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38results about How to "Lower the smelting temperature" patented technology

Clean metallurgical method for low-temperature molten salt of antimony

The invention discloses a clean metallurgical method for low-temperature molten salt of antimony, and belongs to the metallurgical field of non-ferrous metals. The method is characterized by comprising the following steps of: performing reductive sulfur-fixing melting on antimony concentrate and oxide of metal with higher sulfur affinity compared with the antimony in low-temperature inert molten salt to generate liquid metal antimony and sulfur-fixed metal sulfide, and forming molten salt slag by using the sulfur-fixed metal sulfide and non-reacted substances as solid substances; and separating most inert molten salt from the solid substances and then thermally returning the most inert molten salt to the melting process, regenerating NaHCO3 for recycling by using the molten salt slag through a 'water leaching-carbonated precipitation' process, reclaiming the sulfur-fixed metal sulfide concentrate for selling from the leached residue by ore dressing, or performing roasting desulfuration on the leached residue for heat energy utilization and smoke acid making, and returning oxide roasting sand serving as a sulfur-fixing agent to the melting process. The method greatly reduces the antimony melting temperature, produces the crude antimony at one step, realizes reclamation of sulfur and energy utilization of sulfide, thoroughly eliminates environmental pollution of low-concentration SO2 smoke at the same time of simplifying the flow, reducing the cost and greatly improving the direct yield of the antimony, and has the advantages of low carbon, cleanness and high efficiency.
Owner:CENT SOUTH UNIV

Preparation method of boron carbide superfine powder

ActiveCN107758670ADifficult to operateLarge controllable difficultyCarbon compoundsBrickBoron carbide
The invention discloses a preparation method of boron carbide superfine powder. The preparation method is based on a boron carbide smelting device which comprises a smelting furnace body built with refractory bricks and a sunken cover plate buckled at a top opening of the smelting furnace body, wherein a positive pole and a negative pole communicating a power supply are inserted into the side wallof the smelting furnace body. The preparation method comprises the following steps: S1, mixing a boron source with a carbon source fully to obtain a smelting raw material; S2, fully filling the smelting furnace body with the smelting raw material and covering the furnace with the sunken cover plate; and S3, applying a voltage to heat the smelting raw material to 1500-1900 DEG C and keeping the temperature for 24-48h to obtain the boron carbide superfine powder. Boron carbide is prepared by means of a nearly closed high-temperature treatment method according to the preparation method disclosedby the invention, so that impurity pollution is reduced, the product is good in crystallinity, the primary content of the obtained boron carbide superfine powder is greater than 96%, and the productgraded meets the demand of an abrasive material, and meets the quality demand on boron carbide powder in the field of grinding industry or engineering ceramics.
Owner:QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI +1

Crude zinc smelting method and smelting kiln used thereby

The invention discloses a crude zinc smelting method and a smelting kiln used thereby. The method comprises the following steps: a pyrometallury technique is adopted for smelting and the smelting steps comprise loading, preheating, high-temperature smelting and condensing; the smelting kiln is internally provided with a preheating section, a high-temperature smelting section and a condenser; the raw materials are loaded into the smelting kiln by a feed inlet of the smelting kiln, and then enter the high-temperature smelting section for heating after the preheating section is preheated, and thegenerated zinc steam enters the condenser for condensation; the condensed waste gas enters the preheating section to preheat the raw material, and is exhausted out the smelting kiln by a gas outlet arranged on the smelting kiln, and the waste gas uses a cloth bag for removing dust; and the zinc solution generated by condensation is discharged to a zinc storing tank by a liquid outlet arranged onthe smelting kiln, and the waste residue is discharged out the smelting kiln by a spiral residue-discharging device arranged at the tail part of the smelting kiln. The invention is characterized by small occupied area, large yield, high heat utilization ratio, high recovery ratio, low production cost, capability of treating various renewable zinc ash raw materials and the like, not only is suitable for crude zinc smelting, but also is suitable for smelting other similar non-ferrous metals.
Owner:徐建成

Low-temperature fused salt electrolytic cleaning metallurgy method and device for antimony

ActiveCN107326400AEfficient separationReduce pyro-smelting temperatureCellsElectrodesEnvironmentally friendlyPulse current
The invention relates to a low-temperature fused salt electrolytic cleaning metallurgy method and device for antimony. The method comprises the steps that antimony-containing materials and inert molten salt are mixed and arranged in a low-temperature fused salt electrolyzer in a certain material arrangement mode, and low-temperature fused salt electrolytic smelting is conducted under the certain temperature and pulse current conditions. Along with low-temperature fused salt electrolysis, mixed molten salt in a hearth gradually forms a three-layer melt structure. The antimony-containing materials can be added from an antimony-containing material charging port, and obtained liquid antimony can be discharged from an antimony discharging port formed in the lower portion. Accordingly, the existing antimony concentrate pyrogenic attack temperature is greatly lowered, and high-grade antimony is produced through one step; compared with an existing antimony concentrate pyrometallurgy technology, the method has the advantages of being low in energy consumption, high in direct recovery rate of antimony, clean and environmentally friendly. The device is simple and practical, and a good antimony extraction metallurgy effect can be obtained by using the device in a matched mode.
Owner:CENT SOUTH UNIV

Full-quantification and high-value utilization method of electric furnace fly ash and iron extraction tailings thereof

The invention discloses a full-quantification and high-value utilization method of electric furnace fly ash and iron extraction tailings thereof. The method comprises the following processing procedures: (1) pellet preparation, (2) vacuum smelting, (3) vacuum cooling, (4) magnetic separation and recovery of high-purity Zn-Pb alloy, and (5) preparation of sintered bricks from zinc extraction tailings. According to the method, the Zn-Pb alloy is prepared through carbon thermal reduction and assisted by vacuum smelting of the electric furnace dedusting ash iron extraction tailings, the sintered bricks are prepared through the tailings of the Zn-Pb alloy, the high-purity Zn-Pb alloy product and the sintered brick product with the purity larger than or equal to 96.0% are prepared, full-quantization and high-value utilization of the electric furnace dedusting ash and the iron extraction tailings of the electric furnace dedusting ash are achieved, and economic benefits and environmental benefits are remarkable. The method provided by the invention overcomes the defects of long process flow, high cost, large emission, low added value of products and the like in the prior art, and has wide market popularization and application prospects.
Owner:SINOSTEEL MAANSHAN INST OF MINING RES +1

A kind of preparation method of boron carbide ultrafine powder

ActiveCN107758670BDifficult to operateLarge controllable difficultyCarbon compoundsFire brickCrystallinity
The invention discloses a preparation method of boron carbide superfine powder. The preparation method is based on a boron carbide smelting device which comprises a smelting furnace body built with refractory bricks and a sunken cover plate buckled at a top opening of the smelting furnace body, wherein a positive pole and a negative pole communicating a power supply are inserted into the side wallof the smelting furnace body. The preparation method comprises the following steps: S1, mixing a boron source with a carbon source fully to obtain a smelting raw material; S2, fully filling the smelting furnace body with the smelting raw material and covering the furnace with the sunken cover plate; and S3, applying a voltage to heat the smelting raw material to 1500-1900 DEG C and keeping the temperature for 24-48h to obtain the boron carbide superfine powder. Boron carbide is prepared by means of a nearly closed high-temperature treatment method according to the preparation method disclosedby the invention, so that impurity pollution is reduced, the product is good in crystallinity, the primary content of the obtained boron carbide superfine powder is greater than 96%, and the productgraded meets the demand of an abrasive material, and meets the quality demand on boron carbide powder in the field of grinding industry or engineering ceramics.
Owner:QINGHAI INST OF SALT LAKES OF CHINESE ACAD OF SCI +1

Clean metallurgical method for low-temperature molten salt of lead

The invention discloses a clean metallurgical method for low-temperature molten salt of lead. Lead sulfide concentrate, secondary lead raw material or secondary material of lead is smelted in low-temperature inertial molten salt and rough lead is refined in one step; and a metal oxide is used as a sulfur fixing agent, wherein the smelted product comprises liquid metal lead and solid sulfur-fixingmetal sulfide and the solid sulfur-fixing metal sulfide and solid unreacted material are together called solid matter; the majority of the inertial molten salt is separated from the solid matter to return the smelting process in hot state; a small part of the inertial molten salt adhered by the solid matter is processed by a wet method for recycling; the solid matter after the molten salt is removed by soaking is subjected to ore dressing to recover associated metal and the sulfur-fixing metal sulfide; the sulfide is baked for desulfurization; the smoke is used for making acid; and the oxide is calcined and returned to the smelting process and used as the sulfur fixing agent. The method greatly reduces the metallurgical temperature of the lead, produces the rough lead in one step, realizes the recovery of the sulfur and the utilization of the sulfide energy source, has simple flow and low cost, greatly improves the yield of the vertical force and completely eliminates the lead steam produced during the metallurgical process and the pollution caused by the SO2 smoke to the environment.
Owner:CENT SOUTH UNIV

A low-temperature molten salt electrolytic clean metallurgy method and device for bismuth

The invention discloses a low-temperature fused salt electrolytic cleaning metallurgy method and device for bismuth. The method comprises the following steps: mixing a bismuth-containing material withinertia fused salt, putting the mixture into a low-temperature fused salt electrolysis device in a certain material distribution manner, and performing low-temperature fused salt electrolytic smelting under certain temperature and pulse current conditions; and along with low-temperature fused salt electrolysis, gradually forming a "three-layer melt" structure by the mixed fused salt in a furnacehearth, wherein the bismuth-containing material can be continuously added from a feeding port, and obtained liquid bismuth can be discharged from a lower bismuth discharging port. According to the low-temperature fused salt electrolytic cleaning metallurgy method, the treatment temperature of an existing bismuth concentrate pyrogenic process is substantially reduced; high-quality bismuth can be produced by one step; and compared with a smelting process of the existing bismuth concentrate pyrogenic process, the low-temperature fused salt electrolytic cleaning metallurgy method has the advantages of low energy consumption and high direct bismuth recovery rate. The device disclosed by the invention is simple and practical; and by cooperative use, the device can achieve a good bismuth extraction metallurgy effect.
Owner:YIYANG SHENGLI CHEM IND

Crude zinc smelting method and smelting kiln used thereby

The invention discloses a crude zinc smelting method and a smelting kiln used thereby. The method comprises the following steps: a pyrometallury technique is adopted for smelting and the smelting steps comprise loading, preheating, high-temperature smelting and condensing; the smelting kiln is internally provided with a preheating section, a high-temperature smelting section and a condenser; the raw materials are loaded into the smelting kiln by a feed inlet of the smelting kiln, and then enter the high-temperature smelting section for heating after the preheating section is preheated, and the generated zinc steam enters the condenser for condensation; the condensed waste gas enters the preheating section to preheat the raw material, and is exhausted out the smelting kiln by a gas outlet arranged on the smelting kiln, and the waste gas uses a cloth bag for removing dust; and the zinc solution generated by condensation is discharged to a zinc storing tank by a liquid outlet arranged onthe smelting kiln, and the waste residue is discharged out the smelting kiln by a spiral residue-discharging device arranged at the tail part of the smelting kiln. The invention is characterized by small occupied area, large yield, high heat utilization ratio, high recovery ratio, low production cost, capability of treating various renewable zinc ash raw materials and the like, not only is suitable for crude zinc smelting, but also is suitable for smelting other similar non-ferrous metals.
Owner:徐建成
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