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34results about How to "Reduced reunion tendency" patented technology

Method for preparing flame-retardant expandable polystyrene spheres containing delamination graphite

The invention discloses a method for preparing flame-retardant expandable polystyrene spheres containing delamination graphite, relates to a method for preparing flame-retardant expandable polystyrene spheres, and aims at solving the technical problems that the expandable polystyrene containing delamination graphite containing graphite granules prepared by the existing method is polymerized and easily aggregated in a suspension manner, the graphite granules are uneven to disperse in polystyrene, and poor in flame-retardant insulation performance of the expandable polystyrene. The preparation method disclosed by the invention comprises the following steps: 1, weighing raw materials according to parts by weight; 2, preparing a first mixture; 3, preparing a second mixture; 4, adding the second mixture to the first mixture under agitation, adding an emulsifier after reaction, continuing to react, and then adding pentane, charging nitrogen into a reaction kettle, heating up and reacting, naturally cooling after reaction is ended, slowly releasing a gas and discharging until the pressure is zero; washing and drying, so as to obtain the flame-retardant expandable polystyrene spheres containing delamination graphite. The method is applied to the field of preparation of the flame-retardant expandable polystyrene spheres.
Owner:HARBIN INST OF TECH

Method for preparing nanometer toughened inorganic transparent protective coating

The invention relates to the field of inorganic coating, and aims to provide a method for preparing nanometer toughened inorganic transparent protective coating. The method includes weighing various raw components according to set weight percentages; adding methyl silicate, phosphate, nanometer fillers, dispersing agents, surfactants and deionized water into ingredient barrels, and stirring the methyl silicate, the phosphate, the nanometer fillers, the dispersing agents, the surfactants and the deionized water to form mixed slurry; injecting the mixed slurry into nanometer ball mills and grinding the mixed slurry; adding water glass and defoaming agents into dispersion machines, stirring the water glass and the defoaming agents and then adding the ground mixed slurry into the dispersion machines; continuing to stir the water glass, the defoaming agents and the ground mixed slurry to obtain the nanometer toughened inorganic transparent protective coating. The method has the advantages that inorganic coating is toughened by nanometer materials, and accordingly good toughening effects can be realized without deterioration of the mechanical properties (such as the hardness and the abrasion resistance), the water resistance, the aging resistance and the like of coatings; the nanometer materials are stable in performance and can be mixed with the strong-alkalinity inorganic coating without qualitative change; fillers are ground by nanometer sanders, the particle sizes of the fillers can be reduced and are smaller than or equal to 0.2 micrometer, accordingly, the method is favorable for preparing transparent inorganic coatings, the trend of agglomeration of the nanometer fillers can be weakened, and the toughening effects can be effectively realized by the nanometer fillers.
Owner:TAIZHOU BRANCH ZHEJIANG-CALIFORNIA INT NANOSYSTEMS INST

Modified grinding-aiding early strength agent for steel slag as well as preparation method and application method of modified grinding-aiding early strength agent

ActiveCN112919832AIncrease profitGood early strength grinding aidAlcoholSlag
The invention discloses a modified grinding-aiding early strength agent for steel slag as well as a preparation method and an application method of the modified grinding-aiding early strength agent, and relates to the field of steel slag grinding aiding. The modified grinding-aid early strength agent comprises (a) 60%-75% of ester compounds based on the total weight of the modified grinding-aid early strength agent; (b) 5%-15% of polyacrylic acid based on the total weight of the modified grinding-aid early strength agent; (c) 10%-35% of alcohol amine and acrylic acid monomers based on the total weight of the modified grinding-aid early strength agent, the preparation method comprises the following steps: adding water into alcohol amine and acrylic acid, uniformly mixing, heating while stirring, reacting at 60-80 DEG C for 3-4 hours, and cooling the solution to room temperature to obtain the modified grinding-aiding early strength agent which is applied to grinding of a gel material with high doping amount of steel slag, so the problems of low grinding efficiency of an existing grinding aid, low activity of the steel slag in the early stage, complex synthesis process, high cost and the like are solved. The preparation process is simple, the raw material cost is low, the finished product quality and performance are stable, the use effect is good, and the 7d strength increase is greater than or equal to 30%.
Owner:安徽马钢嘉华新型建材有限公司 +1

Soft nanometer micro area flexibility-enhanced PET composite material and preparation method thereof

The invention discloses a soft nanometer micro area flexibility-enhanced PET composite material and a preparation method thereof. The flexibility-enhanced PET composite material comprises the following components in mass percent: 80 to 93 percent of polyethylene terephthalate, 1 to 5 percent of a porous nanometer inorganic powder, 5 to 10 percent of liquid low polymers, 1 to 5 percent of polar grafted polymers, and a proper amount of an antioxidant. The method comprises the steps of grinding PET into a powder after the PET is cooled, soaking the nanometer inorganic powder through the liquid low polymer, so as to ensure that the nanometer inorganic powder is sufficiently soaked and absorbed by the liquid low polymer and to form a soft and elastic spherical nanometer structure, and improving the wetting property of the surface of the nanometer inorganic powder through the polar grafted polymer, so as to ensure that the nanometer inorganic powder can be uniformly dispersed in a PET matrix and a soft nanometer micro area can achieve the effect of flexibility enhancement in the PET. A PET sheet produced by adding the flexibility-enhanced composite material has excellent impact property, and maintains good optical property.
Owner:中山京工高分子材料有限公司

A preparation method of flame-retardant expandable polystyrene pellets containing exfoliated graphite

The invention discloses a method for preparing flame-retardant expandable polystyrene spheres containing delamination graphite, relates to a method for preparing flame-retardant expandable polystyrene spheres, and aims at solving the technical problems that the expandable polystyrene containing delamination graphite containing graphite granules prepared by the existing method is polymerized and easily aggregated in a suspension manner, the graphite granules are uneven to disperse in polystyrene, and poor in flame-retardant insulation performance of the expandable polystyrene. The preparation method disclosed by the invention comprises the following steps: 1, weighing raw materials according to parts by weight; 2, preparing a first mixture; 3, preparing a second mixture; 4, adding the second mixture to the first mixture under agitation, adding an emulsifier after reaction, continuing to react, and then adding pentane, charging nitrogen into a reaction kettle, heating up and reacting, naturally cooling after reaction is ended, slowly releasing a gas and discharging until the pressure is zero; washing and drying, so as to obtain the flame-retardant expandable polystyrene spheres containing delamination graphite. The method is applied to the field of preparation of the flame-retardant expandable polystyrene spheres.
Owner:HARBIN INST OF TECH

A kind of molecular sieve with multi-level pores and wide silicon-aluminum ratio euo structure and its synthesis method

The invention discloses a EUO (Europium Oxide) structural molecular sieve with hierarchical pores and wide silica-alumina ratio and a synthetic method. The synthetic method comprises the following steps: performing crystallization synthesis by taking a long-chain silane compound as a crystallization assistant, taking double quaternary ammonium salt with an alkane structure being substituted by a double quinary heterocyclic group as an organic template, and heating silica-aluminum sol to a target temperature at the rate of 2 to 20 DEG C / h, wherein the target crystallization synthesis temperature is 150 to 200 DEG C; then performing separation, washing, drying and roasting to remove the organic template in order to obtain EUO structural molecular sieve raw powder with hierarchical pores andwide silica-alumina ratio, and performing ammonium ion exchange, drying and roasting in sequence to obtain an H-type EUO structural molecular sieve with hierarchical pores and wide silica-alumina ratio. The zeolite molecular sieve provided by the invention has the advantages of hierarchical pore structure, wide silica-alumina ratio range, small grain size, high relative crystallinity and high hydrothermal stability. Reaction evaluation shows high isomerization activity and selectivity of xylene, so that the EUO structural molecular sieve has a very good industrial application prospect.
Owner:CHINA CATALYST HLDG CO LTD

Novel insulating base for ore-smelting electric furnace

The invention discloses a novel insulating base for an ore-smelting electric furnace. The novel insulating base comprises a furnace cover. The furnace cover and an electrode protective screen are connected in an inserting mode. A sealing ring pedestal is arranged at the top end of the furnace cover, and a supporting frame is arranged at the external diameter position of the sealing ring pedestal.A sealing ring II is arranged at the top end of the supporting frame, and the external diameter of the sealing ring II is fixedly connected with the supporting frame. A sealing brick ring is arrangedat the top end of the sealing ring II. An insulating box II is arranged at the external parameter position of the sealing brick ring, and the external diameter of the sealing brick ring is elasticallyconnected with the insulating box II. The insulating box II is fixedly connected with the supporting frame. A sealing ring I is arranged at the top end of the sealing brick ring, and the external diameter of the sealing ring I is fixedly connected with the insulating box II. An insulating box I which is fixedly connected with the insulating box II is arranged on the outer side of the insulating box II. The insulating box I is fixedly connected with a primary beam and a secondary beam. By adoption of the sealing brick ring, the electrode protective screen can effectively achieve insulated connection, and a good insulation effect is achieved. The sealing effect can be improved through the sealing rings, and the protective fixation function is also achieved. The primary beam and the secondary beam are connected with the insulating boxes, and the insulating effect is good.
Owner:临沂鑫海新型材料有限公司

A kind of molecular sieve with hierarchical hole euo structure and its synthetic method

The invention discloses a hierarchical-pore EUO structure molecular sieve and a synthesis method thereof. The synthesis method comprises the following steps: crystallizing and synthesizing an silicon-aluminium solution by raising to target temperature at the heating rate of 2-20 DEG C / h by taking a long-chain silane compound as a crystallization assistant and biquaternary ammonium salt of a bi-hexa-heterocycle group substituted alkane structure as an organic template agent, wherein the target crystallizing and synthesizing temperature is 150-190 DEG C; then separating, washing, drying and roasting to remove the organic template agent to obtain a hierarchical-pore EUO structure molecular sieve material; and then sequentially performing ammonium exchange, drying and roasting to obtain the H-type hierarchical-pore EUO structure molecular sieve. The zeolite molecular sieve provided by the invention has a hierarchical-pore structure, and is wide in product silicon-aluminium ratio, small ingrain size and high in relative crystallinity, and strong in hydrothermal stability; reaction assessment shows good xylene isomerization activity and selectivity, and therefore, the hierarchical-poreEUO structure molecular sieve has good industrial application prospect.
Owner:CHINA CATALYST HLDG CO LTD

Preparation method of nano toughened inorganic transparent protective coating

The invention relates to the field of inorganic coating, and aims to provide a method for preparing nanometer toughened inorganic transparent protective coating. The method includes weighing various raw components according to set weight percentages; adding methyl silicate, phosphate, nanometer fillers, dispersing agents, surfactants and deionized water into ingredient barrels, and stirring the methyl silicate, the phosphate, the nanometer fillers, the dispersing agents, the surfactants and the deionized water to form mixed slurry; injecting the mixed slurry into nanometer ball mills and grinding the mixed slurry; adding water glass and defoaming agents into dispersion machines, stirring the water glass and the defoaming agents and then adding the ground mixed slurry into the dispersion machines; continuing to stir the water glass, the defoaming agents and the ground mixed slurry to obtain the nanometer toughened inorganic transparent protective coating. The method has the advantages that inorganic coating is toughened by nanometer materials, and accordingly good toughening effects can be realized without deterioration of the mechanical properties (such as the hardness and the abrasion resistance), the water resistance, the aging resistance and the like of coatings; the nanometer materials are stable in performance and can be mixed with the strong-alkalinity inorganic coating without qualitative change; fillers are ground by nanometer sanders, the particle sizes of the fillers can be reduced and are smaller than or equal to 0.2 micrometer, accordingly, the method is favorable for preparing transparent inorganic coatings, the trend of agglomeration of the nanometer fillers can be weakened, and the toughening effects can be effectively realized by the nanometer fillers.
Owner:TAIZHOU BRANCH ZHEJIANG-CALIFORNIA INT NANOSYSTEMS INST
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