick for a carbon anode baking furnace and a preparation method thereof. The micro-expansive brick is prepared from the following components in percentage by weight: 6-8% of calcined bauxite clinker having the granularity of 3-5mm, 29-32% of calcined bauxite clinker having the granularity of 1-3mm, 15-20% of calcined flint clay clinker having the granularity of 0-1mm, 10-15% of Guangxi clay powder having the fineness less than or equal to 0.074mm, 14-15% of kyanite powder having the fineness less than or equal to 0.088mm, and 12-18% of calcined bauxite clinker powder having the fineness less than or equal to 0.088mm. The preparation method comprises the following steps: 1, crushing and screening the calcined bauxite clinker and the calcined flint clay clinker; 2, grinding the Guangxi clay, the kyanite and the calcined bauxite clinker; 3, mixing and stirring; 4, adding a paper pulp waste liquid and mixing; 5, pressing brick blanks; 6, drying and calcining to obtain the finished products. The prepared micro-expansive brick for the carbon anode baking furnace is low in creep rate, high in refractoriness under load, high in high-temperature bending strength and longer in service life, and therefore, the service life of the carbon anode baking furnace can be increased to the utmost extent and the maintenance cost can be reduced.
Owner:河南鑫诚耐火材料股份有限公司

A method for improving the high temperature strength of monolithic alumina-based ceramic molds by chemical vapor infiltration

The invention discloses a method of improving high-temperature strength of an integral alumina-based ceramic mold through chemical vapor infiltration, and belongs to the field of photocuring forming technology quick casting. The method includes the steps that 1, a resin mold is manufactured through the photocuring quick forming technology; 2, ceramic slurry is poured into a resin mold prototype of turbine blades through a gelcasting method to obtain a cast blank; 3, a porous alumina-based ceramic mold is obtained after vacuum freeze drying and ungrease treatment; 4, the alumina-based ceramic mold is subjected to chemical vapor infiltration, SiO2 generated after pyrolytic reaction of a silicon source precursor and matrix alumina react chemically to generate high-temperature strengthened phase mullite, the pore structure of the mold is filled with SiC generated through the pyrolytic reaction, a functional gradient material with the porosity gradually improved from the surface layer to the core part of the mold, and the porosity of the mold is reduced to improve the high-temperature strength of the mold. The method is reasonable in design and convenient to operate, and the high-temperature strength of the alumina-based ceramic mold is enhanced remarkably.
Owner:XI AN JIAOTONG UNIV
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